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The synthesis of the pentacyclic skeleton of Et-743 and the construction of the five chiral centers thereof.1. The core pentacyclic skeleton of phthalascidin was constructed with L-dopa as the starting material via thirteen steps. First, two basic synthons, the C-1 functionalized tetrahydroisoquinoline compounds 8 and N-protected Z-dopa derivative 9, were prepared from L-dopa. They were coupled via amide bond to form the dipeptide compounds 10, which were the first key intermediates. Then the primary hydroxyl groups were transformed into the corresponding amino aldehydes 11 via Swern oxidation. Followed by the intramolecular Pictet-Spengler cyclization, the pentacyclic compounds 12 were synthesized.

五环骨架的构建及五个正确手性中心的确立：1.1我们以L-多巴为起始原料，经过多步官能团保护和转化合成了基本结构单元8然后和苯丙氨酸衍生物9，通过缩合反应生成酰胺中间体10，经Swern氧化得到醛化合物11，然后再次利用分子内改良的Pictet-Spengler反应一步构建c，d两环，得到五环骨架化合物12，最后，实现了21-位羰基向氰基的转化，得到了C-1位官能化的化合物14，化合物14不但具有和Et-743一致的五环骨架，而且分子中五个手性中心立体构型也与其完全相同：其中，3，位和13，位的手性中心由原料L-多巴带入，而1，位，11，位和21，位手性中心则通过不对称诱导而确立。

A system for transmitting a signal via diversity antennas (60, 70; 150, 160, 170, 180; 190, 200) includes: at least one delay element (100) for generating at least one delayed replica of the signal subject to a given delay; the signal and the at least one delayed replica being adapted to be transmitted via the diversity antennas (60, 70; 150, 160, 170, 180; 190, 200), and a control unit (110) for the at least one delay element (100) for varying (110) the given delay (100), whereby the signal and the at least one delayed replica, transmitted via the diversity antennas (60, 70; 150, 160, 170, 180; 190, 200), give rise to alternate constructive and destructive combinations therebetween.

一种用于经由分集天线(60、70；150、160、170、180；190、200)传送信号的系统包括：用于生成受到给定延迟的信号的至少一个延迟复件的至少一个延迟部件(100)；该信号和该至少一个延迟复件适合于经由该分集天线(60、70；150、160、170、180；190、200)传送，以及用于至少一个延迟部件(100)改变(110)该给定延迟(100)的控制单元，由此该信号和该至少一个延迟复件经由分集天线(60、70；150、160、170、180；190、200)传送，导致在其间交替的建设性和破坏性组合。

In this research, the spider silk from the major ampullate gland of native Nephila pilipes was collected via the forced-silking apparatus at the reeling speed of 3 m/min. The obtained silk was dissolved in hexafluoro-isopropanol. The influence of pH and temperature over the secondary structure of the silk protein in solution state was examined via Circular Dichroism. The effect of silk concentration and electrical field strength on the structure conformation of silk protein during film casting process was investigated via FT-IR. During the drying process, the increase of silk concentration and the presence of electric field tend to form β-sheet and β-turn. Finally, the dried film of silk protein was treated with different temperatures and cation solutions to study the post-treatment effects.

本研究所采用之蜘蛛丝蛋白质系取自本土品种人面蜘蛛之大囊壶腺体，以3 m/min之卷丝速度强迫取丝(forced-silking)收集蜘蛛丝，再将纤维溶於六氟异丙醇溶剂中配制成溶液，以圆二色光谱仪分析在不同 pH 值与温度条件下丝蛋白质在溶液中之二级结构变化，再将蜘蛛丝溶液以不同浓度及电场强度下乾燥成薄膜后，以傅立叶红外线光谱仪检测分析丝蛋白质在固体状态下之二级结构，最后以不同温度加温、离子溶液浸泡等条件对乾燥所得之薄膜进行后处理，并分析其二级结构之变化。

The enteroscopy with general anesthesia via the mouth was well tolerated, followed by non-anesthesia enteroscopy via the anus, and non-anesthesia enteroscopy via the mouth and enteroclysis.

