查询词典 triethylamine

Silicoaluminophosphate (SAPO–5) molecular sieves were synthesized by the hydrothermal method, using metakaolin with a certain degree of activity as the silicon and aluminum sources, phosphoric acid as the phosphorus source and triethylamine com- bined with hydrofluoric acid as the template agents.

以具有一定活性的偏高岭土兼作铝源与硅源、正磷酸作磷源、三乙胺和氢氟酸为复合模板剂，用水热方法合成了磷酸硅铝分子筛(SAPO–5)。

The dehydration of sulphonyl derivatives of N-alkylformamide using phosphorus oxychloride in the presence of triethylamine at 0-10℃ provides a useful method for the preparation on sulphonylmethyl isocyanides e.g.

光气同三乙胺或是嘧啶是一组有效的制取异氰基化合物的试剂，但是，由于光气在安全性方面的问题它不适宜在大规模上制取异氰基化合物。

Therefore, the goal ofour work is to synthesize new microporous titanosilicates. A new titanosilicate with a high Si/Al molar ratio (named JLU-3, JilinUniversity No.3), has been synthesized hydrothermally by using Triethylamine astemplate in the SiO2-NaOH-TiO2 system.

鉴于含钛硅微孔材料多具有优良的氧化催化性能，其合成和性能研究一直为国际上的热点，我们把新型钛硅微孔材料开发作为研究方向。

In application of modified phenol-formaldehyde resin in OCC pulp, firstly the application effictiveness of phenol-formaldehyde resin modified by triethylamine and diethylene triamine in OCC pulp was researched, and the optimum application effictiveness was gotten through mon- factor trial.

通过对改性酚醛树脂在OCC废纸浆中的应用研究，考察了二乙烯三胺和三乙胺改性酚醛树脂在OCC废纸浆中的应用效果，并通过单因素实验得到了改性酚醛树脂的最佳应用效果。

The thermal property studies indicate that the mass loss of compound B was 54.39% at 242.2~750℃, and when the temperature was 1000℃, there was 25.11% char residue left, which showed that the title compound has a good thermal stability and char forming capability. Using acetonitrile as the solvent instead of trichloromethane or 1, 2-dichloethane gave higher yield. During the synthesis, the yield was very low when triethylamine was used as acid acceptor alone, and when a little amount of 4-dimethylaminopyridine was added at the same time, the yield could be 81%.

结果表明，所合成的化合物B的结构与预期的结构一致；热性能研究表明，化合物B在242.2~750℃质量损失为54.39%，1000℃时仍有25.11%的炭残渣，显示出优异的热稳定性和成炭性；在相同反应条件下，用乙腈作为溶剂的反应产率比使用氯仿和二氯乙烷为溶剂的高，并且在合成过程中，单独使用三乙胺作为缚酸剂时产率很低，而当同时加入少量4-二甲氨基吡啶时，产率可达81%。

Epoxypropyl triethyl ammonium chloride intermediate was synthesized by the reaction of triethylamine with epichlorohydrin in aqueous methanol using K_2SO_4 as catalyst.

首次将硫酸钾作为催化剂，引入到环氧丙基三乙基氯化铵中间体的合成反应中。

Epoxypropyl triethyl ammonium chloride intermediate was synthesized by the reaction of triethylamine with epichlorohydrin in aqueous methanol using K_2SO_4 as catalyst.

以环氧氯丙烷的转化率和产物中环氧基保留率的乘积作为中间体性能的评价指标，通过正交实验优化出最佳条件：甲醇水溶液为溶剂，反应温度50℃、n∶n=0.010、n∶n=1.0、反应时间为1.5 h。

A series of UV curable waterborne hyperbranched polyester s with different acid/amine terminal rate,which contained -OH?-COOH and methacrylic chain end groups,and were partly neutralized with thertiary amine,were synthesized from trimellitic anhydride,epichlorohydrin,glycidyl methacrylate and triethylamine.

以偏苯三酸酐、环氧氯丙烷、甲基丙烯酸缩水甘油酯、三乙胺合成了末端羧基与氨基不同比例的一系列可UV固化的高支化聚酯，研究了末端官能团对合成产物水溶性、粘度以及凝胶转化率的影响。

Methods The internal standard was diazepam, the samples were extracted by ethyl acetate after basified the plasma., the column was Hypersil C18, and the mobile phase mixed of methanol: water(75:25) containing 0.03%-triethylamine.

色谱柱为Hypersil ODS C18 4.0mm×250mm，流动相为含0.03%三乙胺的甲醇：水（75：25），流速1.0ml/min，紫外276nm波长检测。

In the third step, when the ratio of racemic ester to benzenesulfonyl chloride to triethylamine to catalyst 4-DMAP is 1:1:1:0.1 in 10℃, the yield is 82.9% and high purity is obtained by crystallisation.

在第三步磺酰化反应中，得到合成消旋2-苯磺酸基-2(2-氯苯基)乙酸甲酯的较佳反应条件为邻氯扁桃酸甲酯：苯磺酰氯：三乙胺=1：1：1，催化剂4-DMAP用量为摩尔反应物的10%，反应温度为10℃，收率为82.9%，同时用结晶方法获得高纯度的产物。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。