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Nine new compounds were characterized, and they were: opuntioside Ⅰ(11), 4-ethoxyl-6-hydroxymethyl-α-pyrone (14),--ester (22), 1-butoxyl--malate (24), ethyl α-L-rhamnopyranoside (26), opuntioside Ⅱ(34), kaempferol 7-O-β-D-glucopyranosyl (1→4)-β-D-glucopyranoside (46), methyl α-D-glucopyranoside-6-(methyl 4-malate)-ester (47), and opuntioside Ⅲ(48). Opuntioside Ⅰ,Ⅱ,Ⅲ and 4-ethoxyl-6-hydroxymethyl-α-pyrone belong to the skelecton of α-pyrone.

新化合物分别是:仙人掌苷Ⅰ(11),4-乙氧基-6-羟甲基-α-吡喃酮(14),琥珀酸乙酯--酯(22),L--苹果酸-1-丁酯(24),乙基α-L-吡喃鼠李糖苷(26),仙人掌苷Ⅱ(34),山奈酚7-O-β-D-吡喃葡萄糖基(1→4)-β-D-吡喃葡萄糖苷(46),α-D-吡喃葡萄糖甲苷-6-(苹果酸-4-甲酯)-酯(47),仙人掌苷Ⅲ(48),其中仙人掌苷Ⅰ、Ⅱ、Ⅲ及4-乙氧基-6-羟甲基-α-吡喃酮均为α-吡喃酮骨架类型的新化合物。

This is a picture of Maurice Druon, the Honorary Perpetual Secretary of L'Academie francaise — the French Academy. He is splendidly attired in his 68,000-dollar uniform, befitting the role of the French Academy as legislating the correct usage in French and perpetuating the language. The French Academy has two main tasks: it compiles a dictionary of official French — they're now working on their ninth edition, which they began in 1930, and they've reached the letter P. They also legislate on correct usage, such as the proper term for what the French call "email," which ought to be "courriel." The World Wide Web, the French are told, ought to be referred to as "la toile d'araignee mondiale"— the Global Spider Web — recommendations that the French gaily ignore.

这是莫理斯图翁他是L'Academie francaise的荣誉终身院士–或称法兰西学术院他身穿价值六万八千美元的华丽院士服与他在法兰西学院的职责十分相称他的工作是负责规范法文的正确用法并确保法文永垂不朽法兰西学术院肩负两项使命:编纂官方版的法文字典–现在正在编第九版他们从1930年就开始了,现在编到字母P 这些人也规范语言的正确用法例如,法国人常说的伊媚儿"email"应该叫做电子邮件"courriel"而网际网路"World Wide Web"应该要称为"la toile d'araignee mondiale"–全球蜘蛛网种种法国人兴高采烈地忽略的建议

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物,利用理化性质和波谱技术(UV、IR、EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构,分别为9种蒽醌类化合物:大黄酚,大黄素甲醚,大黄素,芦荟大黄素,大黄酸,番泻苷A或B,ω-羟基大黄素(ω-hydroxylemodin),大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside),芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside);3种菲醌类化合物:丹参酮ⅡA(tanshinoneⅡA),隐丹参酮,丹参酮Ⅰ(tanshinone Ⅰ);1种异黄酮:7,3'-二羟基-5'-甲氧基异黄酮(7,3'-dihydroxy-5' methoxyisofla-vone)以及原儿茶醛,原儿茶酸,黄芪甲苷(astragaloside Ⅳ),苦杏仁苷,2,3,5,4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷(2,3,5,4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside),Z—儿茶素,桂皮酸。

Result: Eight compounds were isolated and they were identified as β-sitosterol (1), succinic acid (2), luteolin-7-O-β-D-glucoside (3), uracil (4), apigenin (5), chrysoeriol (6), chrysoeriol-7-O-β-D-glucoside (7), and apigenin-7-O-β-D-glucoside (8). Conclusion: Compound 4-8 were isolated from L.

结果:从藏药短管兔耳草醋酸乙酯提取物中分离得到8个化合物,经鉴定分别为β-谷甾醇(1),琥珀酸(2),木樨草素-7-O-β-D-葡萄糖苷(3),尿嘧啶(4),芹菜素(5),柯伊利素(6),柯伊利素-7-O-β-D-葡萄糖苷(7)和芹菜素-7-O-β-D-葡萄糖苷(8)。

The results were as follows the change of vitamin C content was a "trial apex"-shape curve, higher in young fruit,incrustation and maturation stages, lower in other periods; the total acid content was the highest in young fruit, after that, it decreased rapidly, maintained lower level, and reached lowest when the fruit matured; the total content of soluble sugar inosculated with the fruit development, it was high when the fruit development was quick, and low when the fruit development was slow; before 59 d after anthesis, the reducing sugar content was high in the total content of soluble sugar and after that ,the nonreducing sugar content was high; before 45 d after anthesis, free amino acid content was obviously correlated with protein content, and they inosculated with the fruit development;4559 d after anthesis, free amino acid content increased quickly, and protein content decreased gradually, this was also the most shaping period of the embryo and endosperm.