全麻下经口腔进镜推进式双气囊小肠镜检查的患者耐受性最佳，其后依次为非麻醉经肛门进镜、非麻醉经口腔进镜和小肠钡灌检查。

The invention provides a dual redundant CAN bus controller, which is arranged on a crewel CAN bus, characterized in that: two CAN bus transceiving modules, two initializing modules are respectively corresponding to the CAN bus controller module A and CAN bus controller module B; the two CAN bus controller modules are respectively connected to the two CAN bus via a driver shifting control unit; the initializing module is connected to the bus control initializing register for initializing the e CAN bus controller modules; a protocol processing module is connected to the FIFO buffer; the FIFO buffer is connected to the node processor via the logical interface; a intermitting process unit sends the corresponding intermitting control signal to the CAN bus transceiving modules according to the CAN bus controller modules; one path of the CAN bus controller module is directly connected to the protocol processing module; another path is connected to the protocol processing module via the bus receiving buffer.

本发明提供了一种双冗余CAN总线控制器，设置于双线CAN总线上，其特征在于：两个CAN总线收发模块、两个初始化模块分别与CAN总线控制器模块A和CAN总线控制器模块B相对应；两个CAN总线控制器模块通过驱动器切换控制单元分别与两条CAN总线相连；初始化模块与总线控制器初始化寄存器相连，对所对应的CAN总线控制器模块进行初始化；协议处理模块与FIFO缓存器相连；FIFO缓存器通过逻辑接口与节点处理器连接；中断处理单元根据CAN总线控制器模块的控制命令对CAN总线收发模块发出相应的中断控制信号；CAN总线收发模块一路与协议处理模块直接相连，另一路通过总线接收缓存器与协议处理模块相连。

The composition and structure of Soybean Protein Isolate are first introduced,Then the functional modification of SPI via chemical ways which include the reaction of amino group,carboxyl group and sulphydryl group,via enzymic ways which include the modification using transglutaminase enzyme and papain,via physical ways which include blending and heat treatment are reviewed.

首先介绍了大豆分离蛋白的基本组成与结构，然后分别从化学改性、酶改性和物理改性三个方面对大豆分离蛋白改性进行了综述。其中，在化学改性方面，针对大豆分离蛋白中含有的氨基、羧基、巯基等不同活性基团的改性原理及研究现状进行了介绍。在酶改性方面，主要介绍了谷胺酰胺转胺酶、木瓜蛋白酶等对大豆分离蛋白的改性作用。在物理改性方面，介绍了共混、加热改性等目前研究较多的方法。

The mice in experimental group and control group were exposed to 350 cGy radiation produced by 60Co. After 3 h, karyocytes at different concentrations in the fresh human umbilical cord blood were injected into the mice in experimental group A, B, C via their tail veins, and the equal volume of normal sodium was also injected into control group via tail veins. After one month, carbon tetrachloride (CCl4) was injected into experimental group A, B and control group via abdominal cavity, and the equal volume of normal sodium was injected into experimental group C. After two months, immunohistochemistry and reverse transcriptase polymerase chain reaction were used to detect the expressions of human cytokeratin-18 (CK18), cytokeratin-19 (CK19) and albumin in liver tissues of all mice.

采用60Co治疗仪γ射线对实验组和对照组行350cGy的亚致死剂量照射，实验组A、B、C3组照射后3h内经尾静脉分别输入1.0×10^7个/只、2.0×10^7个/只和3.0×l0^7个/只人新鲜脐血有核细胞，对照组经尾静脉注入等体积无菌生理盐水。1个月后对实验A、B组和对照组裸鼠经腹膜腔注射四氯化碳(CCl4)，实验C组注射等体积生理盐水。2个月后采用免疫组化和RT-PCR方法检测裸鼠肝组织人源性CK18、CK19和人源性白蛋白的表达。

Once you get of the train, proceed to the main gallery of the station, take the exit to you right and turn left into Via Marsala cross the traffic light and turn right to Via Solferino ,follow the Piazza Indipendenza around to the left and turn left on Via Castelfidardo at the traffic light on that corner.

