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In the process of laboratory study, oxycodone was prepared by oxidating thebaine at 6,14-position under oxydol, hydrodeoxidizing 7,8-position double bond and 14-position ether under palladium catalyst. Furthermore, N-methyl of oxycodone was isolated byα-chloro-ethyl chloroformate under anhydrous condition and protection of 14-position hydroxyl to obtain noroxycodone, which was further converted into methylnaltrexone by N-alkylation in presence of cyclopropyl bromomethane, then by isolating 3-position methyl of methylnaltrexone under boron tribromide, becoming hydrochloride to prepare target compound, natrexone hydrochloride.

实验室工艺方面，本文首先用双氧水氧化蒂巴因的6-位和14-位、在钯炭催化下加氢还原7-8位双键和14-位醚合成羟考酮，然后提出并优化了在无水和14-位保护的情况下，用氯甲酸-α-氯乙酯脱去羟考酮的N-位甲基合成去甲羟考酮，再用环丙甲基溴将去甲羟考酮的N-位烷基化合成甲基纳曲酮，最后采用三溴化硼脱去甲基纳曲酮的3-位甲基和成盐酸盐合成盐酸纳曲酮。

Where two or more policies are effected by or on behalf of the assured on the same adventure and interest or any part thereof, and the sums insured exceed the indemnity allowed by this Act, the assured is said to be over-insured by double insurance (2) Where the assured is over-insured by double insurance The assured, unless the policy otherwise provides, may claim payment from the insurers in such order as he may think fit, provided that he is not entitled to receive any sum in excess of the indemnity allowed by this Act; Where the policy under which the assured claims is a valued policy, the assured must give credit as against the valuation for any sum received by him under any other policy without regard to the actual value of the subject-matter insured; Where the policy under which the assured claims is an unvalued policy he must give credit, as against the full insurable value, for any sum received by him under any other policy; Where the assured receives any sum in excess of the indemnity allowed by this Act, he is deemed to hold such sum in trust for the insurers according to their right of contribution among themselves.

当被保险人或其代表，(1)就同一冒险和利益或其中的一部分订立了两份以上的保险单，且保险金额超过本法所允许的赔偿限额时，被保险人即被视为因重复保险而超额保险。(2)在被保险人因重复保险而超额保险之场合：除非保险单另有规定，被保险人可根据自已认为合适的顺序，依次向其保险人索赔，但他所得金额不得超过本法允许的赔偿限额；如果被保险人凭以索赔的保险单是一份定值保险单，被保险人必须将其他保险单项下他已收取的任何数额从约定保险价值中扣除，无需考虑保险标的的实际价值；如果被保险人据以索赔的保险单是一份不定值保险单，被保险人必须将其他保险单项下他已收取的数额从全部保险价值中扣除；若被保险人得到的金额超过本法所允许的赔偿额，则此种超出金额即被视为由被保险人代各保险人托管，由保险人按他们之间的分摊权利摊回。

Where two or more policies are effected by or on behalf o f the assured on the same adventure and interest or any part thereof, and the sums insured exceed the indemnity allowed by this Act, the assured is said to be over-ins ured by double insurance (2)Where the assured is over-insured by double insurance The assured, unless the policy otherwise provides, may claim payment from the insurers in such order as he may think fit, provided that he is n ot entitled to receive any sum in excess of the indemnity allowed by this Act;Where the policy under which the assured claims is a valued policy, the assured must give credit as against the valuation for any sum rec eived by him under any other policy without regard to the actual value of the subject-ma tter insured;Where the policy under which the assured claims is an unvalu ed policy he must give credit, as against the full insurable value, for any sum rec eived by him under any other policy; Where the assured receives any sum in excess of the indemnit y allowed by this Act, he is deemed to hold such sum in trust for the insurers acco rding to their right of contribution among themselves.

1当被保险人或其代表，就同一冒险和利益或其中的一部分订立了两 32。份以上的保险单，且保险金额超过本法所允许的赔偿限额时，被保险人即被视为因重复保险而超额保险。(2)在被保险人因重复保险而超额保险之场合：除非保险单另有规定，被保险人可根据自己认为合适的顺序，依次向其保险人索赔，但他所得金额不得超过本法允许的赔偿限额；如果被保险人凭以索赔的保险单是一份定值保险单，被保险人必须将其他保险单项下他已收取的任何数额从约定保险价值中扣除，无需考虑保险标的的实际价值；如果被保险人据以索赔的保险单是一份不定值保险单，被保险人必须将其他保险单项下他已收取的数额从全部保险价值中扣除；若被保险人得到的金额超过本法所允许的赔偿额，则此种超出金额即被视为由被保险人代各保险人托管，由保险人按他们之间的分摊权利摊回。

Hyphae, loaded with CTC under pH 6. 8 condition and then grown in pH 8. 0 medium for a little while to destroy the apical acidification, could gave very diffuse fluorescence images of CTC membrame bound Ca〓 and vermiform fluorescence spots due to mitochondrias under pH 6. 8 no longer were clearly distinquished, which implied that besides mitochondrias, other cellular organelles with Ca〓 also were stained with CTC. Thus mitochondrias are not the only one intracellular Ca〓 storage, endoplasmic reticulums and Golgi bodies in the same zone may be also the Ca〓 storages. But the extreme apical zone under 2μm of the growing hyphal tip was still almost devoid of stain under pH 8. 0.The CTC fluorescence was concentrated in the subapic zone beyond about 2μm from the tip and then gradually became lower behind about 40μm from the tip. These results did not support the hypothesis which suggested that the cell wall vesicles in the extreme apical zone were intracellular Ca〓 storages.

