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The results show that among the acetoacetonate complexes,Co_3 has the best catalytic activity.The optimum reaction conditions were as follows:0.764 mmol of Co_3,mole fraction of ethanal 10%based on the substrate,room temperature,oxygen pressure 2 MPa,reaction time 11h and solvent acetonitrile.Under these conditions,13.3%p-chlorobenzaldehyde was obtained with 15.3%conversion and 87.2%selectivity.The oxidation can also be carried out without solvent with 8.1%conversion,89.1%selectivity and 7.2%yield respectively.
在金属配合物中Co_3的催化性能最好,在其用量为0.764 mmol、乙醛用量为反应物物质的量的10%、氧气压力为2MPa时,以乙腈为反应介质,室温下反应11h,反应的转化率和选择性可达15.3%,87.2%,对氯苯甲醛收率可达13.3%;反应也可在无溶剂时进行,此时反应的转化率、选择性及醛的收率分别为:8.1%,89.1%,7.2%。
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The volume ratio of furaldehyde to acetic anhydride is 1∶2; the mole ratio of furaldehyde with anhydrous potassium carbonate is 1.00∶0.54. The best phase transfer catalyst is PEG1000, the mass ratio of PEG1000 with furaldehyde is 4.3%, the reaction time is 11 min, the reaction power of microwave is 260 W. The yield ofα-furanacrylicacid is up to 72.3% under these reaction conditions.
研究结果表明:在微波辐射功率为260 W、微波反应时间为11 min、以聚乙二醇1 000(PEG1000)为相转移催化剂,糠醛与乙酐的体积比为1∶2,糠醛与无水碳酸钾的量比为1.00∶0.55时,α-呋喃丙烯酸的产率为72.3%。
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Optimized the preparation of chitosan hydrogel technological conditions, and the result indicated that: the hydrogel with best quality can be gotten, with the chitosan quantity 1 g, the formaldehydevolume 0.2 mL, the gelatination temperature 50℃.
通过试验优化制备壳聚糖水凝胶的工艺条件,试验结果表明:当壳聚糖量为1 g,甲醛体积为0.2 mL,凝胶化温度为50℃时,制备得到的水凝胶质量优良。
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If "winner unique skill " being to know stock market be watched by person,that "the hero is invincible " is to let people how to deal with stock market; If operating method inside the "winner unique skill " is road no in complete set guerrilla detachment play, the regular army who is that the same stuff is entire then "the hero is invincible " handle system does battle general plan, the person looks at coke target-rization, step order-rization, method hipping, behavior normalizes , the effective safe mechanism manage, will bring deep one revolution to deep one revolution unable nothing chapter speculation way , the form deciding share price some classics of checking gimmick along power destiny unexpected turn of events composes in reply 1 agreeing with 3 buying point, Give investor the best having provided marketplace opportunity to grasp, but the high position faction that risk controls sends out one , two sells stopping that point and mark of archives interpose mean, general cover is difficult to be close to the body.
如果说《赢家绝技》是让人看懂股市,那《英雄无敌》就是叫人们怎样对付股市;如果说《赢家绝技》里的操作方法是不成套路的游击队打法,那么《英雄无敌》就是一套完整操作体系的正规军作战方略,其视焦目标化、步骤次序化、方法模式化、行为规范化,安全有效的机制manage,将给无章无法的炒作方式带来一场深刻的革命,决定股价走势命运的变盘手法之若干经典形态和契合3+1买点,给投资者提供了市场机遇的最佳把握,而风险控制的高位派发一、二卖点和分档设置的止损,又将套难于近身。
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Based on the concept and the theory of forest park and forest tourism, development advantages of Hanzhong forest park were identified as follows: i through the past several years'development, forest tourism products were getting so abundant gradually that a fundamental scale was formed, with three national forest parks as well as three province parks founded; ii the idea of"tourism stimulation"was determined as the development strategy in the province since forest tourism played an increasingly significant part in the development of Hanzhong economy and society; iii geo-topographically, forest park in Hanzhong not only possess similar precipitous view of Qinling, but also equally splendid scenery of Bashan; iv hydrologically, the landscape had a lasting appeal as that in south China to some extend; v the forest located in the best site of the same latitude; vi with the opening of Xihan expressway, access to Hanzhong was upgraded prominently, which made the park a garden of Xi'an and a resort for many citizens.
本文从森林公园及森林旅游的概念及相关理论入手,提出了汉中森林公园和森林旅游的发展优势,即:1、通过多年发展,森林旅游产品日益丰富,初具规模,现有国家级3家,省级3家;2、&旅游活市&被汉中市委、市政府确定为发展战略,在汉中经济社会中的重要地位进一步提升;3、从地貌景观上看兼具秦岭的险峻与巴山的锦绣;4、水文上看,颇具江南山水韵味;5、森林植被处于同纬度最好的地区;6、西汉高速公路开通,汉中交通能级大幅提升,成为西安后花园和区域性休闲旅游地,给森林旅游带来无限生机。
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In order to insure the teaching object completely bring to success, to insure the classroom teaching quality steadily improve, to promote the students body and mind healthy development and to obtain the best teaching effect. The teacher must innovate the traditional teaching design concepts and must put up system optimize design with the elements that impenetrate the teaching process, the structure of each element and the teaching tache with the guidance of modern teaching design theory.