我们要求阁下输入阁下的信用卡资料，只是发送您的资料到酒店，以保证阁下的预订成功。您只会在酒店直接结帐。然而，如您所预订的酒店要求需要缴交押金，这些信息都会列明在&取消条款&条目内，而押金将会直接跟所选择的酒店进行结帐。

The geology research of carbonate reservoirs in Ordovician of Tahe oilfield showed that many large dissolved vugs and fractures were developed. The spread of the reservoir take on a very heterogeneous state. And the typical fractured-vuggy reservoirs was formed. According to the combination of the various spaces, the formation was divided into vuggy formation, fractured-vuggy formation and fractured formation. The research showed that development of the vug is relevant to the its position on the structure, the fractures, the water surface and the weathering surface. Multi-phase charge and recharge of the oil in the reservoirs resulted in the complexity of the fluid distribution. So the"Bottle Model"was brought forward to explain the movement of the water-oil contact. The special storage space and the complex fluid distribution lead to the unstability of the production and the complexity of the water cut. In order to explain the characteristic of the fracture-vug unit was brought forward and the basic principle and method of the partition of the fracture-vug unit was formed. The classification and evaluation of the units were performed according the reserve and energy. Based on the research of geology characteristic and the fluid flow in the reservoir the comprehensive numerical simulation plan of the fractured-vuggy reservoirs were established. Through the selection of the simulation unit, fluid flow type and parameter equivalent the triple media reservoir simulation model was established. Considering the practical application the model was resolved by the DKR decomposition conjugate grads method. Based on the fine reservoir description of Dsitrict IV of the Tahe oilfield the various space type were classified and combined together. The geology model of Unit S48 was constructed. Two typical single well model was established according to the geology and the dynamic phenomena. Finally the single well model and the Unit S48 were simulated by the triple media reservoir simulator. Via the local grid refinement and coarsening in the simulation good matchs were gained. Based on the results of the simulation the reserve distribution, percent of reserve produced in various space and the natural energy were analyzed. The fluid was storaged in the fractures and vugs mostly and more than 90% the produced oil came from the systems. The energy belonged to the active one. The results of simulation accorded with the fact and showed the validity and practicability the research and the simulator.

塔河油田奥陶系碳酸盐岩油藏的地质研究表明，其储层中发育着很多大型的溶蚀洞、缝，储层的平面展布呈现出极度的非均质性，形成了典型的缝洞型碳酸盐岩油藏，根据各种孔隙介质在储层中的组合，将储层分为了溶洞型、裂缝-溶洞型和裂缝型三类；研究表明溶洞储层的发育和构造位置、裂缝的发育、潜水面和风化面的位置等因素有关；多期充注的油气成藏模式导致了流体复杂的赋存状态，由此提出了所谓的"瓶子模型"，解释生产过程中油水界面的变化；特殊的储集空间类型和流体分布特征导致油田在开发过程中表现出很大的不确定性和含水变化的复杂性，为了合理的解释油气田开发过程中的动态特征，提出了"缝洞单元"的概念，并制定了"缝洞单元"纵横向划分的基本原则和依据及划分方法，并对"缝洞单元"进行了分类和评价；基于地质特征和流体在其中流动规律的研究，提出了缝洞型碳酸盐岩油藏的数值模拟综合解决方案，通过模拟单元的选择、流动类型和参数的等效，建立了三重介质油藏三维三相数值模拟模型，采用不完全LU分解预处理共轭梯度法进行了求解；在塔河油田4区精细油藏描述的基础上，将各种类型的孔隙空间进行了归类组合，建立了S48单元的地质模型；通过对油井生产动态进行分析研究，建立了两类和油井地质、生产动态相对应的单井模型；最后应用三重介质油藏数值模拟软件对单井模型和S48单元进行了数值模拟，通过局部加密和粗化等技术模拟流体流动规律，取得了很好的拟合效果；结合数值模拟结果，分析了各种介质中的储量分布、储量产出的百分比以及地层的能量，认为塔河油田缝洞型油藏中流体绝大多数储集于缝洞系统之中，所产出流体90%以上也来自于缝洞系统，其底水能量属于较充足的类型；模拟结果和油田实际情况符合较好，说明了地质研究和油藏数值模拟研究的正确性。

As a sign of HBO 's growing interest in alternative media, the cabler has teamed with Zoom Media to market the third season of "Entourage" and DVD release of the second season via a billboard sampling campaign in 150 gyms and 135 bars and restaurants in New York and Los Angeles.

HBO 与 Zoom 传媒合作，在纽约和洛杉矶的150个体育馆和135个酒吧餐馆通过路牌取样广告活动为《明星伙伴》第三季节目的播出以及第二季 DVD 的发行做宣传，这也表明 HBO 对非主流媒体的兴趣越来越浓。

But this is impossible, as long as it is engaging in a market economy, there are risks in any operation.

但是，这是不可能的，只要是搞市场经济，是有风险的任何行动。

We're on the same wavelength.

我们是同道中人。