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Finally, the cytotoxic and antibacterial activities of the oxamido-bridged binuclear complexes were studied in vitro.. This dissertation consists of three sections as follows:1. The crystal structure of a oxamide dinitrate,(1) [H_4dmaeoxd](NO_3)_2 H_2dmaeoxd = N,N\'-bis[2-ethyloxamide, has been obtained. The diversity of complexes with different structures is carried out by successful synthetic strategy of controlling species of metal ions, counter anions, pH values and solvents in the course of synthesis. Four dinuclear complexes bridged by trans-dmaeoxd2-: [Cu_2_2](ClO_4)_2 (2), [Cu_2_2](ClO_4)_2 (3),、[Cu_2(Me_2phen)_2](ClO_4)_2 (4), [Cu_2_2(H_2O)_2] (5); Four dinuclear complexes bridged by cis-dmaeoxd2-: [NiNi_2](ClO_4)_2 (6), [CuNi_2](ClO_4)_2·2CH_3OH (7), [CuZn_2]-(ClO_4)_2·2H_2O (8), [Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9); three 1-D polynuclear complexes: [Cu_2]_n·nH_2O (10), [Cu_2(H_2O)_2-]_n·4nH_2O (11), [Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12); one 2-D polynuclear complex,[Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n).2nH_2O (13); the others: [VO(H_2O)]·2H_2O (14), [Zn_2_4](ClO_4)_2·H_2O (15), [Cu_2]·2DCM (16) have been synthesized and characterized by X-ray single crystal diffraction, elemental analysis, IR spectra.

本论文主要包括以下三部分：一、合成得到了一个草酰胺配体硝酸盐的单晶结构，[H_4dmaeoxd](NO_3)_2 (1)；通过调控金属离子的种类、端基配体、抗衡阴离子、溶剂、pH值等条件定向合成了四个反式草酰胺桥联双核铜配合物：[Cu_2_2](ClO_4)_2 (2)、[Cu_2_2](ClO_4)_2 (3)、、[Cu_2(Me_2phen)_2](ClO_4)_2 (4)、[Cu_2_2(H_2O)_2] (5)；四个顺式草酰胺桥联同/异双核配合物：[NiNi_2](ClO_4)_2 (6)、[CuNi_2](ClO_4)_2·2CH_3OH (7)、[CuZn_2]-(ClO_4)_2·2H_2O (8)、[Cu(H_2O)Ni_2](ClO_4)_2.0.5CH_3OH (9)；三个一维聚合物： [Cu_2]_n·nH_2O (10)、[Cu_2(H_2O)_2-]_n·4nH_2O (11)、[Cu_2(H_2O)]_n(NO_3)_n·2nH_2O (12)；一个二维聚合物： [Cu_6_3(μ_3-OH)_2(H_2O)_2]_n(ClO_4)_(4n)。2nH_2O (13)；单核钒配合物[VO(H_2O)]·2H_2O (14)、草酸根桥联双核锌配合物[Zn_2_4](ClO_4)_2·H_2O (15)、美洛西康铜配合物[Cu_2]·2DCM (16)，利用元素分析、摩尔电导、红外光谱、电子光谱和单晶X-射线衍射对上述所得化合物进行了结构表征，探讨了结构影响因素，并研究了其超分子结构。

Based on the distribution of the genera in the world,the eight distribution types of the genera were divided.In addition,the distribution characters of the Perlidae in China were also probed preliminarily.So far two subfamilies,four tribe and twenty genera have been found in China.Ten of them,of which three genera are endemic to China,are the Oriental genera;one Palaearctic genus;three Oriental-Palaearctic genera;one Oriental-Nearctic genus;four Oriental-Palaearctic-Nearctic genera and one Oriental-Palaearctic-Nearctic-Afrotropical genus.

