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This invention pertains to compounds of Formula I, their N-oxides and suitable salts wherein A is O or S; G is a 5- or 6-membered heteroaromatic ring or a 5- or 6-membered nonaromatic heterocyclic ring optionally including one or two ring members selected from the group consisting of C, SO or S2, each ring optionally substituted with from one to four R; each J is independently a phenyl ring, a 5- or 6-membered heteroaromatic ring or an aromatic 8-, 9- or 10-membered fused carbobicyclic or heterobicyclic ring system, wherein each ring or ring system is optionally substituted with from one to four R; and R, R, R, R and n are as defined in the disclosure.

本发明涉及式I的化合物、其N-氧化物和适当盐，其中A是O或S；G是任选地包含一个或两个独立选自C、SO或S 2 的环成员的5-或6-员杂芳环或5-或6-员非芳族杂环，各环任选地被1-4个R 2 取代；各J独立地是苯环，5-或6-员杂芳环或芳族8-，9-或10-员稠合的碳二环或杂二环系，其中各环或环系任选地被1-4个R 3 取代；R 1 ，R 2 ，R 3 ，R 4 和n如说明书中定义。

The invention is characterized in that phthalide of general formula, wherein n and X have the meaning cited in the description, is reacted with nitrogen heterocycles of general formula: H-Z, wherein Z has the meaning cited in the description, or with nitrogen heterocycle metal salts of general formula in the presence of an aprotic polar diluent and optionally in the presence of a basic auxiliary reaction agent.

本发明涉及制备通式的2－杂环基甲基苯甲酸衍生物的新的方法，其中n、X和Z具有说明书中给出的意义，该方法提供高收率和高纯度，其特征是，通式的2－苯并呋喃酮，其中n和x具有说明书中给出的含义，与通式的氮杂环：H－Z，其中Z具有说明书中给出的意义，或与通式的氮杂环的金属盐在质子惰性极性稀释剂中并任选在碱性反应助剂存在下反应。

The method adopts the following steps: after mixed, phosphorus source, silicon source, aluminum source, an organic template agent, water and a precursor of the SAPO molecular sieve are hydrothermally crystallized for at least 0.1 hour at the temperature ranging from 110 to 260 DEG C to obtain the SAPO molecular sieve; wherein, the preparation method for the precursor of the SAPO molecular sieve has the following steps:, the molar ratio is 0.03 to 0.6 R:(Si0.01 to 0.98: Al 0.01 to 0.6: P0.01 to 0.6): 2 to 500 H2O; wherein, R stands for mixture solution of raw materials which is blended by the phosphorus source, the silicon source, the aluminum source, the an organic template agent and water of the template agent;, the mixture solution of raw materials prepared in step reacts at the temperature which is at least 50 DEG C lower than the crystallization temperature for at least 0.1 hour.

本发明通过采用包括以下步骤：将磷源、硅源、铝源、有机模板剂、水和SAPO分子筛前驱体混合后在110～260℃的温度下水热晶化至少0.1小时获得SAPO分子筛；其中SAPO分子筛的前驱体的制备包括以下步骤：将摩尔配比为0.03～0.6R∶(Si0.01～0.98∶Al0.01～0.6∶P0.01～0.6)∶2～500H 2 O，式中R代表模板剂的磷源、硅源、铝源、有机模板剂和水混合成原料混合液；将步骤制备的原料混合液在低于晶化温度至少50℃的温度下反应至少0.1小时的技术方案较好地解决了该问题，可应用于含氧化合物制烯烃催化剂的制备过程。