将菌丝在pH6.8条件下负载CTC，再置于pH8.0培养介质中短暂生长一会儿以消散菌丝顶端的酸化区域，则CTC膜结合Ca〓呈现弥散的荧光影像，在pH 6.8培养条件下显示的蠕虫状的线粒体荧光斑点不再能够清晰辨认，说明除了线粒体之外，还有其它含Ca〓细胞器，也被CTC染色，线粒体并不是细胞内唯一Ca〓库，还可能包括内质网、高尔基体等细胞器，但菌丝最顶端2μm以前的细胞壁泡囊区域不能被染色，最大荧光强度仍位于菌丝顶端2μm以后区域，约45μm以后荧光变弱，实验结果不支持细胞壁泡囊为菌丝胞内Ca〓库的假设。

Pereme , separately are 209%,295%,285%; the increasing of accumulating amount separately are 209%,295%,285%; The use of silicon has a tread to rise dry weight of Bermudagrass ,Agrostis Lolium. Pereme ; Under the drought condition , the use of silicon suppressed the reducing of the relative water content of leaf in turfgrass , delaying the time of wither , stress for the 11th day in the drought .compared with water normally and not using silicon ,after use silicon, the RWC of Bermudagrass , Agrostis Lolium. Pereme only separately depressed 14%,16%,32%; Under the drought condition ,the use of silicon can increased the content of proline of Bermudagrass ,Agrostis Lolium. Pereme, stress for the 11th day in the drought and using silicon , compared with water normally and ueing silicon, the content of Pro separately increased 203%,199%,473%;The using of silicon depressing the ET of Bermudagrass and Lolium. Pereme.Under water normally condition, separately depressed 21%,8% at eleven days ;Under drought condition , separately depressed 17%,5%.

施硅增加了草坪草狗牙根、剪股颖和黑麦草的含硅量，分别为209％、295％、285％；积累量分别提高了240％、364％、355％；施硅对草坪草狗牙根、剪股颖和黑麦草的干物质积累有促进趋势；在干旱的条件下，施硅抑制了草坪草的叶相对含水量的降低，延迟了叶片萎焉的时间，在干旱胁华中农业大学2001级时一艳丽硕士学位论文迫第n天，与正CK相比，施硅后狗牙根、剪股颖和黑麦草分别只降低了 14%；16%，32%。；施硅增加了狗牙根、剪股颖、黑麦草在干旱条件下脯氨酸的含量，增强了渗透调节能力，在干旱施硅的条件下，与正51相比，在干旱胁迫第11天，狗牙根、剪股颖和黑麦草脯氨酸的含量分别增加了2叨%、199%、473%；施硅减少了狗牙根和黑麦草的蒸散量在正常浇水的条件下，与正CK相比，第11天狗牙根和黑麦草的蒸散量分别降低了21%、吕%；在干旱的条件下，与干CK相比，在干旱胁迫的第11天，狗牙根和黑麦草的蒸散量分别降低了17%、5%。

Secondly, the pulse discharge plasma with allylamine was discussed, and the modification results with two kinds of discharge models were compared. The results showed that discharge models had influences on the plasma treatment results, especially under lower pressure and higher temperature with pulse discharge. The nitrogen element content in the layer under the pulse discharge was obviously lower than that under the continuous discharge, but there was higher proportion NH〓 groups remaining in the layer under the pulse discharge. The sample surfaces obtained by pulse discharge also had good biocompatibility.

其次讨论了脉冲放电模式下丙烯胺单体的等离子体修饰，比较了两种放电模式对修饰结果的影响，研究结果显示，放电模式对表面修饰层的结果有一定的影响，其中脉冲放电对低压及高温两等离子体条件下的影响尤为明显；脉冲放电下所得到的修饰层中的氮元素含量明显低于连续放电模式下，而脉冲放电下有较高比例NH〓基团保留在修饰层中；脉冲放电所得到的表面修饰层同样有较好的生物相容性。

