查询词典 x ray diffraction

X-ray diffraction is one of the most common and efficient ways to measure a superlattice structure. This dissertation displays the detail results for characterization of Ge〓Si〓/Si superlattices by x-ray diffraction (including x-ray small angle diffraction and double crystal diffraction). It was found, when the growth temperature is lower, the intensities of xray small angle diffraction peaks are modulated by a periodical function, which indicates that both sets of interfaces of the superlattice is highly flat; when the growth temperature is higher, the diffraction peak intensities are simply decay with the increase of diffraction vector, which indicates that one set of interfaces is highly flat but another is not; when the growth temperature is very high, the diffraction peaks are reduced more rapidly, which indicates that both sets of interfaces are not ideal.

本文详细介绍了用X-射线衍射（包括X-射线小角衍射和双晶衍射）方法对Ge〓Si〓/Si超晶格结构特性测试的结果，尤其是发现，当Ge〓Si〓/Si超晶格的生长温度较低时，X-射线小角衍射谱峰的强度随着衍射波矢的增加而周期性调制，表明超晶格的两套界面都十分平整；当生长温度较高时，Ge〓Si〓Si超晶格的X-射线小角衍射谱峰的强度随着衍射波矢呈简单的衰减变化，对应于超晶格内有一套界面不平整的情况；当生长温度进一步提高时，X-射线小角衍射峰明显减少，表明超晶格内两套界面都不理想。

It is showed that in the X-ray diffraction patterns of the interlayer solid solution Ti3Si0.9Al0.3C1.93 and Ti3Si0.8Al0.4C1.93 bulk samples,which were in-situ reactively synthesized by hot-pressing the elemental Ti,Si,Al and C mixed powders,the diffraction peaks of [00L] crystal planes are very weak,there is only a small diffraction peak belonging to the [008],and the diffraction peaks belonging...

结果发现，用热压Ti、Si、Al和C混合粉末原位反应合成的Ti3Si0.9Al0.3C1.93和Ti3Si0.8Al0.4C1.93层间固溶体块体样品的X射线衍射谱中[00L]晶面的衍射峰极其微弱，只有[008]面有一个小的衍射峰，[002]、[004]和[006]面几乎没有衍射峰存在，而该块体样品的粉末的X射线衍射谱中所有[00L]晶面的衍射峰均存在。

The changes in phase structure and Curie temperature of the Sm2Fe17 compound after nitrogen absorption were studied by using X-ray diffraction, differential thermal/thermo-gravimetric analyzer and magnetic measurement. The results of X-ray diffraction showed that the diffraction peaks of the Sm2Fe17 compound shifted toward lower angle after nitrogen absorption, and the characteristic peaks of α-Fe were observed. This showed that the unit cell of Sm2Fe17 expanded, the compound was decomposed to a certain extent and the characteristic peaks of α-Fe appeared.

通过X-射线衍射、差热－热重联用仪以及磁测量等手段，研究了Sm2Fe17化合物吸氮后的相结构及居里温度的变化行为。X-射线衍射表明，吸氮后Sm2Fe17化合物的衍射峰向小角度方向偏移，并且出现了α-Fe的衍射峰，这说明吸氮后化合物的晶胞有所膨胀，并且化合物有一定的分解，产生了α-Fe。

X-ray diffraction, reflection high energy electron diffraction and Phi scan of grazing incidence X-ray diffraction with synchrotron radiation were employed to investigate the structure properties of ZnO thin film.

利用X射线衍射，反射式高能电子衍射和同步辐射掠入射X射线衍射φ扫描等实验技术研究了ZnO薄膜的结构。

Probe into theory of X-ray diffraction testing residual stress in glass-ceramic and effect on accuracy of stress with the X-ray diffraction.

探讨了X射线法测量微晶玻璃残余应力的原理及该方法对残余应力值精确度的影响。

In addition, molecular orientation behaviors induced by shearing, electric field and magnetic field were investigated. The space group of the monomers A3EO7 and A9EO7 were determined as P2〓2〓2 and P112/m by means of electron diffraction and X-ray diffraction. Liquid crystalline properties of the monomer and the polymer were studied using DSC, variable X-ray diffraction, TEM and polarized optical microscope. Both monomers exhibit monotropic liquid crystalline behavior, and they also give a metastable phase on the cooling process. The polymer PA9EO7 shows enantiotropic liquid crystalline properties. Thus the rigid polymer backbone is not a fatal defect that completely distorts the packing arrangement of the mesogenic moiety in the side chain liquid crystalline polyacetylene.

