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The reversible photoisomerization of HOOCAzoC4SH SAM was studied by UV-Vis absorption spectrum and atomic force microscopy techniques.

首先合成羧基偶氮苯衍生物，并在金膜表面制备偶氮苯自组装膜，采用紫外吸收光谱、原子力显微镜观察偶氮苯衍生物的光学顺反异构现象以及偶氮苯自组装膜表面形貌的变化。

Their UV-Vis absorption and photoluminescent properties, as well as their electrochemical properties and thermal stability were also studied.

研究结果表明，这类双极传输材料具有咔唑和芳基噁二唑双功能基的紫外可见吸收和光致发光综合特性。

The UV-vis absorption and photoluminescent spectra of the systems in n-hexane, tetrahydrofuran, and CH2Cl2 are investigated.

并用UV-vis和PL测定了此类化合物在正己烷、四氢呋喃和二氯甲烷不同极性溶剂中的发光性能。

The concentrations of petroleum in photolytic processes were analyzed by UV-Vis.

结果表明，石油在土壤表面上的光化学降解行为符合准一级反应动力学，实验测得石油的光解速率常数为0.002 6-0.017 2 h^-1，半衰期为

In this paper, twenty novel meso-substituted porphyrins of four series were designed and synthesized by increasing the conjugation of porphyrins or introducing substituents with high fluorescence quantum yield into the meso-position of porphine, and then red OLEDs were fabricated by doping porphyrins into a suitable host using ten porphyrins compounds and their electrolumin -escence properties were tested. The main contents and results were generalized as follows:Three meso-tetrakisporphyrins 4a-c and three conjugations of porphine-triarylamine linked by styrene 10a-c were synthesized and characterized by 1H NMR, MS, UV-vis spectra and fluorescence emission spectra.

本文通过增大卟啉分子的共轭结构或将具有高荧光量子产率的基团连接到卟吩环的中位得到了四类共20个新型的卟啉化合物，并选取其中10个化合物制备有机发光器件来考察材料的电致发光性能，具体内容包括以下几个部分：设计合成了3个中位直接被三芳胺取代的卟啉化合物4a-c和3个通过苯乙烯连接的卟吩-三芳胺共轭体10a-c，通过核磁氢谱、质谱、紫外吸收光谱和荧光发射光谱表征了新化合物的结构。

A new unsymmetrical metal porphyrin- 5-{4-[3-(2-nitro-phenoxyl) propoxy]phenyl }-10, 15, 20-tri-(4-methoxy phenyl )porphyrin copper (compound Ⅱ)was synthesized,and its UV-Vis spectra were measured and compared with other three symmetrical metalporphyrins.

本文合成了一个新的非对称卟啉铜化合物，测量了其紫外－可见光谱，并将此光谱结果与其他三种对称金属卟啉的光谱进行了比较。

Pseudocubic shaped α-Fe2O3 nano-films were prepared by dip-coating technique. The structure, morphology and spectroscopy of the thin films were characterized by XRD, AFM, UV-Vis and FT-IR methods.

采用浸渍提拉法制备了准立方体α-Fe2O3纳米薄膜，利用XRD、AFM、UV-Vis和FT-IR对其表面形貌和谱学性质进行了表征。

Two new binuclear complexes, [TpCu(μ-1, 1-N3)2CuTp](1) and [Tp(superscript *)Co2CoTp(superscript *)](2) Tp=tri (pyrazolyl borate and Tp(superscript *)=3,5-dimethyltri borate, have been synthesized and characterized by IR, UV-vis, ESR, and CV. The crystal structures of both complexes have been determined by X-ray single crystal diffraction.

合成了两个新型的含三吡唑硼配体的双核铜配合物[TpCu(μ-1， 1-N3)2CuTp](1)和双核钴配合物[TpCo2CoTp](2)，并通过IR，UV-vis，EPR，CV，X-射线单晶衍射等手段进行表征。

The method by drying/adsorption was used to prepare DNA adsorptively modified electrodes, and thus-resulting DNA-modified electrodes were electrochemically and spectroscopically characterized, including cyclic voltammetry, scanning tunneling microscopy, Raman spectroscopy, in-situ UV/Vis reflection spectroscopy, X-ray photoelectron spectroscopy, and alternating current impedance. Some information about the state of DNA immobilized on electrode surfaces was obtained.

鉴于此，本论文工作首先利用简便的干燥吸附法制备获得DNA吸附修饰电极，采用电化学方法及多种谱学仪器方法如STM，XPS，Raman，交流阻抗，UV-Vis现场光谱等对DNA修饰电极进行了表征，获得了有关DNA在电极表面状态等有价值的信息；又采用自组装单分子层修饰技术，制备出DNA共价键合修饰SAM/电极，并对制备条件进行了优化，利用XPS及电化学方法对修饰电极进行了表征。

Titanium incorporated mesoporous molecular sieves Ti-MCM-41, Ti-HMS, and Ti-MSU were synthesized through S〓I〓, S〓I〓, and N〓I〓 pathways using cetylpyridium bromide, tetredecylamine, and polyoxyethylene (10) stearyl ether as the structure-directing agents, respectively. The framework structure and the titanium coordination environment of these materials were characterized by XRD, N〓 adsorption/desorption, TG, TEM, FT-1R, DR UV-Vis, and ICP-AES. It was confirmed that the titanium was highly dispersed in the silica-based framework positions, and all samples were free of extra framework titanium impurities. The catalytic performance of these titanium containing mesoporous materials was investigated in the oxidation of styrene with aqueous H〓O〓 as the oxidant.

以TEOS和TBOT为硅源和钛源，分别以溴代十六烷基吡啶、十四胺和十八烷基聚氧乙烯基醚为模板剂，通过S〓I〓、S〓I〓和N〓I〓方式合成了含钛的介孔分子筛Ti-MCM-41、Ti-HMS和Ti-MSU，用XRD、N〓吸附/脱附、TEM、FT-IR、DR UV-Vis和ICP-AES等方法对它们的骨架结构、孔道结构以及钛原子的存在方式等进行了系统表征，结果表明钛原子以高分散的形式存在于以SiO〓为基本单元的介孔分子筛的骨架结构中，制备过程中未形成聚集态的骨架外金属氧化物物种。

Methods Clinical data of 3 cases of bile duct injury during laparoscopic cholecystectomy were analyzed retrospectively.

回顾总结3例LC术中胆管损伤的临床资料，分析3例胆管损伤的原因及对策。

These techniques are applied to the gobang.

本文将这些技术用于五子棋中。