查询词典 time-temperature curve

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现；3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布；4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒；5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明：1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致；2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响；3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明，MAO不仅仅只和乙醇作用，MAO还与MgCl_2本身有一定的作用，这是一个极为重要的发现； 3、通过ICP和EDX表征，发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布； 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能，特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化，并且催化剂寿命长，表现出稳定的动力学行为，最终获得了高堆密度(大于0.35g／ml)的球形聚乙烯颗粒； 5、本文选择MSPC-5为研究对象，考察了聚合反应参数对催化剂的活性及其聚合物的影响，研究发现：不同的烷基铝对催化剂具有非常重要的影响，特别足TIBA对MSPC-5的助催化活性最高，烷基铝的加入量有一个较佳值，聚合温度为80度时活性最高，H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小；、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨，制备出了一种的新型的氯化镁载体，并将该载体用于多种单活性中心催化剂的负载化研究，研究表明： 1、通过BET、XRD的表征，再次证实了MAO与MgCl_2之间具有直接作用，与XPS的研究结果相一致； 2、当研磨时间高于12小时时，延长研磨时间对载体的结构没有显著的影响； 3、将配合物3负载于共研磨时间不同的一系列载体上，乙烯聚合结果表明，尽管共研磨时间对负载催化剂的活性具有明显的影响，但是它对聚合物的性能以及催化剂的影响不明显。

Extreme climate elements such as torrential rain, extreme high temperature, extremely low temperature and so on are always used to analyze and evaluate an extreme climate event. There was a continuous sleeting and freezing process with low-temperature in the beginning of 2008. The process had the characteristics of large and sustained precipitation and snowfall, deep and long-time snow accumulation, long time in daily low-temperature with not so-low extreme low temperature. Therefore, it wasn't objective and accurate to choose any single one of these elements to analyze and evaluate this process.

评估极端气候事件，往往用某一项极端气候要素进行分析评估，如暴雨量、极端最高气温等。2008年初出现的持续低温雨雪冰冻过程，具有雨雪量大、持续雨雪时间长、积雪深、积雪时间长、低温持续时间长、但极端最低气温不低的特点，用其中任一因子评估定位该过程，都不能全面反映该过程的综合影响特征。

Based on Bezier curve continuance of first－order and second－order derivative, the characteristic vector equation of two Bezier curve is presented in point of intersection. The algorithm is not only of high accuracy with all of the interpolated points being on the curve theoretically, but also of very high speed in the real－time interpolation processes. The interpolation velocity does not change and the segment tolerance of interpolation can be control by selecting the parameter in cerement rationally every time.

为保证两段Bezier曲线在连接点处一阶导数、二阶导数连续，导出了两段Bezier曲线特征向量应满足的关系方程，Bezier插补法不仅在理论上可使所有的插补点落在曲线上，而且实时插曲补速度高，每次插补时可合理地选择参数增量，能使插补速度保证不变，也可控制弓高误差。

The composite film appeared semitransparent and brown to yellow from optical microscopy. Results show that shorter time sol-heating results in thiner film with less surface roughness, less conglutination to base, and easily to disconnect, while longer time sol-heating results in thicker film with better conglutination to base and worse roughness. RDX distributes in the film everywhere on the whole but discretely on the scale of 2.4 μm according to EDS results. XRD curve of RDX/RF film shows the superposition of RF non-crystal bread curve and RDX crystals diffraction curve. RDX diffraction peaks are broadened and its crystal size is calculated to be lower to 43 nm.

实验所得薄膜半透明，呈棕红色至黄色；实验表明，溶胶恒温加热时间较短时，所得薄膜的单层厚度较小，较平整，但附着力小，干燥后易脱落；恒温加热时间较长时，所得薄膜的单层厚度较大，不易脱落，但表面平整性较差；能谱测试表明，薄膜中的RDX整体上分布较为均匀，但在测试点位间距为2.4μm的微观尺度上呈离散状分布；XRD测试表明，RDX/RF复合物薄膜表现为RF的非晶态馒头峰与RDX衍射峰的叠加，RDX衍射峰明显宽化，其晶粒度可低至43 nm。

The maxima of low-temperature internal friction peaks plot a symmetrical peak-like curve at logarithmic frequency spectrum and the peak-like curve shifts toward high frequencies with the increase of heating rate, indicating that phase transition relaxation time decreases; the maxima of high-temperature internal friction peaks exhibit a linear relation to the reciprocal frequencies, and as the heating rate increases its slope rises, which implies that the heating rate drives the normal movement of phase interface further in low-frequency measurements.

低温内耗峰峰值与对数频率呈现峰形函数关系，随升温速率的增加，频率峰向高频方向移动，相变弛豫时间减小；高温内耗峰峰值与倒数频率成直线关系，随升温速率的增加，直线斜率变大，表明低频测量时升温速率对相界面法向运动的驱动作用更强。

Each of the elevated temperature curves is moved along the horizontal time axis to longer times until it superposes on the reference temperature curve as smoothly as possible and then the master creep curve is obtained.

沿时间轴水平移动非参考温度下的蠕变曲线段使之与参考温度下的曲线图光滑连接，形成一条光滑的主曲线图。

Both the objective temperature curve and the practical temperature curve can be displayed on the CRT at the same time.

目标温度曲线与实际温度曲线能同时显示在屏幕上。

Equipped with AT89C51,the temperature sensor and the modulus convertor and coordinated by soft and hard wares,the system can fufil the instantaneous gathering of multichannel temperature signal,then,by meaus of asynchronous string communication,send the digital signal to PC which can separately display the instantaneous value and the average value of each channel temperature in bar diagram and weblike form,and print the temperature curve graph through data scale transferring,analyzing,and collating.

该系统运用单片机AT89C51、温度传感器保温器及模数转换器，通过软硬件的配合，实现了多路温度信号的实时采集，用异步串行通信发送数字信号到PC机，PC机经过数据的标度转换、分析、整理，分别用棒状图和网状表格显示各路温度瞬时值和平均值，打印出静态降温调温曲线图。

It is found that the resistivity increases linearly with temperature rising in certain range of temperature above the melting point. During subsequent calefaction, the results obviously show that a turn point appears in the resistivity-temperature curve for every composition at certain temperature.

发现在液相线以上一定的温度范围内，其电阻率随温度的升高而线性增加，即其电阻率温度系数α基本保持不变；当温度超过某一临界温度时，α随温度的升高出现异常变化。

Researches reveal that students who suffer from corporal punishment tend to resort to violence in their future life.

研究表明遭受过肉体惩罚的孩子倾向于在他们今后的人生中使用暴力。

Total sugar of sarcocarp and chlorophyll of pericarp increased firstly, and then decreased afterward along with altitude; Titratable acidity, ascorbicacid and anthocyanin of pericarp were increased along with altitude; The content of protein increased firstly and decreased afterward along with altitude; Carotenoid of pericarp were decreased along with altitude.

果肉总糖和果皮叶绿素含量随海拔高度升高先升高后降低；可滴定酸、维生素C和果皮花青苷含量均随海拔升高而升高；蛋白质在1720m处最大，1420m处最小；果皮类胡萝卜素随海拔升高而降低。