查询词典 water column

Samples were saponified with 20 g/L sodium hydroxide. The sexual hormones were then extracted with dichloromethane-acetic acetate (40∶1, v/v) under acidic conditions (pH 3, adjusted with 1 mol/L HCl ). An XTerraTMRP18 column was employed and a mixture of water-methanol-acetonitrile (50∶32∶18, v/v) was used as mobile phase. The seven sexual hormones were detected at 230 nm. The average spiked recoveries for the seven sexual hormones ranged from 75.6% to 97.8% with relative standard deviations of 1.9% to 7.2%. The linear ranges of determination were from 5 to 50 mg/L with correlation coefficients of 0.9999, and the limits of detection were from 3.7 to 12 ng.

先在试样中加入20 g/L氢氧化钠溶液与油脂进行皂化反应，然后用二氯甲烷-乙酸乙酯(体积比为40∶1)混合液在酸性条件下(pH 3)萃取，选择XTerraTMRP18色谱柱，以水-甲醇-乙腈(体积比为50∶32∶18)混合液为流动相，在波长230 nm处检测。7种性激素分离良好并排除了样品中杂质峰的干扰，低、高浓度平均回收率范围为75.6%~97.8%；相对标准偏差为1.9%~7.2%；检出限为3.7~12 ng。

Safety Facilities: traffic lights, traffic signs, solar sign series, roadblocks lights, electronic warning light, road crossings deceleration zone, Wheel Locator, safety alerts cone, electronic flash road cone, crossing pillars, isolation column, Traffic precursor, reflector retaining angle, wide angle lenses, water horse, holding the command, boldface warning, railroad crossing shockproof pad, rail pads, rubber bridge stretching devices, rubber, such as reflective vests.

交通安全设施：交通信号灯、交通标志、太阳能标志系列、路障灯、电子警示灯、公路道口减速带、车轮定位器、交通安全警示锥、电子闪光路锥、道口立柱、隔离柱、分道体、反光护角、广角镜、水马、指挥捧、警示横杠、铁路道口防震垫、钢轨垫片、橡胶桥梁伸缩装置、橡胶止水带、反光背心等。

The determination of amino acids in blood clam antianaemia oral liquid using HPLC-AccQ-Tag method is reported. The oral liquid reacted with 6-aminoquinolyl-N-hydroxysuccini-mdyl carbamate. Then, the corresponding derivatives were analyzed with an HPLC. The chromatographic conditions were AccQ-TagTM C18 column for amino acids analysis (3.9mm×15cm); mobile phase of program elution sodium acetate solution(pH5.02), acetonitrile, Milli-Q water. The amino acids'AQC deriatives were detected at 248nm with a UV-detector. Eighteen kinds of amino acids were completely determined in 35 minutes.

以6-氨基喹啉-N-羟基琥珀酰亚胺基氨基甲酸酯为衍生剂，与毛蚶抗贫血口服液中的氨基酸柱前定量衍生，用WatersHPLC仪，AccQ-TagTM专用C18柱(3.9mm×15cm)，以140mmol·L-1的醋酸钠溶液(pH5.02)为溶剂A，乙腈为溶剂B，超纯水为溶剂C，进行梯度洗脱，检测波长为248nm，35min测试完毕。

The affecting factors of removal of arsenate As(Ⅴ by bone char were studied in batch and column experiments. The results show that the performance of bone char adsorbing As from drinking water is stable after adsorption—desorption—regeneration—re-adsorption cycles.

摘 要：采用骨炭作吸附剂，通过静态和动态吸附试验，研究饮用水中砷去除的效果及其影响因素，以及骨炭反复吸附—解吸—再生—再吸附后骨炭性能的稳定性。

In the commonly used positive cycle of drilling, the mud pump is to rinse the surface with water medium ─﹑ mud or polymer washing fluid at a certain pressure, through the high-pressure hose taps and drill column ﹑ center hole in the bottom of the direct-drill in order to achieve Cooling ﹑ be cutting down the drill cuttings removal and transport to the surface purpose.