结合电子衍射倾转方法和粉末X射线衍射技术，确定了两个液晶小分子A3EO7和A9EO7的晶胞参数和空间群，采用Cerius〓模拟软件，运用分子模拟的方法给出了小分子在晶胞中的排列方式；利用DSC、变温X射线衍射技术和透射电子显微镜研究了小分子和聚合物的液晶态，单体A3EO7和A9EO7表现出单向液晶性质，并且在降温过程中都表现出一个亚稳液晶相或亚稳结晶相，聚合物PA9EO7具有双向液晶性；采用偏光显微镜和X射线平板照相技术，研究了剪切和电场对聚合物分子取向的影响，在不同的液晶态，剪切作用对聚合物PA9EO7具有不同的诱导取向结果，直流电场可以诱导聚合物联苯液晶基元沿施加电场方向取向。

The grafting of polycaprolcatone on starch by ring-opening polymerization of e -caprolactone was initiated from the starch hydroxyl functions in the presence of a catalyst such as stannous octoate Sn(0ct2, Dibutyltin dilaurate or titanium tetrabutoxide. The grafting ration could reach 16%. IR, X-ray diffraction and DSC were used to investigate the grafting-polymer.

在辛酸亚锡Sn(Oct_2、二月桂酸二丁基锡和钛酸丁酯等催化剂作用下，淀粉羟基引发己内酯单体进行配位聚合，淀粉接枝率可以达到16％，并通过红外光谱、X—ray衍射及DSC等测试手段对反应产物进行了表征。

Three classes, forty-eight in total, of pyrazole compounds, imidazolo[1,2-b] pyrazoles, dipyrazolylmethanones and pyrazolyloxadiazoles, have been synthesized, and they have been fully characterized by modern spectroscopic methods, two of which were further confirmed by X-ray diffraction. Most of these compounds have been evaluated for the inhibitions of Gram-positive bacterium represented by Staphylococcus aureus and Gram-negative bacterium represented by Klebsiella pneumoniae.

论文合成了咪唑并[1，2-b]吡唑类、二吡唑基甲酮类和吡唑连噁二唑类共三类48个化合物，使用了现代结构测试手段对所合成的化合物进行了结构表征，其中两个化合物经过了X-Ray射线衍射分析，并对其中大部分化合物进行了以金黄色葡萄球菌和肺炎克雷白杆菌为代表的革兰氏阳性菌和革兰氏阴性菌的初步抑菌活性测试。

Pressure induced amorphous transition of LiB 3O 5 has been investigated by using in situ high pressure X ray powder diffraction and energy dispersive X ray diffraction with synchrotron radiation at the pressure up to 45 1GPa.

采用X射线粉末衍射和同步辐射能散X射线衍射技术，对LiB3O5晶体进行了压致非晶化相变的研究，压力达45.1GPa。

Microscopic characteristics of cladded crystal fiber are analyzed by X-ray diffraction, Laue X-ray diffraction and scanning electron microscopy, it is found that magnesium-ion indiffusion does not affect the single crystal structure and the domain structure of the magnesium diffused crystal fiber. It is found for the first time that MgO-rich layer in the magnesium diffused LiNbO〓 surface layer exhibits the crystal structure of an unknown compound from the Li-Mg-Nb-O ternary system and MgNb〓O〓. It is proposed for the first time that this unknown compound and MgNb〓O〓 in MgO-rich layer are the real sources of magnesium-ion indiffusion LiNbO〓. Their appearance indicate that MgNb〓O〓 is in the surface layer of MgO-rich layer, the unknown compound is in the subsurface layer and beneath where the MgNb〓O〓 is located, and these compounds have obviously preferred orientation.

通过镁离子内扩散法，首次在国内实现了具有阶跃和抛物折射率分布的c轴LiNbO〓单晶光纤和a轴Nd：MgO：LiNbO〓单晶光纤的芯—包层波导结构，为我国在该项目的研究填补了空白；建立了晶纤损耗的测量系统，提出了利用单模石英光纤作为晶纤入射光耦合器的思想；通过对晶纤损耗的测量，得到了包层晶纤比未包层晶纤损耗降低约14倍的好结果，并实现了低次模传输：对经镁离子内扩散实现包层后的晶纤的微观特性，利用X射线衍射，劳厄照相和扫描电镜表征发现，晶纤并不因镁离子的内扩散而影响其单晶结构和镁的扩散层畴的变化。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。