查询词典 x ray diffraction

[Cu2(H2O)4]2 was prepared by the reaction of aqueous 1,2,4-triazol-5-one solution with the solution of copper picrate Cu2 and characterized by elemental analysis, FT IR and X-ray powder diffraction analysis.

本文通过1，2，4-三唑-5-酮水溶液与苦味酸铜水溶液反应，制备了[Cu2(H2O)4]2，用元素分析、傅立叶变换红外光谱分析、X-射线粉末衍射分析对其结构进行了表征。

The Scanning electron microscopy is used to study the morphological features of porcelaneous layer s on surface of freshwater cultured pearls from Zhuji, Zhejiang Province, and the calcium carbonate polymorph of porcelaneous layer s is identified by X-ray powder diffraction.

采用扫描电子显微镜对中国浙江诸暨三角帆蚌养殖珍珠表面特别是无珍珠光泽的瓷质层的微形貌进行了研究，并采用X射线粉晶衍射对瓷质层进行了物相鉴定。

The crystal structure of 4,4'- biphenyldicarboxylic acid ethanol solvate, viz.(H2 bpa), has been determined by X-ray single-crystal diffraction technique at room temperature.

利用X-射线单晶衍射技术在室温下测定了4，4'-联苯二甲酸乙醇溶剂化物(H2 bpa)的晶体结构。

The microstructure of subsonic speed flame spraying WC/Ni metal-ceramic coating has been studied by means of X-ray,scanning electron microscopy,transmitting electron microscopy and selected area electronic diffraction techniques etc.

采用X 射线、扫描电镜、透射电镜及选区电子衍射等手段研究了镍包碳化钨金属陶瓷亚音速火焰喷涂层的微观组织结构。

The powders were characterized by X -ray powder diffraction, transmission electron mi croscopy and vibrating sample magnetometer . The as -prepared particle is a aggregate composed of many plannar tetragon crystallites.

采用X射线粉末衍射、透射电镜、穆斯堡尔谱和振动样品磁强计，对合成样品进行表征。

By means of X-ray powder diffraction and infrared spectrum analysis, it is proved thatthe main mineral composition of Luan Chuan nephrite is tremolite, and its every parameterswere very close to those of standard tremolite.

运用 X 射线粉晶衍射和红外光谱对栾川的蛇纹石玉进行了分析，分析显示该地蛇纹石玉由较为纯净的叶蛇纹石组成。

In this paper we utilize the diffraction character of X ray to analyze the parameters of unit cells ...

从X射线的衍射特征，分析了NaY分子筛的单个晶胞和结晶度的参数，并比较了它们的活性，从而找到了结晶度和活性之间的规律。

Notably, compounds 12–14 can be described as a 3D open–framework with nano–channels, compound 15 can be described as a 3D open–framework with double helical channels, while compound 16 can be described as a 3D heterochiral coordination polymer with double helical channels, which can be obtained by spontaneous resolution from the racemic phosphonic acid.X–ray powder diffraction analysis shows that compound 16 is a pure phase. Surface photovoltage spectroscopy of compound 16 indicates that it possesses positive SPV response in the range of 300–600 nm and shows p–type semiconductor characteristic.

值得注意的是，化合物12-14为具有一维纳米孔道结构的三维开放骨架结构，化合物15是具有双螺旋孔道的三维开放骨架结构，而化合物16是外消旋的有机膦酸配体通过自发拆分而形成的具有双螺旋孔道的多手性三维开放骨架结构。X-射线粉末衍射分析表明化合物16为纯相；化合物16的表面光电压光谱分析中，在300-600nm范围内有3个正的光(来源：ABC论文12网www.abclunwen.com)伏响应带，表明它具有p型半导体的特征；化合物16的诱导表面光电压谱进一步确定它的p型半导体的特征；磁性研究表明，化合物16中两Mn原子之间存在弱的反铁磁相互作用。

Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

In this research, two novel compounds in which alkylenedithiomethylene Malonic acid act as the main coordination agents and the compounds containing N atom (such as pyridine, Phenanthroline Ethanediamine and 4,4'-Bipyridinyl) act as the associating coordination agents have been synthesized by the means of solution and solid-liquid diffusing reactions. 9 coordination complexes and polymers have been designed and synthesized in which the transition metals Cu and Zn acted as the centre ions. These compounds have been characterized by X-ray single crystal diffraction analysis, and some properties of them have been tested and analyzed.

本论文设计合成了两种结构新颖的含有二硫缩烯酮结构的丙二酸类化合物，以此为主要配体，以含氮化合物(吡啶、邻菲罗啉、乙二胺和4，4'-联吡啶)为辅助配体，采用常规溶液合成和固-液相扩散等方法，设计合成了9个过渡金属Cu和Zn离子配合物和配位聚合物，采用单晶X-射线衍射等技术对晶体结构表征，并对其部分性质进行了测试和分析。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。