查询词典 trinitro-toluene

The optimum reaction conditions were that the molar ratio of maleic anhydride and p-nitroaniline was 1.2:1, the volume ratio of toluene and DMF was 10:1, the amination temperature was 20~30℃ the cyclization temperature was 145~150℃ and the cyclization time was 6 h over; the amount of p-toluene sulfonic acid was 12% of total reactant mass, the amount of copper sulfate was 0.1~0.5% of total reactant mass, the amount of hydroquinol was 0.1% of total reactant mass.

得到的最佳工艺条件是：n：n为1.2：1，V：V为10：1；胺化反应温度为20~30℃，环化反应温度为140~150℃，环化反应时间为6h以上；对甲基苯磺酸用量为反应物总质量的1%~2%；硫酸铜用量为反应物总质量的0.1%~0.5%；对苯二酚用量为反应物总质量的0.1%。

Results indicate that the severity of a loss of control for mononitration of toluene by mixed acid can be reduced from medium to low by using semi-batch reactor, the reaction is 1.2 kinetic order in toluene, 1.3 order in nitric acid and 2.5 order in all. The MTSR_max under setting operating conditions are all in the range that can be accepted by the industrial nitration, so the reaction has less hazard potential by using those setting conditions.

分析结果表明：在设定的工艺条件下，反应过程中对甲苯的反应级数是1.2级反应，对硝酸是1.3级反应，采用半间歇反应可以使失控反应的严重度等级从中等降低到低等，在设定操作条件下假定反应失控所引发的MTSR_是在工艺条件允许的范围之内，不具有很大的危险性。

O-MNT、 p-MNT and m-MNT are got by mononitrating toluene, and the quantity of p-MNT and m-MNT that are needed is increased greatly, there is a great economic benefit to improve their ratioes , so the objective of this study is to improve the ratioes of p-MNT and m-MNT in the mononitration of toluene respectively through changing temperature and mixed acid composition in industrial way.

甲苯一硝化生成邻硝基甲苯、对硝基甲苯、间硝基甲苯，其中对硝基甲苯和间硝基甲苯的用量明显增加，提高它们在产物中比例的研究，具有十分可观的经济价值，所以本文从工业化的角度出发，通过改变温度和硝硫混酸的组成，分别对提高一硝基甲苯中对、间位异构体的比例进行研究。

To assess the thermal contribution from oxidation reaction, the standard formation enthalpes of all reactants and products were used to calculate the oxidation enthalpies. It could be found that all oxidation reactions were exothermic. And oxidation played a more important role during the toluene trinitration at high temperature, because the reaction temperature of toluene trinitration is the higher than mononitration and dinitration, and the temperature coefficient of oxidation is higher than that of trinitration too.

为了考察不同阶段氧化副反应对反应放热的贡献，用反应物和产物的标准生成焓推得氧化反应的理论反应热，计算结果表明，各段硝化的氧化副反应均为放热反应，其中三段硝化反应由于反应温度最高，氧化反应的温度系数比硝化反应高，故氧化副反应对三段硝化影响最大。

The paper introduced three processes to prepare isochroman from β-phenethyl alcohol and polyformaldehyde:HCl catalysis,AlCl_3 catalysis and toluene-p-sulfonic acid catalysis,and discussed its reaction mechanism,using toluene-p-sulfonic acid catalysis method to prepare isochroman ,the yield is 46%,purity is 96%.

用β-苯乙醇和多聚甲醛为原料，进行了HC l催化法，三氯化铝催化法和对甲苯磺酸催化法的合成路线的实验，并对其反应机理进行了探讨，应用对甲苯磺酸催化法合成异色满的合成路线，得率46%，纯度96%。

Waste oil category: Waste oil, waste hydraulic oil, waste oil, waste oil injection, waste kerosene, waste of white mineral oil, white waste oil, waste oil sparks, the repeal of toluene, waste cutting oil, gear oil, lubricants, batteries oil, spindle oil, zorra, oil, turpentine oil, solvent oil, gear oil, oil rails; waste chemical categories: one, the repeal of toluene, xylene waste, spent 2 pure benzene, acetone waste, waste Ding ketone, cyclohexanone 3 waste, waste dichloromethane, dichloroethane waste, waste Dichloropropane 4, solvent categories: soluble oil 6 #, 120 # dissolving agents, dissolving agents 200 # 5, trichloro ethylene, dichloromethane, trichloroethane; tetrachlorethylene, trichloromethane 6, the repeal of methanol, ethanol, waste, waste alcohol, isopropyl alcohol waste 7, the repeal of ethylene glycol, diethylene glycol waste, spent three 8 glycol, waste butyl acetate, ethyl acetate wastewater, waste acetate 9, the repeal of ethyl ether, acetonitrile waste, waste petroleum ether 10, cleaning categories: cleaning agent, washing machine water, days that water; wash board water,×oil wastewater liquid 11, the supply of tires category: special supply of fuel oil, non-standard oil, burner oil, waste oil and other refined crude oil.

