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Silicon phthalocyanine dihydroxide was prepared from silicon phthalocyanine dichloride through two methods. The first was alkali treating that meaned silicon phthalocyanine dihydroxide was treated in the ethanol solution containing sodium methylate .The second was acid treating meaned precipitating its solution in concentrated sulfuric acid into ice water. The product yield of the second method was 77.0％, which was higher than the method of alkali treating.

此外将合成的二氯酞菁硅采用两种方法转化为二羟基酞菁硅，第一种方法是碱处理法即将二氯酞菁硅在甲醇钠的乙醇溶液中回流得到，最高收率为53％第二种方法是酸处理法即采用二氯酞菁硅的硫酸溶液在冰水析出的方法转化为二羟基酞菁硅，其中酸溶析出法收率为77.0％。

RESULTS: The average dose of venlafaxine was (196±s 48) mgd^(-1), the average effective time was (8±3) d, and the effective rate was 68%. The average dose of mirtazapine was (32±11) mgd^(-1), the average effective time was (12±6) d, and the effective rate was 65%. The scores after treatment were significantly decreased in both groups. The scores of HAMA were (33±3)%(wk 1) and (50±3)%(wk 4) in venlafaxine group,(14±3)% and (31.0±2.3)% in mirtazapine group.

结果：文拉法辛组治疗剂量为(196±s 48) mgd^(-1)，显效时间(8±3) d，有效率68%，米氮平组分别为(32±11) mgd^(-1)、(12±6) d、65%。2组疗效量表评定结果均较治疗前有显著下降，特别是文拉法辛组wk 1和wk 4的HAMA减分率为(33±3)%和(50±3)%，米氮平组为(14±3)%和(31.0±2.3)%，前者下降更为明显。

The relationship between the ratio of Ca to Si with shrinkage value was needed to be studied further.The strength of M-AAS was comparatively high, but the flexural strength was regressed in the long term. The compressive and flexural strengthes of 3 days were able to surpass 8MPa and 78MPa, respectively, and compressive strength of 90 days were all around 100MPa, but compared to flexural strength of 28 days, the flexural strength of 90 days was regressed by 19.0%. The high strength property of M-AAS associated with its hydration products and Interfacial Transition Zoo. The main hydration products of M-AAS were microcline and CSH, no calcium hydroxide was found. The coexistence of microcline and CSH worked as micro-aggregate by each other, and no weak ITZ, both resulted in its high strength. The regression of its strength was related to its high shrinkage property, because the crazing caused by shrinkage would decrease the strength, especially the flexural strength.

M-AAS强度较高，但长期抗折强度倒缩。3天抗折和抗压强度分别可超过8MPa和78MPa，90天抗压强度在100MPa左右，但90天抗折强度比28天抗折强度相比低19.0％。M-AAS的高强特性与其水化产物和界面过渡区有关，M-AAS的水化产物主要为微斜长石和CSH凝胶，没有氢氧化钙，微斜长石与CSH凝胶相互填充和配合共同起到强度的作用，M-AAS砂浆中几乎没有发现界面过渡薄弱区。M-AAS的强度倒缩现象与其收缩值较大有关，收缩会引起M-AAS硬化体内部出现微裂缝，使强度下降。

It was found that the samples PVP-PdCl2-CdCl2 and PVP-PdCl2-HgCl2, compared with PVP-PdCl2, exhibited much higher catalytic activity and dechlorination selectivity, and the yields of the coupling by-products were obviously decreased. For example, when p-chloroaniline was used as substrate, the reaction time was shortened to 1/8, and the yield of dechlorination product was about 25 times as much as the original one, and when p-chlorotoluene was used as substrate, the yield of coupling by-product catalyzed by bimetallic catalyst was 1/390 of that catalyzed by monometallic catalyst.

与负载型单金属催化剂PVP-PdCl2相比， PVP-PdCl2-CdCl2和PVP-PdCl2-HgCl2对氯代芳烃脱氯有高得多的催化活性和脱氯选择性，且偶联副产物显著减少；以对氯苯胺为底物时，双金属催化下的反应时间缩短为单金属催化下的1/8，而脱氯产物收率提高25倍；底物为对氯甲苯时，双金属催化下的偶联副产物仅为单金属催化下的1/390。

The results showed that,the sound pressure level increased significantly when narrow transverse groove was used;the effect of speed on the sound pressure level was greater than loading;the noise of S-shaped straight groove was lower,and the difference of sound pressure level between positive and negative rotation was small;the sound pressure level of 15° oblique groove was higher than 0° and 15° alternate groove,but the difference of sound pressure level between positive and negative rotation of 0° and 15° alternate groove was bigger.

