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In this paper, the main work has been focused on the rare reported arsenomolybdates, and nine novel compounds have been synthesized. Sandwich arsenomolybdates:(NH_4)_(12)[Cr_2AsMo_7O_(27_2]·11H_2O (1)(NH_4)_(14)[Cu_2AsMo_7O_(27_2]·13H_2O (2) Double sandwich arsenomolybdates:(NH_4)_(12)Cu(H_2O)_4[As_2Fe_6Mo_(22)O_(85)(H_2O)]·19H_2O (3)(NH_4)_(15)[As_2CoFe_5Mo_(22)O_(85)(H_2O)]·16H_2O(4)(NH_4)_(14)Mn_(0.5)[As_2Fe_5MnMo_(22)O_(85)(H_2O)]·22H_2O(5) Cagelike arsenomolybdate:(NH_4)_(11)[AgAs_2Mo_(16)O_(54)]·9H_2O (6) Organic-inorganic molybdenum arsenate complexes:CuAs_6Mo_6O_(30{[Cu_4]_3[CuAs_6Mo_6O_(30)]}_2·6H_2O (7),[Cu_2]_3[As_3Mo_3O_(15)]_2·2H_2O (8)(NH_4)_(10){Cu(H_2O)_4}[AsMo_6O_(21)(O_2CCH_3)_3]_2·12H_2O (9)All of the above polyoxomolybdates were characterized by IR spectroscopy, TG-DSC, elemental analysis, and single-crystal X-ray analysis to identify their structures and chemical compositions.

本文选择目前报道尚少的砷钼杂多化合物为研究重点,合成了不同结构类型的九个新的杂多化合物:单夹心化合物:(NH_4)_(12)[Cr_2AsMo_7O_(27_2]·11H_2O(1)(NH_4)_(14)[Cu_2AsMo-7O_(27_2]·13H_2O(2)双夹心化合物:(NH_4)_(12)Cu(H_2O)_4[As_2Fe_6Mo_(22)O_(85)(H_2O)]·19H_2O(3)(NH_4)_(15)[As_2CoFe_5Mo_(22)O_(85)(H_2O)]·16H_2O(4)(NH_4)_(14)Mn_(0.5)[As_2Fe_5MnMo_22_O_(85(来源:AbcccBC论文网www.abclunwen.comH_2O]·22H_2O(5)笼状结构化合物:(NH_4)_(11)[AgAs_2Mo_(15)O_(54)]·9H_2O(6)有机配体修饰的化合物:CuAs_6Mo_6O_(30{[Cu_4]_3[CuAs_6Mo_6O_(30)]}_2·6H_2O(7) [Cu_2]_3[As_3Mo_3O_(15)]_2·2H_2O(8)(NH_4)_(10){Cu(H_2O)_4}[AsMo_6O_(21)(O_2CCH_3)_3]_2·12H_2O(9)对上述新化合物进行了瓜光谱分析、元素分析、热分析和X-射线单晶衍射测试,确定了它们的组成和结构,对部分化合物还进行了UV-vis及荧光光谱分析和循环伏安表征。

By means of UV-vis spectrophotometer, the complex abilities of calix [4] arene ligands with metal ions were researched, and the effect of solvent systems was discussed.

使用紫外-可见分光光度法研究了杯[4]芳烃配体与金属离子的络合性质,并考虑了溶剂对配体与金属离子配位的影响,评价了杯[4]芳烃的不同取代基对过渡金属离子及稀土离子的配位作用。

Fluorescence, UV-vis and NMR are the most common methods in the research of chiral recognition. According to these methods, the latest research progress in the synthesis of chiral receptors based on calix[4]arenes and their applications in the chiral recognition are summarized.

在手性识别的研究中,荧光、紫外和核磁是3种最常见的研究方法,本文根据这3种方法进行分类,综述了近年来以杯[4]芳烃为分子骨架的手性受体的合成及其在手性识别中的应用。

UV-VIS spectrophotometry method and HPLC were used to determine the content of total flavone and gallic acid in Polygonum capitatum from five different provenances.

方法]采用紫外分光光度法和高效液相色谱法分别测定5批不同种源头花蓼中总黄酮及没食子酸的含量。

The results can be expressed as follows:(1) With the increase of water phase content, the amine salt aggregated orderly in different forms such as W/O micro-emulsion, nodus-knot catenulate aggregates, layer liquid crystal and O/W micro-emulsion.(2) In layer liquid crystal, SO〓 mainly combined with amine salt cation by two oxygen atoms in bridge.(3) In UV-VIS spectrum of layer L. C., there is an absorption about 500 nm and "light short circuit"appeared about 430 nm. These phenomena may be very important for measuring the distance between the layers of the L.

研究发现该体系随水相含量的增加,胺盐发生不同形式的有序缔合,分别形成了W/O型微乳液、&节-结&型链状缔合体、层状液晶和O/W型微乳液:在层状液晶中,SO〓主要以桥式双齿配位形式存在,中性胺分子有利于体系中液晶的形成;层状液晶于500nm波长处有一吸收峰,在430nm附近发生&光短路&现象,该现象可能对测定层状液晶的层间距有重要意义。

UV-Vis spectrum showed that some monomer or oligomer were existed in this film. The results demonstrated that the PPy chains were served as both the reductant of chloroauric acid and the ligands to stabilize gold-NPs.

接着利用吡咯单体及寡聚体具有的还原性,将新合成的聚吡咯膜浸泡在氯金酸水溶液中搅拌反应,通过扫描电镜观察发现,在膜中还原生成了大量的金纳米粒子,同时在膜的表面也观察到了金纳米粒子的存在。

And the content of capillary ion chromatography instrument includes micro-flow pump, injector, suppressors, conductometric detectors, UV-Vis detectors and fluorescence detectors with small volumes.

对毛细管离子色谱仪的总结包括微流量泵、小体积进样器、适合毛细管离子色谱系统的小体积抑制器、电导和光学检测器等。

And the content of capillary ion chromatography instrument includes micro-flow pump, injector, suppressors, conductometric detectors, UV-Vis detectors and fluorescence detectors with small volumes.

对毛细管离子色谱仪的总结包括微流量泵、体积进样器、合毛细管离子色谱系统的小体积抑制器、导和光学检测器等。

Raman spectrum, UV-Vis spectra, IR, NIR and XPS spectra were used to characterize the material. The result indicates that there is a conjugative effect between MWNT and bromine, which induces the change of electron distribution on the MWNT surface. It increased the car- rier density and the electrical conductivity of MWNT became higher.

通过拉曼光谱,紫外可见光谱,红外吸收光谱,近红外吸收光谱和X光电子能谱等方法研究,结果表明:溴与多壁碳纳米管之间存在共轭作用,使多壁碳纳米管表面的电子云分布发生了变化,导致空穴载流子的产生,增加了载流子浓度,提高了多壁碳纳米管的导电性能。

The structure of cuprous oxide nanospheres was characterized by XRD, SEM, BET and UV-vis spectrophotometer.

采用XRD、SEM、BET和紫外-可见分光光度法等手段对所制备的纳米Cu2O开口空心球进行表征。

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