废油类：废机油，废液压油，废柴油，废注塑机油，废煤油，废白矿油，废白电油，废火花机油，废甲苯，废切削油，齿轮油，润滑油，废电池机油，锭子油，索拉油，松节油，溶剂油，齿轮油，导轨油等；废化工类：1、废甲苯、废二甲苯、废纯苯2、废丙酮、废丁酮、废环已酮3、废二氯甲烷、废二氯乙烷、废二氯丙烷4、溶剂类： 6#溶油剂， 120#溶油剂， 200#溶油剂5、三氯乙烯，二氯甲烷，三氯乙烷；四氯乙烯，三氯甲烷6、废甲醇、废乙醇、废丁醇、废异丙醇7、废乙二醇、废二甘醇、废三甘醇8、废醋酸丁酯、废醋酸乙酯、废醋酸甲酯9、废乙醚、废乙腈、废石油醚10、清洗类：清洗剂，洗机水，天那水；洗板水，去渍油等废液废水11、废轮胎类供应：特价供应燃料油，非标油，烧火油，废油提练的原油等。

Results The mixing, loading and storing processes of the construction, might generate lots of occupational hazards, including toluene, dimethylbenzene, trimethylbenzene, isopropanol, butyl alcohol, propanol, methyl methacrylate, butyl acetate, methyl isobutyl ketone, methyl ethyl ketone, acetic ether, nitro-cotton, n-hexane, n-heptane, carbinol, ethanol, ethyl propionate, diisobutyl ketone, glycol ether, isoamyl acetate, 2,4-toluene diisocyanate, isophorone, noise, power frequency electric fields.

结果 该项目在混兑生产和装卸、仓储过程中，可能产生的职业病危害因素主要有甲苯、二甲苯、三甲苯、异丙醇、丁醇、丙醇、甲基丙烯酸甲酯、乙酸丁酯、甲基异丁基甲酮、丁酮、乙酸乙酯、硝化棉、正己烷、正庚烷、甲醇、乙醇、乙酸丙酯、二异丁基甲酮、乙二醇乙醚、乙酸异戊酯、2，4甲苯二异氰酸酯、异佛尔酮、噪声、工频电场。

Catalytic degradation of polystyrene in supercritical toluene and n-hexane using barium oxide were carried out. The results show that toluene is better.

本文以氧化钡为催化剂分别在超临界甲苯和超临界正己烷中考察了聚苯乙烯的降解过程，结果表明超临界甲苯的效果优于超临界正己烷。

Dissolve the residue in 8 ml of toluene R. Filter through a membrane filter (45 μm), rinse the flask and the filter with toluene R and dilute to 10.0 ml with the same solvent.

残留物用8ml甲苯溶解，并用滤膜（45um）过滤，用甲苯冲洗蒸发瓶和过滤器，并稀释到10ml

The residue is then cooled and acidified with dilute hydrochloric acid. The toluene layer is separated off, washed with water and distilled. Toluene and other low-boiling fractions first distil over and finally pure diethyl phenylmalonate is obtained boiling at 165-166°C, under 20 mm. pressure and having m.p. 16 °C. The yield is 85% of the theoretical.

剩余物冷却然后用稀盐酸酸化，分理出甲苯层，用水洗涤，然后蒸馏，甲苯和其他低沸点馏分先被蒸馏出来，最后获得20毫米压力下沸点为165-166摄氏度的二乙基苯基丙二酸酯，其熔点为16摄氏度，理论收率为85%。

A small, rubber-headed hammer used in examination or diagnosis by percussion.

叩诊槌用在通过''。'振荡'。''所作的检查或诊断中的橡皮头的''。'小'。''槌

Affixes are limited in number in a language, and are generally classified into three subtypes, namely, prefix, suffix, and infix, depending on their position with reference to the root or stem of the word.

语言中词缀的数量总是有限的，根据它们跟词根或词干的相对位置，一般可以把词缀分外三小类：前缀，后缀和中缀。