为了确保课堂教学目标的全面完成,确保课堂教学质量的稳定提高,全面促进学生身心的健康发展,教师必须改革传统的教学设计观念,必须以现代教学设计理论为指导,对参与教学过程的要素,各个要素构成的结构和教学环节等进行系统优化设计,以期获得最佳的教学效果。
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Band differencing is feasible in water and irrigable field, but it couldnt monitor the changes of whole land use and its precision is the lowest. For the mufti-temporal composite method, it is difficult to choose the exact regions for change detection. Based on the previous accurate classification result, the post classification comparison method gets the best result compared with the other two methods, but also with the hand-on mistakes.
图像差值法对河流水面和水浇地的监测效果比较好,但对所有地类监测结果不令人满意,精度较低;多时相波段复合分类法中,变化土地类型训练区的确定较困难;分类后比较法是在前面土地信息准确提取的基础上进行的分析,精度较高,监测结果图也一目了然,是土地利用动态监测的一种有效方法,但它是在自动识别分类基础上进行的比较,传递了分类产生的误差。
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The Snow Queen, whose original Finnish name is Lumikuningatar, starts and ends with what's the best in this movie for children: the sight of Outi Vainionkulma as Greta, dancing and playing, together with the other protagonist of the story, Greta's dear friend Kaj.
雪女王,其最初的芬兰名字是lumikuningatar ,开始和结束的最佳时机在这部电影的孩子们:看到outi瓦伊尼翁库尔马为greta ,跳舞,玩,连同其他主角的故事, greta的亲爱的朋友kaj 。
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The decisive influencing factor of viscosity in carboxyl-methylation was cross-linking reaction. Carboxyl-methylation was the main influencing factor of solubility and swelling capacity in modification of high content amylose starch. The structure and gelatinization property of different amylose content were analyzed with an Olympus Vanox BHS-2 multi-function optic microscope, and the results were as follows. The structure of ordinary cornstarch was different from the high amylose; gelatinization temperature and pH value of starch were affected deeply by amylose content, but had little difference between the gelatinization of high content amylose starch contained 50% and 70% amylose; pH value had much more effect than temperature on the gelatinization of high content amylose cross-linked starch. Monochloroacetic acid consumption, alcohol concentration and pH value influenced the starch carboxyl-methylation. When alcohol concentration was 60%, pH value 10, monochloroacetic acid/starch mass ratio 55%, the carboxyl-methylation of high amylose cross-linked cornstarch had the best result. With the In-Vitro digestibility model and biodegradation experiment, the digestibility and biodegradability of high amylose cornstarch and its modified starch were detected.
采用Brabande粘度测定仪和Olympus Vanox BHS-2型多功能光学显微镜等分析手段对链淀粉含量50%和70%的高链玉米淀粉及其交联和交联羧甲基化淀粉的结构和性质进行了表征和分析,结果表明,普通玉米淀粉结构与含链淀粉50%和70%高链玉米淀粉结构不同;高链淀粉比普通淀粉难糊化,高链改性淀粉糊化受pH值影响较大,受温度影响较小;淀粉的冻融稳定性、透光率、溶解度、膨胀度和粘度受链淀粉的含量和改性的影响,但是,链淀粉含量超过50%时,则链淀粉含量对淀粉的膨胀度和溶解度影响不大;改性淀粉性质的影响因素中,影响粘度主要因素是交联反应,影响透明度、溶解度和膨胀度主要因素是羧甲基化改性;一氯乙酸用量、反应时乙醇浓度及碱性条件都会影响高链淀粉及其交联淀粉的羧甲基化改性效果,制备羧甲基化改性淀粉的最佳工艺是在pH值为10的60%的乙醇浓度介质中按一氯乙酸/淀粉质量比为55%进行取代反应。
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The discussions which the study investigated were chicken and pork meat processing for elders via different tender mode. In this study, we want to evaluate the nutritions of elders and focus on animal protein. The experiment was injected marination with CaCl2, NaHCO3 and enzyme on pork and chicken meat quality traits. Treatment on the meat was analyzed proximent quality and textural properties by response surface stepwise regression. The best tender method was discovered the elder's sensory evaluation of different tender mode and observed degradation of myoglobulin by muscle tissue slice and SDS-PAGE (10%). The function of sous-vide cooking collocated with tenderization that was evaluated by textural properties and sensory evaluation. It looks for discussion about meat processing for elders.
中文摘要本试验目的在利用市售禽畜肉为原料,针对高龄者之营养需求,分别使用氯化钙、碳酸氢钠与嫩化酵素等常见之嫩化方式对禽畜肉进行嫩化处理,搭配反应曲面法分析一般特性与物性测定,并进行高龄者品评测试以探讨不同嫩化方式之口感影响以求得不同禽畜肉之最佳嫩化处理,并以肌纤维组织切片与电泳分析观察肌肉蛋白质之分解现象,最后利用真空调理法搭配嫩化处理并分析物性测定与品评测试,评估真空调理法增进嫩化之效果,探讨禽畜肉开发为适合高龄者之加工产物模式。
- 推荐网络例句
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Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.
在对危险的南部地区访问时,他斥责什叶派民兵领导人对中央集权的挑衅行为。
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In fact,I've got him on the satellite mobile right now.
实际上 我们已接通卫星可视电话了
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The enrich the peopling of Deng Xiaoping of century great person thought, it is the main component in system of theory of Deng Xiaoping economy, it is a when our country economy builds basic task important facet.
世纪伟人邓小平的富民思想,是邓小平经济理论体系中的重要组成部分,是我国经济建设根本任务的一个重要方面。