The preferred organometallic compounds of the present invention are of the formula (R1)m M(PR23)x, where M is a metal selected from the group consisting of manganese, technetium, rhenium, iron, cobalt, nickel, ruthenium, rhodium, palladium, osmium iridium and platinum wherein m is 0, 1, 2, 3 or 4; x is 2, 3, 4 or 5 and m+x are 2, 3, 4, 5, 6, 7 or 8, m and x selected according to each metals appropriate valence; each R1 is independently selected from the group consisting of hydrogen, deuterium, N2, H2, D2 and a variety of substituted alkyl groups; each R2 is independently selected from the group consisting of lower alkyl, aryl, arylalkyl, and alkyl-Z, aryl-Z and arylalkyl-Z where Z is selected from the group consisting of oxy, silyl, siloxy, oxysilyl, siloxy, oxysiloxy, silyalkyl, oxysilylalkyl, siloxyalkyl, oxysiloxyalkyl, silylalkoxy, silylalkoxy, siloxyalkoxy and oxysiloxyalkoxy; and wherein when M is cobalt and one group R1 is selected to be N2, then m is 2 and the second group R1 is hydrogen or deuterium.

有机化合物的首选本发明的配方是米(R1代)米×(pr23)、那里是一米的金属挑选出来，第一组由锰、锝、铼、铁、钴、镍、钌、铑、钯、锇、铱铂其中M是0、1、2、3或4； X是2，3， 4或5米×+有2，3，4，5，6，7或8 米和X挑选合适的价按每个金属； R1的是每一组由独立选自氢、氘、氮、氢气、 D2和各种烷基取代群体； R2中的每个组由独立选自烷基低、芳、芳基烷基、烷基的Z、芳基、芳基烷基的Z-那里的ZZ是选自组风、含硅、氧、oxysilyl、硅、oxysiloxy，silyalkyl， oxysilylalkyl，siloxyalkyl，oxysiloxyalkyl，silylalkoxy，silylalkoxy，siloxyalkoxy和oxysiloxyalkoxy；其中，M是当钴一派R1的选择是氮气、然后是2米，第二组R1的氘是氢或者。

The method is based on a variable structure to control the SVC, wherein, the variable structure control method comprises two aspects of the unbalanced load equalization compensation and the parameter control of a PI controller, wherein, the unbalanced load equalization compensation adopts the SVC compensation susceptance computational method which is based on the synchronous rotation reference coordinate transformation of a virtual symmetrical three-phase system; meanwhile, in the stabilization control of the system voltage, the ant colony algorithm optimization method is adopted to real time adjust and to optimize the parameter kp and ki of the PI controller.

本发明公开了一种静止无功补偿器的不平衡补偿和蚁群优化方法，基于变结构对静止无功补偿器SVC进行控制，其中变结构控制方法包括不平衡负荷平衡化补偿和PI控制器的参数控制两个方面，其中不平衡负荷平衡化补偿采用基于虚拟对称三相系统的同步旋转参考坐标变换的SVC补偿电纳计算方法；同时在系统电压稳定控制时，采用蚁群算法优化方法，对PI控制器的参数kp、ki进行实时调整、寻优。

The present invention relates to a halogen-free, multilayered, uniaxially oriented heat shrink film comprising a core layer comprising a blend of polyolefins; a first skin layer on the upper surface of the core layer, and a second skin layer on the lower surface of the core layer, wherein the first and second skin layers independently comprise a polyolefin blend and wherein the shrinkage of the film is at least about 40% in the machine direction at 270 DEG F.

本发明涉及一种不含卤素、多层、单轴取向的热收缩薄膜，包含含聚烯烃共混物的芯层；在芯层上表面上的第一皮层，和在芯层下表面上的第二皮层，其中，第一和第二皮层独立地包含聚烯烃共混物，并且其中，在270°F，在纵向薄膜的收缩率至少约为40％。

The experimental result showed that 1086 and 848 proteins were identified by MALDI-TOF-TOF and ESI-Q-TOF respectively, wherein 633 proteins were homolog; 38 and 33 proteins were found to be differentially expressed by more than 0.5 fold by MALDI-TOF-TOF and ESI-Q-TOF respectively, wherein 3 proteins were the same proteins.