Similarly, if the strong shear, which could suppress all the scattering in the quiescent two phase region, stopped, the follow-up phase separation also displayed characteristics of anisotropism and relaxation, In this dissertation, the transposed"butterfly'and"streakpattern were observed for the first time within the shear-history-influenced phase separation, which is found closely relevant to the anisotropical relaxation behavior of macromolecules. 5. The phase separation kinetics of PS/PVME under oscillatory shear was further studied on the base of that done under simple shear. It is found that, under specific temperature and strain amplitude, the occurrence of phase separation is strongly contingent on oscillatory frequency and only intermediate frequency could effectively induce phase separation; If all considered oscillatory shear could stimulate phase separation, a fixed frequency can maintain specific most probable phase size and higher frequency yields smaller phase, which makes a higher elasticity but weaker stress relaxation; Furthermore, higher frequency can produces stronger compulsory oscillation on the MPPS but won't change the mean of the MPPS. Under given frequency and strain amplitude, the phase separation kinetics dramatically depends on the phase angle of oscillation and the phase separation corresponding to different phase angle follows different dynamical process.

在简单剪切场下相分离动力学研究的基础上进一步对振动剪切场下PS／PVME的相分离动力力学进行了尝试性的研究，发现：在一定温度和振幅条件下，相分离的发生强烈的依赖于振动频率，只有中等频率的振动剪切才能有效地促进相分离的发生；在都能使相分离发生的前提下，一定频率的剪切能够使体系维持一定的最可几相尺寸，较高频率的剪切导致体系形成的相区尺寸较小，因而体系的弹性效应较强而应力松弛效应较弱；同时，更高频率的剪切对最可几相尺寸的强迫振动效应越强，但不会使最可几相尺寸的平均值发生改变；在一定的振幅和频率条件下，相分离的动力学过程会强烈地依赖于相位角，不同相位角对应的相分离遵循不同的动力学过程但机理一样。

Methods: Fifty-six cases of cholelith in residual gallbladder after cholecystectomy were analysed retrospectively. Among them, 18 patients under went conventional cholecystectomy, 16 patients underwent mini-lap cholecystectomy, 22 patients underwent laparoscopic cholecystectomy; 30 patients under went emergency operation and 26 patients under went selective operation; 42 patients' first operation was performed by under grade three hospital and 14 patients were performed by up gradethree hospital.

对56例残余胆囊结石再次手术的病例进行回顾性分析。56例中初次手术行经典胆囊切除术18例，小切口胆囊切除术16例，腹腔镜胆囊切除术22例；急诊手术30例，择期手术26例；初次手术在三级以下医院施行42例，在三级以上医院施行14例。

The accumulated contributions of main effect QTLs for AC and PC were 35.34%, 37.33% under normal conditions and 53.40%, 58.10% under water stress condition, and the accumulated contribution of digenic epistasis for AC and PC were 66.74%, 57.49% under normal conditions and 48.65%, 36.59% under water stress conditions, respectively.

主效QTL对直链淀粉和蛋白质含量的联合贡献率在非胁迫条件下为35.34%和37.33%，在胁迫条件下分别为53.40%和58.10%；互作位点对直链淀粉和蛋白质含量的联合贡献率在正常水分条件下分别为66.74%和57.49%，在胁迫条件下分别为48.65%和36.59%。

How to ensure this new structure to be in elastic state under frequent earthqu ake, be mendable under design earthquake and not collapse under infrequent earthquake, especially the last item, is the problem to be solved imminently in engineering field. Center around this problem, 5 aspects of investigation are carried out as following:(1) The experiment of seismic performance of ASCCs in this new frame structure has not been reported, in order to study this problem, 9 ASCC specimens with shear steel plate are tested subjected to the horizontal low cyclic loading, in which, the shear span ratio is 3 and axial compression ratio is different. The hysteretic curves of 9 specimens are obtained. The seismic performance indexes such as energy dissipation, stiffness degradation, strength degradation, skeleton curves and ductility of this kind of column are acquired, and the seismic fortification measures including ultimate values of axial compression ratio under different seismic degree are suggested.

1新型框架结构中所采用的角钢混凝土柱抗震性能的试验研究尚未见报道，针对这一问题，本文进行了9根剪跨比为3、不同轴压比、采用钢板箍的角钢混凝土柱在水平低周反复荷载作用下的试验研究，获得了9根试验柱的滞回曲线，考察了该类柱的耗能、刚度退化、抗力衰减、骨架曲线及延性等抗震性能指标，建议了角钢混凝土柱在不同抗震等级下的轴压比限值等抗震构造措施。

Wenxing consistently adheres to the principle of "trict Management,All Member Participation,Quality First,Users Foremost" and follows the business philosophy of excellent quality,highly active and pursue excellence,thus outdoing its counterparts in terms of technology,production scale and administration.

文兴一贯秉承&严格管理、全员参与、质量第一、用户至上&的企业方针，遵循优质、高效和追求卓越的经营理念，从而实现在技术上、规模上、管理上处于同行领先地位。

The left atrium of the guinea pigs was innervated by the two afferent system.

豚鼠左心房受心脏的两个传入系统的双重支配。