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Methods The pesticides were extracted with acetone and dichloromethane, warmed with water at 40℃,and circumrotated and evaporated until it was nearly dry, then it was purified by Envi Carb column and Sep Pak NH2 column. Afterwards, gas chromatography mass spectrometry and selected ion monitoring were used to determine 42 pesticide residues, such as organo-phosphorus, pyrethroid, organochlorine, carbamate and weedicide.

该法采用丙酮、二氯甲烷提取，40℃水浴旋转蒸发近干，以Envi-Carb柱和Sep-Pak-NH2柱净化，以气相色谱－质谱选择离子监测方式分析检测有机磷、有机氯、拟除虫菊酯、氨基甲酸酯和除草剂等42种农药残留。

To exploit highly bioactive natural antifungal medicaments from starfish, water-soluble starfish glycosides from Asterias rollestoni were isolated and purified by macroporous resin column and silica gel column chromatography, and their antifungal bioactivities were also examined.

为了分离纯化出具有强抗真菌活性的水溶性海星皂苷，以罗氏海盘车腕为实验材料，利用水抽提方法获得水溶性海星皂苷粗品，依次利用大孔树脂和硅胶柱层析对水溶性海星皂苷进行了纯化，并对其抗真菌活性进行了测定。

A determination method of ursolic acid in Callicarpa macrophylla Vahl leaves by reversed- phase high performance liquid chromtograph was established. The chromatographic column (Symmetry Shield RP18), methanol-water mobile phase(88:12, V/V) with 1.0 ml/min flow rate, the detection wavelength (210nm) and the column temperature (25℃) were adopted.

建立反相高效液相色谱测定其含量的方法，色谱柱为Symmetry Shield RP18柱，流动相为甲醇-水（体积比88∶12），流速1.0 ml/min，检测波长210 nm，柱温25℃。

A determination method of ursolic acid in Callicarpa macrophylla Vahl leaves by reversed- phase high performance liquid chromtograph was established. The chromatographic column (Symmetry Shield RP18), methanol-water mobile phase(88:12, V/V) with 1.0 ml/min flow rate, the detection wavelength (210nm) and the column temperature (25℃) were adopted.

建立反相高效液相色谱测定其含量的方法，色谱柱 Symmetry Shield RP18柱，流动相为甲醇-水（体积比88∶12），流速1.0 ml/min，检测波长210 nm，柱温25℃。

MethodsSeparation was performed on an Agilent ZORBAX SBC18 (4.6 mm×250 mm, 5 μm) analytical column with mobile phase consisting of acetonitrile and water with gradient elute at the flow rate of 1.0 ml/min and the column temperature 40℃.

色谱柱： Zorbax SBC18柱（250 mm×4.6 mm，5 μm），流动相∶乙腈水，检测波长：203 nm，柱温：40℃，流速：1.0 ml/min，分析时间：90 min。

Different chromatographic parameters including elution profiles, column temperature were investigated in order to optimize separation conditions of different fatty acid phenacyl ester derivatives. A gradient elution using methanol/acetonitrile (90:10, V/V)-water as mobile phase at 0.35 mL/min, detection wavelength at 246 nm, and column temperature of 35℃ were chosen.

经优化确定以(90：10)-水为流动相梯度洗脱，在检测波长246 nm，柱温35℃，流速0.35 mL/min的色谱条件下，18 min内能完成对13种脂肪酸衍生物的分离检测。

Methods: The pesticides were extracted with acetone and dichloromethane. The extract was warmed with water at 80℃, circumrotated and evaporated until it was nearly dry. Then it was cleaned-up by Envi-Carb column and Sep-Pak-NH2 column.

本法采用丙酮、二氯甲烷提取，40℃水浴旋转蒸发近干，以Envi-Carb柱和Sep-Pak-NH2柱净化，以气相色谱－质谱选择离子监测方式分析检测有机磷、有机氯、氨基甲酸酯和除草剂等32种农药残留。

The sample was redissolved in the acetonitrilved in the acetonitrile-water (3:2, v/v), then analyzed using LC-MS/MS in multiple reaction monitoring mode via positive electrospray ionization with an Agilent ZORBAX SB-C18 column as the analytical column.

样品用1%醋酸乙腈溶液萃取，经Waters Sep-Pak Vac固相萃取柱净化，乙腈－甲苯（体积比为3：1）洗脱，旋转蒸发浓缩，用乙腈－水（体积比为3：2）溶解，以Agilent ZORBAX SB-C18色谱柱分离，以电喷雾电离串联质谱在正离子多反应监测模式下进行测定。

The optimum condition for separating and purifying SAM was using the solution at pH of 5.0 containing 3.0 g SAM per liter at the flow velocity of 6 L/h through the ion-exchange column (φ50 mm×1500 mm)filled with D152 resin. Impurities were removed first by eluting the column with double-distilled water and acetic acid, and then with 9 L to 15 L of sulfuric acid of 50 mmol/L concentration at the flow velocity of 6 L/h.

论文对SAM的性质、药理作用以及当前国际上关于SAM的研究进展进行了较为详尽的综述，并在此基础上确立了研究内容，取得了如下成果： 1利用本实验室构建的基因工程菌JM71发酵生产S-腺苷-L-蛋氨酸，在50 L发酵罐中发酵6天后，SAM终产量达到6 g/L发酵液。

Methods The amino acids in the injections were pretreated with 6-aminoquinolyl-N-hydroxysuccinimdyl separately and their derivatives were analyzed on Waters 2695 HPLC using AccQ-Tag column. Gradient eluents consisted of sodium acetate solution (pH 4.95), acetonitrile and water. The Detection wavelength was 248 nm and column temperature 37℃.

采用AccQ-Tag法，以6-氨基喹啉－N-羟基琥珀酰亚胺基甲酸酯为衍生试剂，与复方氨基酸注射液(18AA-V)中17种氨基酸柱前衍生，用Waters 2695 HPLC仪器，AccQ-Tag柱，以醋酸钠(pH 4.95)缓冲液为流动相A，乙腈为流动相B，水为流动相C进行梯度洗脱，检测波长为248 nm，柱温为37℃，进样量为5μL。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。