结果表明，用MALDI-TOF-TOF和ESI-Q-TOF方法分别鉴定出1086种和848种蛋白质，其中相同的蛋白质为633种；MALDI-TOF-TOF和ESI-Q-TOF方法分别找到38种和33种表达差异在0.5倍以上的蛋白质，其中3种为相同的蛋白质。

The process of the invention mainly comprises disintegrating substrate material of waste printing wiring board into particle material whose particle size is 0.5-3.5 micron, the mixing with double bond reactant, adding with phenyl ethene, conducting reaction under gamma ray irradiation condition, modifying substrate material particles, then commixing material which is treated with acrylonitrile-butadiene-styrene, wherein the adding quantity of substrate material particle is 35%-35%, conducting extrusion pelleting for commixing material on a plastic extruder, wherein extruding temperature is 200-250 DEG C, and finally obtaining plasticity plastic particles with excellent property.

本发明方法主要是：先将废旧印刷线路板基板材料粉碎成为粒径为0.5～3.5微米的颗粒料，然后与具有双键的反应物混合，再加入苯乙烯，并在γ射线的辐照条件下进行反应，将基板材料颗粒进行改性处理。

--- Method and apparatus for abstracting water from air wherein in a first phase of a recurring cycle a stream of cool, moist air from the atmosphere first cools a first heat storage condenser (1) and then humidifies a hygroscopic medium (14); in a second phase a stream of warm air additionally heated by solar radiation expels moisture from the hygroscopic medium and carries the moisture into said first heat storage condenser (1) where it condenses, releasing condensation heat, and drains away; in a third phase another stream of cool, moist air from the atmosphere first cools a second heat storage condenser (2) and then rehumidifies the hygroscopic medium, and in a fourth phase another stream of warm air heated by solar energy again expels the moisture from the hygroscopic medium and carries the moisture to said second heat storage condenser where it condenses and drains away, and wherein the warm air streams of the second and fourth phases, are preheated using the heat of condensation picked up by the said second heat storage condenser (2) in the fourth phase and the heat of condensation picked up by said first heat storage condenser (1) in the second phase, respectively, before being additionally heated by solar radiation and being used to expel moisture from the hygroscopic medium.

摘要---方法和仪器取水，从空气，其中在第一阶段的周期性循环流冷静，潮湿空气从大气中的第一冷却的第一个蓄热冷凝器（ 1 ），然后humidifies一吸湿中等（ 14 ）；在第二阶段流的暖空气此外，激烈的太阳辐射驱逐水分从吸湿中等，并进行水分成表示，第一蓄热冷凝器（ 1 ）凡它凝结，释放出凝结换热，及雨水渠的距离；在第三阶段另一流的冷静，潮湿空气从大气中冷却，第一第二蓄热冷凝器（ 2 ），然后rehumidifies该吸湿中等，而在第四个阶段的另一流的暖空气加热太阳能再次驱逐水分从中期和吸湿性带有水分说，第二蓄热冷凝器而凝结及排水渠远离，和其中的暖空气流，第二和第四阶段，预热用热凝结回升，由说，第二蓄热冷凝器（ 2 ）在第四个阶段和热凝结回升，由说，第一蓄热冷凝器（ 1 ）在第二个阶段，分别之前，此外激烈的太阳辐射和被用来驱逐水分从吸湿中等。

Further, the prior coating methods for shielding electromagnetic wave of electronic equipments include three kinds of methods including 1 a vacuum metalizing wherein the metal is vaporized and deposited on the material surface under vacuum; 2 a conductive paint spray wherein the solution containing

此外，先前的对电子设备进行电磁波屏蔽的涂层方法有三种方法，包括1）真空金属镀层，这里，金属在真空下被蒸发并沉积在材料表面；2）导电涂料喷溅，这里，含金属粉末的溶液被喷雾到材料表面；3）化学镀，这里，待涂覆的

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。