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The chemical structure of the product was characterized by means of the melting point and IR. The results show that tetraethylammonium bromide which was used as a phase transfer catalyst in this reaction had optimization effect on the interfacial diffusive reaction of BTC and PNP. Higher concentration of sodium hydroxide, lower temperature and a higher dosage of BTC produced a small amount of 4-nitrophenyl chloroformate, while lower concentration of sodium hydroxide and a lower dosage of BTC made reaction incomplete, which affected the yield.

结果表明,在碳酸二(4-硝基苯基)酯合成中使用的相转移催化剂四乙基溴化铵对受界面扩散控制的BTC气与对硝基酚钠反应有良好的相转移催化效果;氢氧化钠质量分数较低时,酚钠盐向溶有BTC的油相扩散速度较小,较高时会产生氯甲酸对硝基苯酯;温度较低、BTC量较高时,会产生少量氯甲酸对硝基苯酯,BTC用量较低会使反应不完全,这些都影响着收率。

The obtained results show:After applying Yelükang ball fertilizer,the active iron in the chlorotic fruit tree leaves increased by 8.7%~20.2%,the chlorophyll content of apple tree increased by 18%;the chlorotic degree of fruit trees decreased 2~3 scales,the yield per tree increased by 56%~89%.

研究结果表明:施用叶绿康球肥可使失绿果树叶片的活性铁提高8.7%~20.2%,苹果叶片的叶绿素含量提高18%;果树失绿程度降低2~3级,果实单产提高56%~89%。

The obtained results show: After applying Yelükang ball fertilizer, the active iron and total iron in the chlorotic peach tree leaves increased by 18.7%~19.5%, the chlorotic degree of peach trees decreased 2~3 scales, the fresh weight and dry weight of 100 leaves also increased apparently; the yield per tree increased by 56%~89%.

结果表明:施用球肥可使桃树叶片失绿程度降低2~3级,百叶重明显增加,单株产量提高56%~89%,全铁和活性铁含量提高18.7%~19.5%,可降低叶片中N,P,K,Cu和Zn的含量,使这些营养元素与铁的拮抗作用减弱。

It stands that the coenobium number is not enough as a basis for fertilization recommendation, and results in the P recommending application rate on the high side and K on the low side. Under the same goal yield, the Monte Carlo method may obtain the average P and K recommending application amounts which are within the P and K optimum application rates based on NP, NK and NPK multivariate representative models in the same experiment sites.

在相同目标产量下,改用Monte Carlo法,平均推荐用量介于相同试验地所建立的氮磷、氮钾和氮磷钾典型肥效模型的推荐用量之间,结果明显优于产量频率分析法。

In the ammonifying procedure, al cohol is used as solvent or phase transfer catalyst is added. The results sh ow that the reaction time decreases evidently and the yield of bactericide in creases further.

在产品制备的胺化步骤,作者采用乙醇作为溶剂或加入相转移催化剂,明显缩短了合成时间,使产品双烷基二甲基溴化铵的产率得到了进一步提高。

Semiconductor industry has been a central figure to the economic growth in Taiwan, especially for the fabrication sector of integrated circuit that has evolved into world-leading status. The fabrication technology advances so far that the feature size (or critical line-width) of IC devices has now broken the 0.1 ?慆 barrier and into the nano-scale age. This progress discloses that the traditional definition of a "cleanroom" environment may become increasingly inadequate because prevention of particulate contamination may no longer be a critical issue. As the condensable organic airborne molecular contaminants depositing on wafer surfaces, it results in deterioration on device performance and reduces semiconductor device yield.

半导体产业已成为我国最重要的经济发展产业,其中积体电路制造技术的快速发展,使我国早已跃升成为世界晶圆代工重镇之一,然而当制程的关键线宽尺寸突破0.1微米而正式进入奈米等级之际,传统针对微粒污染控制所设计之洁净室将无法符合气态分子污染物之洁净需求,其中凝结性有机分子污染物质(organic airborne molecular contaminants)一旦沈积吸附於晶圆表面,将导致元件缺陷与制程良率下降。

In the course of establishing standard operating procedure, The temperature, time , the feasibility without decorticating and efficiency were investigated when alliinase was deactivated used a dry heating apparatus in tunnel type, but the efficiency can be achieved less than 70%, need to be improved; The reformative cribriform plate has been proved to be good in practice result in pulping enzyme-deactivated garlic without dehulling; The extraction efficiency achieved more than 90% when volumic ratio of 20% alcohol and water is 3 I 1 and 2:1 was adopted to extract alliin two times respectively; During exact filtration, the ratio of diatomite in precoating and filtration was 3% and 1% respectively, the losses of alliin adsorbed by diatomite in extraction solution were not remarkable. In the stage of alliin isolation by ion exchange resin, three simple and sensitive detected measures were successfully adopted to control the whole process; the efficiency of alliin isolation was similar to laboratory results; The alliin yield was over 50% in acidic fractions and the purity quotient of alliin achieved above 50% after drying; Furthermore, the phenomenon was found that losses of alliin were seriously affected by the temperature and time periods in concentration.

在制定中试生产标准操作规程中,考察了隧道式干热烘干机杀酶的温度、时间和效率,干热灭酶效率只能达到70%,待改进;改良的筛板使带皮打浆效果良好,证明非脱皮熟蒜打浆的可行性,减少了工序,降低了成本;提取过程中,20%酒精分别1∶3和1∶2提取2次,效率达90%以上;硅藻土板框过滤时,探索了精滤过程中提取液中预涂和过滤时硅藻土的比例分别为3%和1%,并考察硅藻土对蒜氨酸的吸附损失,滤液澄明度良好,蒜氨酸损失很少;在树脂吸附分离阶段,采用三种简便灵敏检测手段控制生产过程,分离蒜氨酸的效果与实验室一致,酸性流分中蒜氨酸收率可达50%以上,干燥后蒜氨酸纯度达50%以上;试验发现浓缩蒜氨酸洗脱液时温度和浓缩时间对蒜氨酸损失的具有很大影响。

Under the instruction of above-mentioned theoretical results, in the thesis chapter 10, the strongly electron-withdrawing anion, C_5O_5~(2-)[dianion of croconic acid (4,5-dihydroxycyclopent-4- ene-1,2,3-trione)], was chosen as the chelator to coordinate with boron to form lithium salt, which will yield high ionic conductivity solutions, and exhibit wide electrochemical stability windows and high thermal stability. As described in the chapter, two new lithium salts containing C_5O_5~(2-), lithium bisborate and its novel derivative, lithium borate for Li-ion battery electrolytes were synthesized.

在上述理论结果的指导下,论文第十章选择了克酮酸二价阴离子——具有很强的酸性、较好的芳香性、较大的电荷分散性、形成的配合阴离子具有较显著的共轭性——作为配体与B配位,合成了二种新的锂盐,通过实验测定了它们的结构和在有机溶剂中的溶解性。

The results indicated, catalytic activity was very high, the average rate of O 2 uptake was 4.25×10 -2 mmol/min after 10 min, the yield of cyclopentanone was up to 83%.

实验结果表明,该催化体系对环戊烯的羰基化显示出较高的催化活性,反应 1 0 min,反应的平均吸氧速率为 4.2 5× 1 0 -2 mmol/min,环戊酮的收率可达 83%。

Results indicated that rate of delignification is 84.12% and pulp yield is 38.12% under the pulping conditions.

结果表明,该蒸煮体系对稻草木质素的脱除率达到85 。1 2 %,纸浆得率

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

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However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。