查询词典 water of crystallization

The experimental results showed that the raw materials can be totally conversed when reacted for 45 min;and the average size of prepared barium carbonate was 1 μm.It also discovered that crystal water was not feasible for accelerating the reaction speed and increasing the degree of crystallization.

试验结果表明：反应45 min原料即可完全转化，制备的碳酸钡颗粒平均尺寸约1 μm，并且发现利用结晶水加快反应速度、提高产物结晶程度是不可行的。

Furthermore, the form of hot water of rich silicon shows formation of the micro crystallization quartzite by the carbonate rocks.

地形地貌、地质环境和矿石结构等条件是影响微结晶石英岩风化形成粉石英矿的主要因素。

In the preparation method, zirconium is mixed with benzenephosphonic acid according to the molar ratio of 1:2 to 1:4, and Alpha-zirconium phenyl phosphonate is produced by centrifugal washing after one to five days of crystallization under the temperature of 50 DEG C to 100 DEG C; deionized water is added in order to prepare Alpha-zirconium serosity, the solid content of which is 4 percent to 8 percent; the Alpha-zirconium serosity is granulated and dried by a rotary spray dryer, the feeding speed of the Alpha-zirconium serosity imported into an atomizer is controlled between 20ml/min and 80ml/min, and the temperature of a hot air inlet is controlled between 120 DEG C and 200 DEG C.

本发明涉及一种大比孔容微球α-苯膦酸锆及其制备方法，其颗粒尺寸为10～100μm，比孔容为0.908cc/g，比表面积为125.8m 2 /g；其制备方法是将锆和苯膦酸以摩尔比1∶2～1∶4混合，在50～100℃温度条件下晶化1～5天，离心洗涤得到α-苯膦酸锆；加入去离子水配制α-苯膦酸锆浆液，其固含量为4-8％；将α-苯膦酸锆浆液用旋转式喷雾干燥器进行造粒、干燥，控制α-苯膦酸锆浆液输入雾化器的进料速度为20～80ml/min，控制热风进风口温度为120～200℃；该方法具有操作简单、合成条件温和，对环境污染小等特点，该材料应用于催化、催化剂载体、吸附、离子交换等方面。

Significant processing steps can include: a phase changes involving either the desired molecule or the solvent, inert carrier or vehicle, e.g., dissolution, crystallization, evaporation, sublimation, distillation or absorption; b a phase separation such as filtration or centrifugation; c any chemical change involving the desired molecule, e.g., removal or addition of water of hydration, acetylization, formation of the salt; d an adjustment of the solution containing the molecule such as adjustment of pH or pO2; e a precision measurement of contained or added BPC components, in-process solutions, recycled materials is performed, i.e., weighing, volumetric measuring, optical rotation, spectrophotometric determinations, etc.; and f changes occur in surface area, particle size, or lot uniformity, e.g., milling, agglomeration, blending.

意义较大的步骤可能会包括：a相变化，包括指定分子或溶剂，惰性载体或溶媒，如溶出作用，结晶，蒸发，升华，蒸馏或吸附；b相分离，如过滤或离心；c涉及指定分子的任一化学变化，如结晶水的除去或添加，乙酰化作用，成盐；d包含分子的溶解的调节，如调节pH或pO2；e 含有或添加原料药组分，过程内溶液，回收物料的精密测量，如，称重，体积测量，旋光度，分光光度测定，等和f 表面，粒度，或批一致性的变化，如磨碎，凝块，混合。

In order to overcome the fault of 5'-GMPNa2 product quality, such as amorphic state, lower purity and inconstant water content, a systematical study on the crystallization process of 5'-GMPNa2 had been presented in this thesis. A new crystallization process has been developed, with which the high quality crystals of 5'-GMPNa2 can be obtained.

针对目前国内生产5'-鸟苷酸二钠基本为无定形体，且产品纯度低、水含量不稳定等问题，本文对5'-鸟苷酸二钠的结晶过程进行了系统的研究，提出了新型精制结晶工艺，解决了制备高质量的I型5'-鸟苷酸二钠晶体的问题。

The crystallization behavior is affected by the concentration and cooling rate simultaneously when the solution is cooled.The freezable water of ...