结果表明，无论加刻什么类型的横向细沟槽，声压级都大幅升高；速度对声压级的影响程度大于负荷；在3种类型的横向细沟槽中，S形直沟槽噪声较小，且正、反转时声压级差异小；15°斜沟槽声压级较0°与15°交替排列沟槽略高，但0°与15°交替排列沟槽的正转和反转声压级差异较大。关键词：轮胎；轮胎噪声；胎面花纹；横向细沟槽中图分类号：TQ336.1；TB533+。2文献标识码：B文章编号：1006-8171(2009)

The conclusions were as follows: theνO-H andνC=O IR absorption maxima shifted towards higher wave numbers after imprinting 17β-estradiol on TFMAA-co-TRIM copolymer with the red shift of theνO-H groups being apparent after precipitation polymerization for 16h while that forνC=O groups being observed after polymerization for 24h. A strong interaction between TFMAA and 17β-estradiol was confirmed by the high selectivity for 17β-estradiol, as indicted by the values of the separation factor of isomers of 17β-estradiol/17α-estradiol (2.28) and the imprinted factor (3.01). Particle diameter of TFMAA-co-TRIM polymer was between 300 nm and 1.5μm, which suited well for solid phase sorbent throughout at low column pressure. The recognition of imprinting TFMAA-co-TRIM polymer for sterol molecules was driven by enthalpy eluted with acetronitile, and low temperature was in favor of the separation of sterol structure analogues on imprinting column. TFMAA-co-TRIM polymer possessed of determinate anti-heat stability, with melting point beginning at 255.84℃, Tp=257.40℃, control TFMAA-co-TRIM polymer and imprinting TFMAA-co-TRIM polymer were respectively decompounded at 267.79℃and 343.11℃, and solid micro-extraction noddle prepared by the special polymerization also showed definite recognition for 17β-estradiol by GC/MS detecting at 270℃. By selection of various washing and elution solvents, elution reagents of close polymerization system were of more advantage in template molecules retention and recognition on molecularly imprinted solid phase extraction column. At a certain extent, progesterone, 17α-estradiol, 17β-estradiol and 4-androstene-3, 17-dione could be intercepted on the MISPE column. Especially, MISPE had high selectivity for progesterone, and imprinting TFMAA-co-TRIM polymer could achieve adsorption balance within 50 min by absorption kinetics test for 17β-estradiol. However, MISPE column showed better selectivity and enrichment property for 17β-estradiol than C18 and CSPE columns according to the data from HPLC and GC/MS analyses. Recovery of 17β-estradiol on MISPE column was up to 85.5% while when prime extracting solution of milk powder was sampled, the recovery of CSPE and C18 columns were 43.7% and 30.7%, respectively.

通过研究阐明：紫外聚合产物TFMAA-co-TRIM中的νO-H振动吸收峰在聚合16h后红移，νC=O振动吸收峰在聚合24h后红移；TFMAA-co-TRIM对雌二醇异构体的印迹因子达到了3.01，α为2.28，优于其它功能单体参与得到的聚合物识别特性；TFMAA-co-TRIM聚合物粒径介于300 nm至1.5μm之间，作为色谱固定相具有良好的通量和低的柱压；在乙腈流动相中，TFMAA-co-TRIM分子印迹固定相的分离过程主要被焓驱动，低温有利于分子印迹固定相分离甾醇结构类似物；TFMAA-co-TRIM分子印迹聚合物在255.84℃时开始熔融，Tp=257.40℃，聚合物CP的降解温度在267.79℃，MIP降解温度在343.11℃，制备的固相微萃取头初步经GC/MS 270℃的耐热性测定；不同的洗提溶剂筛选证明了选择接近聚合溶剂的洗脱体系更有利于MISPE发挥识别效应；分子印迹固相萃取柱对孕酮、17α-雌二醇、17β-雌二醇和雄烯二酮都具有不同程度的保留特性，可作为此类化合物的吸附材料，特别对孕酮强保留的富集特性，可作为孕酮的选择性识别吸附剂，其分子印迹聚合物对17β-雌二醇的吸附动力学测定显示在50 min内基本达到吸附平衡，具有作为传感器核心敏感材料的潜力；对比萃取奶粉中17β-雌二醇性能，MISPE柱比非分子印迹固相萃取柱和C18柱具有更高的保留，回收率依次为85.5%，43.7%和30.7%。

A new general kinetic equation was derived in which the effect of the removal of condensation water was taken into account completely, and was applied to the polyesterification kinetic study of AA/HPHP and AA/NPG. It was found that the reaction order of self-catalyzed polyesterification was not constant. For these polyesterifications, the reaction order was 2.5 at a low temperature, while 3.0 at a high temperature.