在常用的正循环钻探中﹐泥浆泵是将地表冲洗介质─清水﹑泥浆或聚合物冲洗液在一定的压力下﹐经过高压软管﹑水龙头及钻杆柱中心孔直送钻头的底端﹐以达到冷却钻头﹑将切削下来的岩屑清除并输送到地表的目的。

METHODS: 5 g CPC was dissolved in 2 mL water, and then 0.1 g Doxorubicin microspheres was incorporated into the powder-phase CPC. The column microsphere bone cement was prepared at a diameter of 0.18 cm and a height of 1.12 cm. While untreated CPC was taken as blank control and Doxorubicin control was also prepared.

将2 mL水加入5 g骨水泥粉中，然后迅速将干燥的0.1 g多柔比星微球加入其中，搅拌均匀成糊状后推入预制磨具中制备成直径0.18 cm，高1.12 cm的柱状载微球骨水泥，两断端平行，打磨光滑平整，同时制备不载多柔比星的空白对照组、多柔比星原药对照组。

Ethyl cellulose membrane material has produced in physical modification method. The fundamental characteristics of reverse osmosis on EC membrane can be correlated with HPLC experimental conditions. By using EC membrane material as column packing, double-distilled water as mobile phase, the retention times are measured with suitable inorganic and organic compound as solutes.3. Complying with the retention times, the partition coefficient of the solute and the ratio of the surface excess concentration of solutewith the concentration of the parent fraction are calculated .

利用物理改性的方法研制了乙基纤维素(Ethyl Cellulose，简称EC)膜材料，并将其作为高效液相色谱柱的固体填料，以高效液相色谱模拟反渗透实验平衡条件，以水为流动相，选择合适的无机物和有机物作为溶质，测定乙基纤维素对它们的相对保留时间及平衡分配常数K_A′。3。

Enhanced heat transfer ; pressure loss ; water drop-shaped column ; numerical calculation

强化传热；压力损失；水滴形扰流柱；数值计算

Methods The sample was separated with a C18 column (150mm×4.6mm, 5μm) at 30℃ with the mobile phase of methanol and water (74:26); A fluorescence detector was used (λex=230nm λem=460nm); The floss rate was 1mlmin^(-1) Results The retention time of aesculin was(3.620±0.05)min; A good linear relationship of aesculin in the plasma samples at the concentration between 0.1mgL^(-1) and 100mgL^(-1) was observed (r=0.997); The mean absolute recovery was 74.0%~82.6% and the lowest detective limit was 0.05ng; Both the intra-day and inter-day precisions were less than 9.0%.

以C18柱(150mm×4.6mm，5μm)分离；流动相为甲醇－水(76：24)；流速：1mlmin^(-1)；柱温：30℃；荧光检测器，激发波长230nm，发射波长460nm：结果秦皮甲素的保留时间为(3.620±0.05)min；血药浓度在0.1~100mgL^(-1)范围内线关系良好(r=0.997)；绝对回收率为74.0%-82.6%，日内、日间精密度均＜9.0%，最低检测限为0.05ng。

OBJECTIVE:To establish the RP-HPLC method for determination of methyl hydroxybenzoate and ethyl hydroxybenzoate in oral liquid preparations METHODS:The Nova-Park C18 column(3 9mm×150mm,5μm)was used The mobile phase consisted of acetonitrile-water(25∶75)at a flow rate of 1ml/min,the detection wavelength was set at 254nm and the sensitivity was set at 0 01 AUFS RESULTS:The linear ranges of methyl hydroxybenzoate and ethyl hydroxybenzoate were 0 4 412～13 2 360μg/ml(r=0 9 999) and 0 6 672～20 0 160μg/m...

目的 ：建立内服液体制剂中羟苯甲酯和羟苯乙酯的反相高效液相色谱测定方法。方法：色谱柱：Nova -ParkC18 柱(3 9mm×150mm ，5μm)；流动相：乙腈-水(25∶75)；流速：1ml/min ；检测波长：254nm ；灵敏度：0 01AUFS。结果：羟苯甲酯浓度在0 4412～13 2360μg/ml范围内线性关系良好(r=0 9999)；羟苯乙酯浓度在0 6672～20 0160μg/ml范围内线性关系良好(r=0 9998)。结论：该方法简便、快速、准确，可用于医院制剂中防腐剂的检测。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。