降温过程中的结晶热可用来确定溶液降温后的冻结水含量以及最大冻结浓缩溶液中的水分含量。

Finally,the crystallization metastable zone of cefazolin sodium pentahydrate in water and the mixture of water and 2propanol at different temperatures was determined by the laser method.Valuable thermodynamics data for the industrial manufacture of cefazolin sodium pentahydrate were obtained.KEY WORDS Cefazolin sodium pentahydrate;Crystallization;Thermodynamics;Metastable zone

本文测定了5~35℃范围内头孢唑林钠在不同配比的水乙醇、水丙酮、水异丙醇混合溶剂中的溶解度数据，采用热分析仪测定了头孢唑林钠的差热分析数据，推导了头孢唑林钠溶解度模型，为头孢唑林钠的结晶分离提供了热力学数据。

The method adopts the following steps: after mixed, phosphorus source, silicon source, aluminum source, an organic template agent, water and a precursor of the SAPO molecular sieve are hydrothermally crystallized for at least 0.1 hour at the temperature ranging from 110 to 260 DEG C to obtain the SAPO molecular sieve; wherein, the preparation method for the precursor of the SAPO molecular sieve has the following steps:, the molar ratio is 0.03 to 0.6 R:(Si0.01 to 0.98: Al 0.01 to 0.6: P0.01 to 0.6): 2 to 500 H2O; wherein, R stands for mixture solution of raw materials which is blended by the phosphorus source, the silicon source, the aluminum source, the an organic template agent and water of the template agent;, the mixture solution of raw materials prepared in step reacts at the temperature which is at least 50 DEG C lower than the crystallization temperature for at least 0.1 hour.

本发明通过采用包括以下步骤：将磷源、硅源、铝源、有机模板剂、水和SAPO分子筛前驱体混合后在110～260℃的温度下水热晶化至少0.1小时获得SAPO分子筛；其中SAPO分子筛的前驱体的制备包括以下步骤：将摩尔配比为0.03～0.6R∶(Si0.01～0.98∶Al0.01～0.6∶P0.01～0.6)∶2～500H 2 O，式中R代表模板剂的磷源、硅源、铝源、有机模板剂和水混合成原料混合液；将步骤制备的原料混合液在低于晶化温度至少50℃的温度下反应至少0.1小时的技术方案较好地解决了该问题，可应用于含氧化合物制烯烃催化剂的制备过程。

Organic solvent repetition crystallization method showed that 60% ethanol was the suitable solvent system. After 5 times repetition crystallization, the purity of product can be up to 98%, and the crystal state was yellow club-shaped, length of which is above 3mm. The productivity of this method is 30.01±1.26%, which is 2 times high than water repetition crystal method. So this method has good exploitation foreground.

有机溶剂重结晶法，选择60%浓度乙醇为适合的二氢杨梅素结晶体系，经过5 次重结晶后，产品的纯度可达98%，晶体为黄色、棒状，长度可达3mm，结晶产率为30.01±1.26%，较水重结晶法高2 倍左右。

I also have synthesized nanocrystallinecobalt phosphides via metathesis reaction at 180℃. Different routes have been appliedto prepare nanocrystalline Ni〓P. The influences of the crystallization water of metalchloride were also discussed.A series sulfides of VIII metals have been fabricated.

1采用溶剂热技术通过置换反应在300-350℃合成了20nm的CrN纳米晶，与传统固相制备法相比，大大降低了反应和结晶温度；在180℃合成了磷化钴纳米粉，XRD显示两相共存(C0〓P、CoP)，TEM中也证实两种形貌的存在；该技术成功的解决了前驱物易水解的问题。

But we don't care about Battlegrounds.

但我们并不在乎沙场中的显露。

Ah! don't mention it, the butcher's shop is a horror.

啊！不用提了。提到肉，真是糟透了。