查询词典 x ray diffraction

Two organosulfonate complexes, [M22]·H2O (M=Cd 1, M=Pb 2), were obtained from the reaction of 1,10-phenanthroline, sodium 4-aminonaphthalene-1-sulfonate tetrahydrate and Cd2·2H2O or Pb (NO3)2 in a mixed solvent of water and methanol at 25 ℃. The compounds were characterized by elemental analysis, IR, and X-ray diffraction single crystal structure analyses.

合成了2个新型有机磺酸配合物，[Cd22]·H2O(1)和[Pb22]·H2O(2)(phen=1，10-邻菲咯啉，ans=4-氨基-1-萘磺酸根)，通过元素分析、红外光谱等对配合物进了表征，用X-射线单晶衍射方法测定了配合物的单晶结构。

The tetravalence vanadium was found in V2O5 gel thin films by measuring the electrical resistance change of V2O5 gel thin films with temperature, ESCA and X-ray diffraction analysis. in this paper, from miniamount redox in melting V2O5 and crystal structure, the influencing mechanism of miniamount redox on changing valence of vanadium was analyzed and discussed in detail.

通过对V2O5凝胶薄膜试样的电阻随温度的变化测试和电子能谱和X射线衍射分析发现V2O5凝胶薄膜中有四价钒的存在，本文从V2O5熔体的微量氧化还原和晶体结构的角度分析讨论了微量氧化还原影响钒离子价态变化的机理。

Effects of temperatures on thaumasite formation were investigated.X-ray diffraction,scanning electron microscope,energy dispersive spectrum and laser Raman spectrum analysis were used to identify thaumasite in paste sample stored in 10% of MgSO 4 solution at different temperatures.

研究了环境温度对碳硫硅钙石形成的影响。降浸泡于不同温度的质量分数为10%的MgSO 4 溶液中的含石灰石粉水泥石试样进行X射线衍射分析、扫描电子显微分析、能谱分析和激光Raman光谱分析。

The nematic thermotropic liquid crystalline behaviour of ten kinds of PEAs obtained was studied by polarizing microscope , DSC and X-ray diffraction.

用热台偏光显微镜，DSC和X光衍射方法研究了热致液晶的相转变行为，确认了这十种聚酯酰胺均为向列型热致液晶。

By using synchrotron radiation energy dispersive X-ray diffraction and diamond-anvil-cell technology at room temperature,the in-situ high pressure structure of natural titanite had been studied experimentally.

利用同步辐射和金刚石压腔技术对天然矿物榍石进行原位高压能散模式X射线实验研究，结果表明榍石在3.9 GPa和10.9 GPa分别发生P 21/a→A 2/a和A 2/a→A 1结构相变，并首次确定10.9 GPa→25.1 GPa榍石结构很可能稳定保持A 1相。

One mixed-ligand complex ofnH2Otpa=terephthalate, tripy=4'-(4methyoxyphenyl-2,2':6',2-terpyridine was synthesized and characterized by IR, elemental analysis and thermo-gravimetric analysis. The crystal structure of the product was established by single-crystal X-ray diffraction.

采用水热法合成了新的维链状锌的配位聚合物nH2O（tpa=对苯二甲酸，tripy=4'-（4-甲氧基苯基）－2，2'：6'，2-三联吡啶），通过红外光谱和元素分析对该配位聚合物进行了结构表征，用X射线单晶衍射测定了晶体结构。

Compound 1 and 2 are pure tungstosilicate cluster,the others are transition-metal tungstosilicate clusters All compound characterized by elemental analyses,IR,TG,and single-crystal X-ray diffraction..

其中，前两个化合物为纯硅钨簇，后三个化合物为含有金属的硅钨簇。所有的化合物都通过元素分析，IR，TG和单晶X-射线分析进行了表征。另外，对于化合物3、4和5，我们还对其电化学性质进行了研究。

A three-unite hydrogel that had a thermoresponsive shape memory was prepared by copolymerizing a hydrophobic monomer n-stearyl acrylate with n- undecylenic acid and acrylamide,and its structure and properties were studied by X-ray diffraction,DSC and DMA.

选用疏水性单体丙烯酸十八酯和十一烯酸以及亲水性单体丙烯酰胺制备了三元共聚凝胶P(SA-co-AM-co-HA)，通过X射线衍射、DSC、DMA等对三元凝胶的结构和性能进行了研究，发现三元凝胶形成了有序排列，这种有序排列会随着温度的变化发生可逆转变，从而使凝胶显示较好的形状记忆特性。

The microstructure of the magnesium alloy before and after ECAP were examined by means of OM and TEM. The hardness of the as-extruded and unextruded Mg-6Zn-1Gd-0.6Zr magnesium alloy was examined by vickers hardness tester. The rolling of the crystal plane in the process of ECAP was analyzed by X-ray diffraction.

采用光学显微镜和透射电子显微镜分析了试样ECAP变形前后的显微组织变化，采用显维硬度计对Mg-6Zn-1Gd-0.6Zr合金ECAP变形前后进行了硬度测试，采用X-射线分析法分析了ECAP变形过程中晶面的转动。

The fretting wear experiments were made on nitrogen imp-larted samples and unimplanted samples of 9Crl8Mo steel respectively in this in vestigation. SEM was used to observe the topography of the fretted surfaces. AES and micro-region X-ray diffraction were also used to deter mine the elements distribution and phase construction of the implanted surface tilm and wear track surface.

作者对9Cr18Mo钢的氮离子注入试样及未注入试样进行了微动磨损的对比试验，利用扫描电子显微镜对磨损表面的形貌进行了观察，利用俄歇电子能谱仪和微区X-射线衍射仪对氮离子注入试样表面与磨损表面的元素分布及相组成进行了分析。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。