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Based on the previous literatures, the following major innovation works were carried out in this dissertation:(1) The derivatization reaction conditions of ephedrine and pseudoephedrine with sensitive derivation reagent in aqueous system were studied and two new methods were developed for the assay of them by microemulsion electrokinetic chromatography and micellar electrokinetic chromatography with LIF detection. The sensitivity and analysis times were greatly improved compared with the previous reports;(2) A new method of CZE with indirect LIF detection was developed for the simultaneous determination of six coumarin compounds (esculin, esculetin, isofraxidin, genistein, naringin and sophoricoside) with fluorescein as the probe. The proposed method enlarges the application range of LIF detector, and provides new approach for the analysis of certain compounds difficult to derivatize;(3) Based on the above research, an MEKC with indirect LIF detection method for the simultaneous determination of adenine and guanine in DNA extracts from fungus, maize and soybean was established;(4) A new method for the investigation of the complexes formed between human serum albumin and ampicillin sodium under the simulated physiology conditions using laser light scattering technique was developed.

该论文在综述前人工作的基础上,开展了如下未见文献报道的创新性的研究工作:(1)使用灵敏的衍生试剂对麻黄碱和伪麻黄碱在水体系中的衍生反应条件进行了系统研究,建立了微乳电动色谱-激光诱导荧光检测法和胶束电动色谱—激光诱导荧光检测法测定麻黄碱和伪麻黄碱的灵敏分析新方法,与以前的报道相比,灵敏度和分析时间均有很大改善;(2)使用荧光素钠作为背景荧光试剂,建立了同时分析测定六种黄酮类化合物(秦皮甲素、秦皮乙素、异秦皮定、染料木素、柚皮苷和槐角苷)的毛细管区带电泳—间接激光诱导荧光检测新方法,扩大了激光诱导荧光检测的应用范围,对难衍生化合物的分离分析提供了一种新思路和新途径;(3)以荧光素钠作为背景荧光试剂,建立了一种用于同时测定食品提取DNA中的腺嘌呤和鸟嘌呤含量的胶束电动色谱—间接激光诱导荧光检测新方法;(4)用动态和静态激光散射法研究了模拟生理条件下人血清白蛋白与氨比西林钠盐相互作用所形成的复合物,为药物分子与蛋白质的相互作用、药代动力学等的研究提供了一种新思路。

In this article two functional modes of the Fly-back Converter (Continuous Conduct Mode and Discontinuous Conduct Mode) are particularly analyzed, which include their characteristics, applications, the critical pattern of two functional modes is argued, both the exact boundary from the angle of circuit parameters is crystallized, at the same time, basic principle of PFC under the DCM mode is introduced, which settle theoretical basis for the subsequent design; by establishing the mathematic model of the converter, a further investigation of the configuration is made, qualitatively and quantitatively, analyzed to settle exactly theoretical basis for the subsequent emulation and the experimental parameter; from the angle of steady-state analysis, the transfer function of the system is deduced to establish dynamic small-signal state equation, emulating the system with the help of matlab, then according to the simulation result and the theory of PFC revise the system, lastly, we adopt the project which add a zero-pole compensator to the voltage loop, by this way, a satisfied system performance is gained and the PFC scheme is ensured successfully; finally, based on the previously-done work, we combining with the situation of specific design requirement, acquired the numerical value of each unit devices in this converter

详细分析了反激式变换器的两种工作状态,连续模式(Continuous Conduct Mode ,简称CCM)和断续模式(Discontinuous Conduct Mode,简称DCM)以及各自的特点、应用场合,论证了两种工作状态的临界模式,从电路参数的角度明确了二者的界限,同时还介绍了DCM模式下PFC的基本原理,为后面的设计奠定理论基础;通过对整个变换器系统建立准确的数学模型,对此变换器的电路结构做了进一步的研究,定性、定量地分析了变换器各部分的工作状态,为仿真和实验参数的确定以及电路参数的优化提供理论依据;从稳态分析的角度,为系统建立了动态小信号状态方程并推导出系统的传递函数,利用matlab对系统进行仿真,进而根据仿真结果以及PFC的相关理论对系统进行校正,采用在电压环加入零点—极点补偿器的设计方案,得到了满意的系统特性并且保证了PFC的顺利实现;最后,在前面所做工作的基础上,结合设计要求计算出此变换器系统中每个元器件的数值,利用Pspice对其进行了仿真、优化,然后根据仿真结果搭建了硬件电路。

Based on the characteristic of the model reaction system for n Butane oxidation to maleic anhydride and the forced unsteady state operation technique in catalytic reactor, an experimental set up was built for investigation of FUSO in fixed bed reactor operated under feed composition cycling mode.

根据人为非定态操作技术和丁烷氧化制顺酐反应的特点,以 CDS- 80 4微反系统为基础,建立了一套用于丁烷氧化制顺酐固定床反应器浓度周期操作的实验装置,具有操作方便、运行可靠的特点。

Investigation on subway tunnel engineering of England was included. And the technology researching was improving under the cooperation between shng-hai suwan construction compary and Tongji University, the cooperation will garn the leading place.

