查询词典 x ray diffraction

A new photochromic organic compound of thiosemicarbazone, 4-( p -bromo-α-methylaminothiocarbonyl hydrazonobenzal)-2,5-dihydro-3-methyl-5-oxo-1-phenyl pyrazole, was synthesized and characterized by elemental analyses, IR, 1H NMR spectra, and X-ray single-crystal diffraction analysis.

文章合成了一个新的有机化合物1-苯基-3-甲基-4-对溴苯亚甲基-吡唑啉酮-5 缩甲基氨基硫脲(1)，并分别用元素分析、红外光谱、氢核磁共振及X-射线单晶衍射对化合物的结构进行了确证和表征。

Two new binuclear complexes, [TpCu(μ-1, 1-N3)2CuTp](1) and [Tp(superscript *)Co2CoTp(superscript *)](2) Tp=tri (pyrazolyl borate and Tp(superscript *)=3,5-dimethyltri borate, have been synthesized and characterized by IR, UV-vis, ESR, and CV. The crystal structures of both complexes have been determined by X-ray single crystal diffraction.

合成了两个新型的含三吡唑硼配体的双核铜配合物[TpCu(μ-1， 1-N3)2CuTp](1)和双核钴配合物[TpCo2CoTp](2)，并通过IR，UV-vis，EPR，CV，X-射线单晶衍射等手段进行表征。

Provided are carbide derived carbon materials prepared by thermochemically reacting carbide compounds and a halogen containing gas and extracting all atoms of the carbide compounds except carbon atoms, wherein the intensity ratios of the graphite G band at 1590 cm -1 to the disordered-induced D band at 1350 cm-1 are in the range of 0.3 through 5 when the carbide derived carbon is analyzed using Raman peak analysis, wherein the BET surface area of the carbide derived carbon is 1000 m 2 /g or more, wherein a weak peak or wide single peak of the graphite (002) surface is seen at 2 = 25 DEG when the carbide derived carbon is analyzed using X-ray diffractometry, and wherein the electron diffraction pattern of the carbide derived carbon is the halo pattern typical of amorphous carbon when the carbide derived carbon is analyzed using electron microscopy.

提供了得自碳化物的碳，其通过热化学反应碳化物化合物和含卤族元素的气体并提取除了碳原子之外的碳化物化合物的全部原子制备，其中当使用拉曼峰分析法分析该得自碳化物的碳时，在1590cm -1 的石墨G波段与在1350cm -1 的无序引发的D波段的强度比为0.3至5，其中该得自碳化物的碳的BET表面积是1000m 2 /g或更大，其中当使用X射线衍射法分析该得自碳化物的碳时，在2θ＝25°观察到石墨(002)面的弱峰或宽单峰，以及其中当使用电子显微法分析该得自碳化物的碳时，得自碳化物的碳的电子衍射图是代表无定形碳的晕图案。该发射体具有良好的均匀性和长寿命。可以使用比用于生产常规碳纳米管的方法更廉价的方法制备发射体。

In this article, three novel cyclopalladated ferrocenylimine triphenylphosphine complexes 2-4 were easily synthesized and characterized by elemental analysis, IR, 1H NMR, 31P NMR and X-ray single crystal diffraction.

为筛选高效催化Suzuki反应的催化剂，合成了3种新的环钯化二茂铁亚胺-三苯基膦配合物2~4，经元素分析、红外光谱和核磁共振谱对其结构进行了表征，并通过X射线单晶衍射测定了化合物3的晶体结构。

A chiral phase transfer catalyst, N-benzyl quinine bromide, was synthesized from natural chiral compound. And 2,5-bimethyl-4-(3-nitrobenzene)-1,4-bihydrogenation pyridine-3--4-methyl formate (viz. nitrendipine) was synthesized by this chiral phase transfer catalysis, and characterized by elemental analysis, infrared spectrum,1H nuclear magnetic resornace, and X-ray single-crystal diffraction.Key words: ammonium; chiral phase transfer catalyser; crystal structure

通过对天然手性物质进行修饰合成手性相转移催化剂N-苄基溴化奎宁，并对目标分子2，5-二甲基-4-(3-硝基苯)-1，4-二氢吡啶-3-甲酸乙酯-5-甲酸甲酯进行不对称催化合成，并通过红外光谱和核磁共振氢谱对化合物进行了表征，用X射线单晶衍射法测定了该化合物的晶体结构。

The complex fluorides were characterzed by means of X-ray powder diffraction, environmental scanning electron microscopy and fluorescence spectrometry.

运用X射线衍射、环境扫描电子显微镜和荧光光谱等测试技术对所制备产物进行了表征。

The gemological characteristics of lemon-yellow serpentine jade are studied by the conventional gemology instrument and the polarizing microscope; the Fourier transform infrared spectroscopy, ultraviolet-visible light absorption spectra, X-ray power diffraction and electron probe quantitative analysis have also been used to study the lemon-yellow serpentine jade.

通过常规的宝石学仪器和偏光显微镜来研究柠檬黄色的蛇纹石玉的宝石学性质，进一步用Fourier变换红外光谱、紫外－可见吸收光谱、X射线粉晶衍射和电子探针定量分析对柠檬黄色的蛇纹石玉进行研究，结果表明：这种柠檬黄色的蛇纹石玉主要成分为利蛇纹石，含有少量的纤蛇纹石、水镁石、橄榄石、菱镁矿等。

A total of fifteen metal complexes have been synthesized and characterized by means of elemental analysis, molar conductance analysis, IR, electronic spectra, EDS, X-ray powder diffraction analysis and TG-DTA analysis.

本文合成了15种金属配合物，应用元素分析、摩尔电导、红外光谱、能量色散谱、X-射线粉末衍射、热重-差热分析等手段对这些配合物进行了常规结构表征，确定了配合物的组成。

METHODS:Nimodipine solid dispersions were prepared using solven t-dispersion with excipientsN as carriers. DTA,X-ray powder diffraction,Scanni ng electron microphotographs and Infra-red spectra were used to determine the s tatus of nimodipine in carriers, and dissolution characteristics were studied in water.

以混合辅料N为载体采用溶剂分散法制备固体分散物，差热分析，X-射线粉末衍射，扫描电镜和红外线光谱鉴别药物在载体中的状态，并进行溶出度研究。

By using the results from systemical petrography, X-ray powder diffraction, and EPMA analyses on the run products from experimental simulaion under constant temperature and pressure, we have explored the paragenesis for the pelites suffering metamorphic dehydration under high pressure condition, the process and mechanism for these metamorphic dehydration, and the relation between the components for garnets, one of the major phases in the paragenesis, and the experimental conditions including pressure, temperature, and chemical compositon in a system.

由恒温、恒压实验产物系统的岩相学、X射线粉晶衍射和电子探针分析，揭示了天然泥质岩发生高压变质脱水作用后的矿物相组合，确定了泥质岩高压变质脱水作用的过程和机理，以及主要矿物相石榴子石的组成与压力、温度和体系化学组成的关系。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。