文中还就中国郋科昆虫的地理分布及特点作了初步的探讨，结果表明：在我国已知的2亚科4族20个属中，东洋区分布的有10个属，其中有3个属仅分布于我国；古北区分布的有1个属；东洋-古北区分布的有3个属；东洋-新北区分布的有1个属；东洋-古北-新北区分布的有4个属；东洋-古北-新北-非洲区分布的有1个属。

Four thin-layer drying models were investigated for the description of FIR-assisted freeze-drying characteristics. The models were exponential model, Page model, diffusion model, and approximation of the diffusion model. Tests were conducted using a three-level, three-factor (drying temperature, distance between sample and FIR heater, and sample thickness) design, and quadratic polynomial analyses were performed to relate the drying parameters of thin-layer drying model. The performance of these thin-layer drying models was evaluated by comparing the coefficient of correlation (R2), the sum of squares, and the RMSE amongst four models. Drying parameter K of the Page model gave the best results in describing freeze-drying with FIR of Tylose and sweet potato.

运用四种薄层乾燥模型（指数、Page、渗透模型及近似渗透模型）研究远红外线冷冻乾燥之乾燥特性，实验采用三阶层、三因子（远红外线加热器设定温度、远红外线加热器至样品表面之距离及样品之厚度）的实验设计，对於薄层乾燥模型的乾燥参数以二次多项式函数表示之，乾燥参数之二次多项式函数的最适性判断主要是藉由决定系数、模式缺乏适合性及均方根误差等值的比较而加以评估，以Tylose及甘薯样品而言，其中四种薄层乾燥模型的乾燥参数以Page模型之K值的结果为最佳。

It was isolated from the mosquito stomach HIV, found that absorption of the mosquito's blood after AIDS patients, HIV can survive in the mosquito stomach three to four days, but the amount of virus in mosquitoes can cause the number of HIV transmission is not clear, and the mosquitoes In a suction blood, at least three to four days no longer vampire bites, and some died soon; Some people also said: mosquitoes but the remnants of blood containing HIV will be transmitted to humans.

有人从蚊子胃内分离出HIV，发现蚊子吸了艾滋病病人的血之后，HIV可在蚊子胃内存活3~4天，但蚊子体内带毒量的多少才可引起HIV传播尚不清楚，而蚊子在吸一次血之后，至少3~4天不再叮咬吸血，有的很快死去了；又有人说：蚊子嘴上残留的血液含有HIV会传染给人。

The following is the research frame of this dissertation:Chapter one: Introduce background, research significance, research object, research contents and methods of this dissertation; review the history of clusters theoretical research in detail; dissertate main research dynamic status of domestic and international;Chapter two: Through explain theoretical foundation of cluster research, it defines and demarcates clusters, introduces the concept of private enterprises" cluster on this basis, and summarizes current situation of Quanzhou private enterprises" cluster;Chapter three: Propose the concept of cluster competitiveness, collect and analysis those factors which influence cluster competitiveness, and set up an appraisal system of private enterprises" cluster competitiveness;Chapter four: Define developing stages of private enterprises" cluster with clusters" dominance competitiveness, analysis characteristic and law of private enterprises" cluster in different life cycle, give out strategic countermeasures separately which promote cluster competitiveness in different stage;Chapter five: On the basis chapter three and chapter four, propose what we can use cluster strategic planning to promote Quanzhou cluster competitiveness; and recommend thought of cluster strategic planning;Chapter six: Introduce the case of Quanzhou sports shoes cluster, use competitiveness appraise system and life cycle theory for empirical analysis, and put forward detailed countermeasure that can promote cluster competitiveness;Conclusion: Summarize the research of full dissertation, and point out some weaknesses of this dissertation.

本文的研究框架如下：第一章：介绍本文选题的背景、研究意义、研究对象、内容与方法，并详细论述集群理论研究的历史回顾及当前国内外主要研究动态；第二章：通过阐述产业集群研究的理论基础，定义及界定产业集群，在此基础上引入民营企业产业集群的概念，并归纳总结了泉州市民营企业产业集群的现状；第三章：提出产业集群竞争力的概念，对影响集群竞争力的因素进行分析，初步建立一套民营企业产业集群竞争力的评价体系；第四章：应用集群显性竞争力来界定民营企业产业集群发展的生命周期阶段，并分析民营企业产业集群在各个不同生命周期阶段呈现的特征及规律，分别给出在不同阶段提升集群竞争力的战略对策；第五章：在第三、四章的基础上提出应用产业集群战略规划来提升泉州民营企业产业集群的竞争力，并介绍了集群战略规划的思路；第六章：引入泉州运动鞋产业集群的案例，应用本文构建的集群竞争力评价体系及生命周期理论进行实证分析，并提出提升该集群竞争力的详细对策；结论：总结全文的研究，并指出本论文研究的一些不足之处。