本文还报道了上海地铁建设公司与同济大学携手合作开展地铁隧道复合纤维混凝土管片技术研究,将开创国内地铁隧道复合纤维混凝土管片技术之先河。

This paper deals with an experimental investigation of fault diagnosis in a multistage gearbox under transient loads.

本文论述的实验调查故障诊断中的一种多级变速箱下的瞬态负载。

Investigation was made of the sputtering rate in glow discharge lamp with re-lation to constituent of 25 different specimens of 6 binary systems, namely, Cr-Fe, Bi-Sb,Cu-Zn, Ag-Cu, Al-Zn and Cd-Sn, by measuring mass loss after each sputtering under con-stant Ar pressure and voltage applied. The correlation, in general, between sputtering rate andconcentration of constituent of these non-intermetallic binary alloys obeys the hyperbolic lawunder steady state, yet may be approximately regarded as linear only on certain special condi-tion if the two components of the alloys with similar sputtering rates.

在恒定气压和电压条件下,用测量溅射减量的方法,系统研究了Cr—Fe,Bi-Sb,Cu—Zn,Ag—Cu,Al-Zn和Cd—Sn六个系统的25个试样在辉光放电灯中溅射率与组分的关系结果表明;阴极溅射在稳态时,二元合金的溅射率与组元浓度的普遍关系是双曲线,只有在某些特殊情况下,两组元的溅射率相差不大时,可以近似看成线性关系。

"Please, praised me" is a live rural YangGongQi : because my father when the former life, especially looking to praise by time, so he went to the newspaper about how to save a risk of female students was raped OuYangHua, but no one believed him, he was constantly, finally caught everywhere, under the leadership of the newspaper correspondents ancient national anthem ryohei gloze investigation.

求求你,表扬我》讲述的是一个家住农村的打工仔杨红旗,因为父亲当了一辈子劳模,心里特别期待自己也能受一次表扬,于是他到报社讲述自己如何解救一名险被强奸的女大学生欧阳花的事迹,可是没有人相信他,他便不断地四处讲述,终于引起了报社领导的重视,派记者古国歌进行调查。

An investigation onnew type burner with inclined intersection of gyrate air flow with gas flow,renovation on furnacestructure and regulation on the vaccum pressure of windbox under furnace are also presented.

介绍了以高炉煤气为主要燃料的新型烧结节能点火炉,叙述了新设计的斜交旋转多空气流烧嘴的研制、炉体结构的改造以及点火风箱负压的控制。

Horticola , in which Compositae, Cruciferae, Laguminosae and Cucurbitaceae are the main families. It occurs seriously on lettuce, cauliflower, pea, rape and horsebean. The hosts can be divided into four types: the most fitting host, fitting host, preferable host and secondary host. The oviposition of C. horticola on 8 kinds of hosts selected was checked under microscope, which had proved the investigation of host suitability and lettuce is the favorite host.

2004年对扬州地区露地蔬菜上的豌豆彩潜蝇寄主种类及危害程度进行了调查,采用五点取样法共查到豌豆彩潜蝇的蔬菜寄主6科23种,主要分布在菊科、十字花科、豆科和葫芦科等的蔬菜上,其中以莴苣、花椰菜、豌豆、油菜、蚕豆受害最为严重;选择性田间调查和室内试验证明,莴苣是豌豆彩潜蝇最嗜好寄主。

In this paper the key points discussed were that, under the condition of a sharp hypsography of desert areas of Ordos basin, we used some new geophysical methods in the investigation of surface structure to obtain high accurate surface structure data and provide reliable scientific foundation for data acquisition and process; we dealt with the optimum coupling of surface geophones and the digital realization technique in desert areas, dug into a method of high frequency compensation according to attenuations by absorption near surface, adopted data processing and correction technique, solved high frequency attenuation and geophone coupling, eliminated the influences of sharply transverse fluctuation of hypsography in desert area on the seismic data, enhanced the fidelity and SNR of seismic section, and finally picked up more geologic information on the seismic profile and improved the precision of the lateral prediction for the reservoir beds.

本文旨在研究鄂尔多斯盆地沙漠区地表变化比较大的情况下,在表层结构调查中通过应用一些地球物理新方法,以获取高精度的表层结构数据,为资料采集和数据处理提供更科学的依据;研究在沙漠区地表检波器最佳耦合的方式与数字实现技术,研究通过近地表的吸收衰减规律进行高频补偿的方法,采用数据处理校正技术,解决高频吸收及检波器耦合,消除沙漠区表层横向剧烈变化对地震资料的影响,提高地震剖面的保真度和信噪比,从而使更多的地质信息能够从地震剖面中反映出来,提高储层横向预测的精度。

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Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气,收缩臀部肌肉;拱起身体,尽量抬起头来,右腿伸直朝向天花板(膝微屈,以避免肌肉紧张)。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化,但却比去年同期高8%。

However, to get a true quote, you will need to provide detailed personal and financial information.

然而,要让一个真正的引用,你需要提供详细的个人和财务信息。