查询词典 synthesized

Secondly, organical composite thermal storage materials which takethe PNIPAAm gels as the carriers and the palmitic acid and the lauric acidmixture for phase change materials were Synthesized by radicalpolymerization ,and organical/inorganical composite materials which takeP(NIPAAm-co-AAm) gels as the carriers and the palmitic acid、thelauric acid and Na_2HPO_4·12H_2O mixture were also Synthesized byradical polymerization.

其次，本文采用自由基聚合法，合成了以PNIPAAm凝胶为载体，棕榈酸和月桂酸的混合物为相变材料有机复合相变蓄热材料；及P(NIPAAm-co-AAm)凝胶为载体，棕榈酸、月桂酸和Na_2HPO_4·12H_2O为相变材料的有机／无机复合相变蓄热材料，采用红外光谱、示差扫描量热法、热重分析、扫描电镜等手段对两种复合材料的结构及热性能进行了表征与分析，研究了有机酸和无机盐的百分含量对复合材料的相变温度和相变焓的影响。

The experimental results showed that SiC ultrafine powder was synthesized at 1500℃for 120 minutes by used rare earth lanthanum as additive. Its primary particle size was about 100nm and aggregated particle size was about 360nm and the particle shape was regulation, non-aggregation and well dispersibility. While the rare earth ceria used as the additive, SiC ultrafine powder was synthesized at 1500℃for 150 minutes but the particle shape was irregulation and seriously agglomerated and had numerous crystal whiskers.

实验结果表明：以稀土镧为添加剂时，在1500℃×120min合成工艺下，可以合成出一次粒径为100nm左右，二次粒径为360nm的SiC细粉，且SiC粉体颗粒形状规则，无团聚，分散性好；以稀土铈为添加剂时，在1500℃×150min合成工艺下，也可以得到单相的SiC，但SiC粉体颗粒形状不规则，有大量晶须存在，且团聚严重。

Isocyanurate based on TDI was synthesized and the heat-resistance property of casting polyurethane elastomer which synthesized using isocyanurate based on TDI and PEPA was obviously enhanced compared to polyurethane elastomer which did not introduce the isocyanurate by the TGA under the different temperature and the mechanics performance maintenance rate at high temperature.

在催化剂作用下，合成了TDI-100型异氰脲酸酯，并与己二酸乙二醇丙二醇酯合成了浇注型聚氨酯弹性体，通过不同温度下的热失重分析和弹性体的力学性能高温保持率对比分析表明，在TDI型聚氨酯弹性体中引入异氰脲酸酯基团，可明显提高弹性体的耐热性能。

Two coordination polymers composed of in situ synthesized ligand deriving from isophthalic acid through the hydroxylation on the 2-position have been synthesized under hydrothermal conditions.

利用铜离子的氧化还原性质，以铜离子和间苯二甲酸在水热条件下反应使配体发生羟基化衍生成2，6-二羧基苯酚，并组装出2个含衍生配体的配位聚合物。

In addition, a chalcone derivative was synthesized as fluorescent and colorimetric chemosensor for anions such as F~- and AcO~-.5. Mesoporous SQ/SBA-15 on the basis of the interaction of squaraine dye and mercaptol was designed and synthesized.

设计合成了一个查尔酮化合物5，加入碱性较大的阴离子后，紫外可见吸收光谱和荧光光谱均发生变化，有望发展为荧光和生色双功能阴离子传感器。5。

Firstly, a series of organic molecules which use phthalimido group as electron acceptor, N as electron donor, COO~- as eletrofugal group were synthesized based on SET-promoted photocyclization processes. These compounds were irradiated by 500 W ultraviolet under nitrogen atmosphere in room temperature. After filtration of the photochemical character of these molecules, substrate S1 and S2 were selected as appropriate model reactants. Secondly, the monosubstituted derivatives at the 6-position ofβ-cyclodextrin were synthesized as chiral template of photocyclization.

首先，以单电子转移机理为指导，设计了一系列以邻苯二甲酰亚胺基为电子受体、N为电子给体、羧基为离去基团的光环合反应底物，这些化合物在氮气保护下以500瓦紫外光室温下进行光照反应，对这一系列的分子的反应情况进行了研究与筛选，最终选择底物S1和S2作为研究光环合反应中立体控制方法的模型底物；其次，又合成了一系列6-位单取代β-环糊精，以此作为光环合反应的手性模板。

Firstly, 2-Hydroxy-4-octyloxybenzophenone was synthesized from 2,4-dihydroxybenzophenone and octyl chloride in the presence of N-octyl-diethanolamine borate as ion liquid, and 2-Hydroxy-4-methyloxybenzo phenone was synthesized from 2,4-dihydroxybenzophenone and dimehylsulfate in the presence of N-octyl-diethanolamine borate as catalysis.

首先作为离子液体催化合成了2-羟基-4正辛氧基二苯甲酮和作为相转移催化剂合成了2-羟基-4甲氧基二苯甲酮。

Paper electrophoresis showed that the Onobrychis viciaefolia and Medicago sativa cell line transformed with A〓 synthesized agropine and mannopine, and Onobrychis viciaefolia cell line transformed with LBA9402 Bin19 only synthesized agropine.

红豆草转化系获得再生植株。LBA9402 Bin19转化系可以抗100mg／l卡那霉素。苜蓿A4转化系未能得到再生植株。纸电泳分析表明红豆草A4转化系和苜蓿A〓转化系可以合成农杆碱和甘露碱，而红豆草LBA9402Bin19转化系只能合成农杆碱。

This NS-MCM-41-Pd proves to be an efficient heterogeneous catalyst to catalyze aryl bromides with organozinc reagents for Negishi reaction. In the third suject, fluorescent surfactants with different conjugated aromatic moieties and changeable and gradually extended hydrophobic lengths were successfully synthesized by multiple synthesized manipulations.

首先利用颗粒大小为奈米尺度(约100 nm)、表面积约 660 m2/g 与孔径大小约 2.6 nm 且孔道分布为虫洞结构之孔洞材料，NS-MCM-41，作为异相触媒担体，稼接上钯错合物形成异相催化剂 NS-MCM-41-Pd，催化 aryl bromides 与 organozinc reagents 进行 Negishi reaction，并探讨触媒反应后再回收活性测试。

In the thesis, a series of novel single and multi-armed oxadiazole bridging ligands and pyridyl-4, 5-imidazole dicarboxylic acid ligands have been synthesized. The coordination chemistry of these novel ligands with transition metal ions was investigated. In addition, two 1, 3, 4-oxadiazole bridging ligands end-capped by chelating Schiff-base coordination sites have been designed and synthesized. The coordination chemistry based on one of the two ligands with metal ions was primarily investigated.

本文报道了一系列新颖的含1， 3， 4-Oxadiazole杂环的单臂及多臂有机配体，研究了它们与过渡金属离子的配位反应化学；合成了吡啶基-4，5-咪唑二羧酸有机配体，研究了它们在水热条件下与过渡金属离子的配位反应化学；另外，还合成了1， 3， 4-Oxadiazloe杂环桥联的双Schiff-base有机配体，初步探讨了其与过渡金属离子的配位反应化学。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失