Three Die three-, four-mode four more power-cold heading machine, trimming production of 2.60, with 2.60, furniture screws, 11 words, the flat head, and so on non-standard products, welcomed the new and old customers calls来人negotiations.

三模三冲、四模四冲多功位冷镦机，生产外六角切边、内六角、家具螺丝、十一字、大扁头等等非标产品，欢迎新老客户来电来人洽谈。

Wenzhou Ou Hai Hong-machine factory was built in 1994, the factory specializing in the production of Z46-6, Z47-8 three-three-, four-mode four more power-cold heading machine.

温州市瓯海鸿通机械厂建于1994年，本厂专业生产Z46-6、Z47-8三模三冲、四模四冲多功位冷镦机。

Those who know Brahma's day which comprises the duration of four billion three hundred and twenty millions years and his night also the duration of four billion three hundred and twenty million years are knowers of day and night.

博拉玛的一天是地球上的四十三亿零两千万年，它的一夜也是这么长。懂得了这一点的人才知道什么是白天和黑夜。

Sowe selected the colchicine optimum parameters were 0.6μg/ml and 6 hour culturedduration.The second, there were no significantly differences between the four groupsin 2 hour groups; and there were significantly differences between 0.2μg/ml groups and other three groups in 4 hour groups; and there were no significantlydifferences between the four groups in 6 hour groups; and there were significantlydifferences between 0.4μg/ml groups and other three groups in 8 hour groups onthe metaphases (P＜0.05), in the experiment of the effect on the mouse 8-cellembryo stage single blastomere of colchicine with different concentrations andduration by x~2 statistical analysis.

根据实验的实际情况，适宜制备小鼠4-细胞期胚胎单卵裂球染色体标本的秋水仙素的处理浓度和时间是0.6μg／ml和6小时。2、在确定秋水仙素不同处理浓度和时间对小鼠8-细胞期胚胎单卵裂球中期分裂相数影响的实验中，经统计分析，阻断培养2小时组中四个浓度组差异均不显著；阻断培养4小时组中0.2μg／ml浓度组与其他三组差异显著；阻断培养6小时组中四个浓度组差异均不显著；阻断培养8小时组中0.4μg／ml浓度组与其他三组差异显著(P＜0.05)。

At last, according to three-microphone method, four-microphone with two different ends method and four-microphone method, this paper compare with this three methos from principle, formula and measuring ways.

最后，针对目前驻波管法的三传感器法、改变边界条件的四传感器法和四传感器法三种隔声量测量方法，从原理、计算公式的推导及测量方法等方面进行了比较。

The work of this paper is as follows: 1. Looking back the progressing history of the linear motor, introducing the features of the elevator driven by linear induction motor, radicating the topic of this paper "the digital frequency variable control of the elevator bi-side direct driven by linear induction motor". The research of this paper covers the conventional VVVF control, space vector based VVVF control, vector control and DTC.

本文主要开展了以下几个方面的工作： 1 回顾了直线电机发展历史，电机的驱动技术演变，特别是针对直线电机的驱动，简要介绍了直线感应电机驱动电梯的优点和不同结构类型，对传统的v／f控制，基于空间矢量法的v／f控制，矢量控制，和基于电压空间矢量的直接转矩控制进行了比较，确立了本课题的研究主题：直线感应电机双边直推式驱动电梯的全数字变频控制。

The article combines with the treatment of a superficial civil air defense work to introduce how the grouting method to improve the performance of the backfill soil.

文章从治理漂浮人防工事的角度提出了注浆技术在改善回填土性质方面的应用，并详细阐述了注浆技术的施工流程。