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Olivine LiFePO4 was synthesized by microwave heating and the reactions could be finished within few minutes.

使用了微波合成LiFePO4，在几分钟即可以完成反应。

Several transient compounds were synthesized by the homo- and heterogeneous reactions of reactive halogen compounds, In-situ ultraviolet photoelectron spectroscopy and photoionization mass spectroscopy as well as theoretical calculations were used to study their molecular structures, stability and molecular orbital properties, their electronic structures and geometric structures were obtained for the first time; Simultaneously, the electronic structure and thermal dissociation of acetyl peroxynitrate and trifluoroacetyl peroxynitrate which have great importance in the atmospheric chemistry were studied; The substituent effects of series of halopyridines and halothiophenes were studied by the ultraviolet photoelectron spectroscopy method for the first time. The atmospheric chemical reaction between peroxyacetyl radicals with IO radicals as well as the dissociation of the most stable isomer of CH3COIO3 were calculated by density functional theory, it was found that the CH3COOIO2 isomer may be act as a new reservoir of inorganic iodine in the stratosphere.

通过活性卤素的系列均相与非均相化学反应合成了几种瞬态物种，采用原位紫外光电子能谱和光电离质谱结合量子化学理论计算对化合物的分子结构、稳定性以及分子轨道特性进行了研究，首次获得了这些物种的电子结构和几何结构的信息；同时研究了大气中有重要作用的乙酰过氧硝酸酯和三氟乙酰过氧硝酸酯的电子结构性质及热解过程；采用紫外光电子能谱手段首次研究了系列卤代吡啶和噻吩的取代基效应；通过量子化学理论计算研究了乙酰基过氧自由基与IO自由基的大气化学反应及其最稳定异构体CH3COOIO2的解离，发现该物种可能是无机碘化合物在平流层中的储库物种。

In order to study its structure function relation, seven peptide segments and five analogues were designed and synthesized.

为进一步研究其结构与活性的关系，设计并合成了它的7个肽片段和5个类似物。

For the first time ,AgBr organosol was obtained by using oleic acid to extract and modify the AgBr nanoparticles in hydrosol. And the optimum molar ratio of oleic acid to AgBr nanoparticles was found. AgBr nanoparticles, modified by oleic acid were mixed with MMA. After polymerization was carried out, the polymeric photochromic material was synthesized.

首次采用油酸萃取并包覆了水溶胶中的AgBr纳米粒子，制备了AgBr有机溶胶；并找到了萃取率最佳时的油酸与AgBr的摩尔比；再将油酸包覆的AgBr掺杂到甲基丙烯酸甲酯中，进行本体聚合，从而制备了AgBr光致变色有机玻璃。

Results of a series of orthogonal design methods demonstrate that a crosslinked PAA superabsorbent composite with sodium tungstate, which is synthesized with a composition of 45.5 wt% of monomer, 0.4 wt% of crosslinker, 1.0 wt% of initiator, a neutralization degree of 83%, and a reaction temperature of 90℃, has a good water absorbency.

此外，通过对WPAA-Na的制备与吸水性能的一系列正交实验分析后得出，当单体浓度为45.5%、反应温度为90oC、交联剂浓度为0.4%、引发剂过硫酸钾浓度为1.1%以及中和度为0.85时，树脂的吸水倍率为佳。

Starch phosphate monoester s were synthesized with the corn starches and orthophosphate mixture by the wet process.

以玉米淀粉为原料，与混合磷酸盐作用，采用湿法工艺制备淀粉磷酸单酯。

Phosphorylated chitosan (phosphorylate-modified chitosan,P-CTS) was synthesized by the reaction of monosodium orthophosphate with urea in the presence of HAc.

壳聚糖(chitosan，CTS)是由β(1~4)键合的D-葡糖胺残基和数目不同排列无规的N-乙酰基葡糖胺残基组成的线性多糖，是生物界中大量存在的唯一的一种碱性多糖。

A dominant B2CN crystal with orthorhombic structure was synthesized using ...

与立方氮化硼的合成相比，立方B(CxN1-x)的形成温度下降了近200℃。

Firstly,the presence and location of AAT in amphioxus was studied by Westernblotting and immunohistochemical methods.The results first revealed that AATpresent in amphioxus,a cephalochordate.Also it was demonstrated that AATdistributed in cellular plasma in hepatic diverticulum,the pouch that protrudesforward as an outpocketing of the digestive tube and extends along the right side ofthe posterior part of the pharynx,which has long been considered to be the precursorof vertebrate liver.In vertebrate,AAT is primary synthesized in liver.

我们首先利用免疫组化和Western blotting方法，研究了AAT在文昌鱼的组织表达和定位，首次在头索动物文昌鱼中证明了AAT的存在，结果显示，AAT定位于文昌鱼肝盲囊的细胞浆内，从AAT在文昌鱼中的合成部位来看，在功能上文昌鱼的肝盲囊等同于脊椎动物肝脏，肝盲囊是在发育分化过程中消化道组织向右前方突出沿着咽后部向前扩展和延伸形成的一个囊袋状结构。

It is feasible to overgrow mesoporous MCM-41 on the rough surfaces of the grains. The obtained samples possess the ordered hexagonal mesoporous structure of MCM-41-type molecular sieves. Mesoporous molecular sieves (denoted as MZ-B) with ordered hexagonal structure have been successfully synthesized by the assembly of the precursors from filtrate of alkali-treated ZSM-5 zeolite with CTMABr surfactant micelles in alkaline media based on S+I– static electricity route.

而碱处理ZSM-5沸石得到的滤饼为富含超细化颗粒的晶粒，且晶粒粗糙度很高，因此易于附晶生长介孔分子筛，得到的微孔颗粒表面附晶生长的介孔分子筛，具有很好的长程有序度，为六方排列的孔道结构。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失