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Under the optimized parameters,i.e.,resorcinol to potassium carbonate molar ratio of 1∶0.5,reaction temperature of 155℃-160℃,reaction time of 6 hours-7 hours,and dimethyl acetamide as solvent,the yield of 2,6-dihydroxybenzoic acid was up to 29.38%.

溶剂羧化法Kolbe-Schmitt反应,是在有机溶剂氛围中,由酚的成盐和酚盐的羧化两步完成,一直应用在农药、医药以及化肥的合成过程中。

The reaction mixture was cooled to 10 °C and excess liquid ammonia added to form the acyclic carbamate 13 in 95% yield.

在反应混合物冷却到10 ° C和过剩的液氨补充,形成环氨基甲酸酯类13 95 %的产量。

Pulp mill used with a view to fuel aerification and gas turbine technology 2020, raise steam of electric power / to yield rate.

废水经过回收、利用和蒸发,使工厂的废水排放接近"0"排放。2020年纸浆厂将着眼于采用燃料气化和燃气轮机技术,提高电力/蒸汽的产出比率。

It may cut against the grain of human nature to yield the power to decide.

它可能会cut againt屈服于势力而作出决定的人的天性。

Sodium cyclohexanoloxyacetate was synthesized by 1mol︰1.15mol of cyclohexyl sodium alcoholate to sodium chloroacetate at 135145℃.The reaction time was 2.5h and the yield was about 81%.The sodium cyclohexanoloxyacetate was acidified by HCl to get the intermediate product,2-cyclohexanoloxyacetic acid.

以摩尔比为1︰1.15的环己醇钠和氯乙酸钠为原料,在135145℃下反应合成了环己氧基乙酸钠,反应时间为2.5h,收率约为81%,再将环己氧基乙酸钠用盐酸酸化制得中间体环己氧基乙酸。

In the third step, when the ratio of racemic ester to benzenesulfonyl chloride to triethylamine to catalyst 4-DMAP is 1:1:1:0.1 in 10℃, the yield is 82.9% and high purity is obtained by crystallisation.

在第三步磺酰化反应中,得到合成消旋2-苯磺酸基-2(2-氯苯基)乙酸甲酯的较佳反应条件为邻氯扁桃酸甲酯:苯磺酰氯:三乙胺=1:1:1,催化剂4-DMAP用量为摩尔反应物的10%,反应温度为10℃,收率为82.9%,同时用结晶方法获得高纯度的产物。

For the market of the feed from sellers' market transit to buyers' market theses years, many feed enterprise face a flinty position, for example, sale yield decreased and produce ability super abound and fixed the scale advantage and higher cost of product, those question lead to the company benefit decreased and even take a heavy effect to the survive of the enterprise.

近几年,饲料行业由卖方市场过渡到买方市场,使大多数业饲料企业形势十分严峻,销售不畅,生产能力过剩,规模优势无法发挥,生产成本居高不下,经济效益明显下降,严重影响到企业的生存。

ABSTRACT: In the presence of sodium t-butoxide and DMSO,ethyl 2-oxocyclopentanecarboxylate was subjected to C-alkylation with 2-(4-bromomethylphenyl)propanoic acid with high regioselectivity to give 2-[4-(1-ethoxycarbonyl-2-oxo-1-cyclopentanylmethyl)phenyl]propanoic acid (4) which was followed by hydrolysis,decarboxylation and salt formation to afford loxoprofen sodium in about 72% overall yield.

在叔丁醇钠和二甲基亚砜的存在下,2-丙酸对2-乙氧羰基环戊酮进行C-烷基化,再经水解脱羧,成盐即得洛索洛芬钠,以2-丙酸计算,总收率为72%。

In the industry believe that each of these "cow" in the steel V-E was the last trading day become the proportion of ultra-holder, was clearly not up to the C of E, but to get the right line climbing Steel shares and then spread through the market or to obtain a higher yield.

业内认为,这些&牛钢虚拟环境中的&各是最后一个交易日成为超比例持有人,显然没有达到权证的,但可以得到正确的路线攀登钢股份,然后通过市场传播,以获得更高的收益率。

The main research work of this dissertation is as follows: Based on the chemical reaction engineering theory and the nitrobenzene electroreduction mechanism, the plate and frame electrolyzer was designed and applied to the process of electroreduction nitrobenzene to p-aminophenol. This dissertation measured the residence time distribution data of the electrolyzer by means of the pulse response method and studied the rule of flow pattern along with the current capacity change. Under different conditions ,this dissertation studied the cyclic voltammetry properties of nitrobenzene on different electrodes by means of the dynamic cyclic voltammetry method and the electrode materials applied to the NB electroreduction have been selected primarily.Baseed on the results of cyclic voltammetry tests, this dissertation used p-electrode systems to measure the steady-state- polarization curves of nitrobenzene on different electrodes in H-type diaphragm cell, and obtained each primary factor s influence rule and the exchange current density value of each electrode.And then on the basis of the conclusions of fundamental researchs upword, the effects of influence factors on the the yield of p-aminophenol and the current efficiency,such as electrode material, current density, quantity of electricity circulated, nitrobenzene concentration . sulpuric acid concentration and so on, have been studied in detail in the systems of hign temperature , strong acidity and oxygen-poorthrough a series of electrolysis experiments in this paper.After all using Pb as anode Monel metal as cathode Dupont Nafion 417 cation-exchange membrane as membrane, this dissertation obtained the optimum technological condition: reaction temperature about 85C, current density 500A m-2, sulphuric acid concentration 20%wt.

论文的主要研究工作为:运用化学反应工程理论,结合硝基苯的电还原机理,设计出用于硝基苯直接电还原合成对氨基苯酚实验的板框式电解槽,并利用脉冲响应法测定了该板框式电解槽的停留时间分布数据,研究了流型随流量变化的规律;通过动态循环伏安法研究了硝基苯在不同电极上、不同条件下的循环伏安特性,初步评选出了用于硝基苯电还原的电极材料;结合循环伏安的测定结果,在H型隔膜电解槽中采用三电极体系测定了硝基苯在不同电极上、不同条件下的稳态极化曲线,得到了各主要因素的影响规律及硝基苯在各个电极上电还原的交换电流密度数值;在基础研究结论指导下,采用板框式电解槽,在高温、强酸、贫氧系统中,进行了一系列的电解实验,分别考察了电极材料、电流密度、通电量、硝基苯浓度、硫酸浓度等因素对收率及电流效率的影响,最终选择以蒙乃尔合金电极作为阴极、铅合金为阳极、Dupont Nofion 417阳离子交换膜为隔膜,得到由硝基苯直接电还原制对氨基苯酚的最佳电解工艺条件:反应温度85℃,电流密度500A·m~(-2),硫酸浓度20%wt。

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Yield To Temptation
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She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了,但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场,你等着挨绳子吧!

Several theories about reigniting and extinguishing of the arc have been refered.

本文综合考虑了几种电弧重燃和熄灭理论。