结果表明,Vc含量呈&三峰&型曲线,幼果时、硬核后和成熟时较高,其他时期较低;有机酸含量以幼果期最高,以后迅速下降并维持较低水平,果实成熟时含量最低;可溶性总糖含量与果实发育状况基本相吻合,果实发育速度快时含量较高,慢时较低;在谢花后59 d以前,可溶性糖以还原糖为主,之后以非还原糖为主;游离氨基酸和蛋白质含量,在谢花后45 d以前两者呈高度相关,且与果实生长速度相吻合,谢花后4559 d是胚和胚乳的主要形成期,此期游离氨基酸含量迅速增加,蛋白质含量持续下降。西北林学院学报21卷第5期张传来等金光杏梅果实发育期间主要营养成分动态变化研究

The dynamic simulation test showed that, the removal rate of TN、 NH_3-N、TP of Oenanthe javanica floating-bed was positive correlated with water temperature. The average removal loading rate of TN and TP were 0.80g/m.~2·d and 0.11g/m~2·d, respectively. The inhibition on algae was steady and the average inhibition rate was 57.3%. We also got the best value of hydraulic loading rate, floating-bed coverage rate, water depth under dynamic polluted river. They were 1.0m~3/(m~2·d)、 30%、 30cm.

动态模拟试验表明:水芹菜浮床对动态污染河水中TN、NH_3-N、TP的去除率与水温正相关,TN的平均去除负荷为0.80g/m~2·d,TP的平均去除负荷为0.11g/m2~2·d,对藻类的抑制作用较为稳定,平均抑制率为57.3%;获得了对动态污染河水最佳净化效果时的水力负荷参数为1.0m~3/(m~2·d)、浮床覆盖率为30%、水深为30cm。

Good Rogue/Spriest teams target switch, so don't be surprised when they decide to leave you alone and run after your druid after he comes out to heal you, your druid should always be ready for the switch, when I play good double DPS teams I know if they go for me first and fail, the next game they will try going for my druid.

好的贼+暗牧能迅速地切换目标,所以他们丢下你转而去搞D的时候不要惊讶,你的D要时刻做好准备。在对优秀的双DPS组合时,如果他们从我开刀时失败了,下一次再碰上就会去打D的主意。

Currently has a class of calcium agents, such as amino acid calcium, Stachyose calcium, vitamin C calcium are among the elements of calcium, they can be absorbed by the body take the initiative and do not need the help of vitamin D, but it does not take elements of calcium Children do not need vitamin D, because the absorption of dietary calcium of vitamin D is still needed help.

目前有一类钙制剂,如氨基酸钙、苏糖酸钙、维生素C钙等都属于分子钙,它们可以被人体主动吸收,并不需要维生素D的帮助,但并不是说服用分子钙的孩子就不需要维生素D,因为食物中钙的吸收仍然需要维生素D的帮助。

Across joins 2 be: Both sides makes alternate connection, mutual promotion opposite party needs the keyword of promotion, if A B C D stands, a B station is my site, c D station is site of the other side, it is me above all with A the station puts join of station of C of the other side, the other side joins with D station my B stands, such quality that makes the A station that the condition is me asks like Pr and the condition of the D station of the other side is a balance, such we just make connection significant, simple for the rank that such purpose is the C station that we popularize him in side the other side, the other side is popularizing the rank that our B stands, be mutual benefit actually, a lot of had not become alternate connective friend, should turn to them a little only next turns, they are muddleheaded, it is a dot really so it is cerebrum begins god-given report, but the result that such doing is very fast, the result that compares direct trade is good, because search engine to like one-way link, such rank is collected what come is fast, most stationmaster feels to inquire inconvenience so, what such doing is easy let stationmaster consider as cheating join, because such inquiry is no-go, unlike straight contact joins into the other side the connection that can see he stands is checked easily, anyway aught has the one side of its advantages and disadvantages!

交叉连接二是:双方都做交叉连接,互相推广对方需要推广的关键词,如 A B C D 站,A B 站是我的站点, C D站是对方站点,首先是我用A站放对方C站连接,对方用D站连接我的B站,这样的做条件是我的A站的质量如pr要求和对方的D站的条件是平衡的,这样我们才做连接有意义了,简单来说这样的目的是我们在帮对方推广他的C站的排名,对方在推广我们的B站的排名,其实都是互利的,好多没有做过交叉连接的朋友,只要稍微给他们转下弯,他们就糊涂了,这样的确是点是大脑开始难得反映,但是这样做的效果很快,比直接交换的效果好,因为搜索引擎喜欢单向连接,这样的排名收录都来的快,大多数站长觉得这样查询不方便,这样做的容易让站长认为是在骗连接,因为这样的查询是不方便,不像直接点进对方连接能看见自己站的连接容易检查,反正任何事物都有它的利弊的一面吧!

He said: One of the things I always enjoyed about that separation between Blizzard and Blizzard North was that the Diablo games had a very distinct art style. They had different art directors, they had different people working on it, they had a different sensibility about them. Diablo was I think grittier and darker and a little more leaning towards the photo realistic.

对于暴雪和暴雪北方的&分居&,我最欣慰的一点是D系列的艺术风格更加独立。D和blz其他系列的游戏使用的艺术指导不同,工作人员不同,对游戏的感觉也不同。D在我心中,应该是更加粗犷,更加黑暗,更加倾向于真实画感。

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推荐网络例句

Lugalbanda was a god and shepherd king of Uruk where he was worshipped for over a thousand years.

Lugalbanda 是神和被崇拜了一千年多 Uruk古埃及喜克索王朝国王。

I am coming just now,' and went on perfuming himself with Hunut, then he came and sat.

我来只是现在,'歼灭战perfuming自己与胡努特,那麼,他来到和SAT 。

The shamrock is the symbol of Ireland and of St.

三叶草是爱尔兰和圣特里克节的标志同时它的寓意是带来幸运。3片心形叶子围绕着一根断茎,深绿色。