考虑缩合水的排除对反应体系的影响，用体积浓度单位推导出一个新的聚酯反应总包动力学方程，并应用到AA/HPHP和AA/NPG两个聚酯化反应的动力学研究中，研究发现，自催化聚酯反应的反应级数并不是固定值，对于AA/HPHP和AA/NPG两个聚酯化反应而言，低温时反应级数为2.5，高温时反应级数为3.0。

It was the best of times, it was the worst of times, it was the age of wisdom, it was the age of foolishness, it was the epoch of belief,it was the ep och of incredulity.

这是一个隆盛之世，但也是一个衰微之世；这是一个智慧的时代，但也是一个愚蠢的时代；这是一个有信仰的新纪元，但也是一个充满怀疑的新纪元。

The results showed that the number of chromosome, which was from the cultured seedlings of meristem tip and the rank seedlings of meristem tip, was not altered, both the number were 2n=16,the hereditary stability of callus and regeneration plant was poor; and the variation percentage of chromosome in callus was 43.4%, among which haploid accounted for 6.7%, triploid accounted for 2.5%,tetraploid accounted for 10%,pentaploid accounted for 4.2%,hexaploid accounted for 3.3%,septuploid accounted for 4.2%,octoploid accounted for 3.3%,dysploid accounted for 9.2%;the chromosome variation percentage of differentiation seedlings derived from callus was11.7%,among which haploid was 6.7%,triploid accounted for 1.7%,tetraploid was 3.3%.

结果表明，茎尖分生组织培养的幼苗及丛生苗遗传稳定，其染色体未发生倍性变异，均为2n=16；愈伤组织及其再生苗遗传稳定性较差，愈伤组织染色体数变异率为43.4%，其中单倍体占6.7%、三倍体占2.5%、四倍体占10%、五倍体占4.2%、六倍体占3.3%、七倍体占4.2%、八倍体占3.3%、非整倍体占9.2%；愈伤组织分化苗染色体变异率为11.7%，其中单倍体占6.7%，三倍体占1.7%，四倍体占3.3%。

Moonlight shadow -- Mike Oldfield The last that ever she saw him Carried away by a moonlight shadow He passed on worried and warning Carried away by a moonlight shadow Lost in a river last Saturday night Far away on the other side He was caught in the middle of a desperate fight And she couldn't find how to push through The trees that whisper in the evening Carried away by a moonlight shadow Sing a song of sorrow and grieving Carried away by a moonlight shadow All she saw was a silhouette of a gun Far away on the other side He was shot six times by a man on the run And she couldn't find how to push through I stay, I pray See you in heaven far away I stay, I pray See you in heaven one day Four a.m. in the morning Carried away by a moonlight shadow. I watched your vision forming Carried away by a moonlight shadow Star was light in a silvery night Far away on the Will you come to talk to me this night But she couldn't find how to push through Caught in the middle of a hundred and five The night was heavy but the air was alive.

But she couldn't find how to push through 月光的影子麦克欧菲尔德她最后一次见到他因为月光的影子而失去意识他发出了警讯因为月光的影子而失去意识上个周末夜在河里迷失在远远的那一边他被困在一场亡命的打斗中而她不晓得该如何是好树林在黄昏时分低语因为月光的影子而失去意识唱一首关於忧愁与悔恨的歌因为月光的影子而失去意识她看到的是一把枪的轮廓在远远的那一边他被一个奔跑的男子连开六枪而她不晓得该怎麼办才好我停留，我祈求在遥远的天堂相见我停留，我祈求总有一天在天堂凌晨四点钟因为月光的影子而失去意识我注视著你的幻影形成因为月光的影子而失去意识银色的夜里星光熠熠在远远的那一边今晚你会来找我吗但她不晓得该怎麼办才好夜色沉重但空中充满生气但她不晓得该怎麼办才好

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。