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Furthermore, TiCN nanocrystals were synthesized at 420 for 8h using TiCU, CCl4 and NaN3 via chemical metathesis method.

通过TiCl_4，CCl_4和NaN_3之间的化学交换反应，在420℃加热8小时也制备出了TiCN纳米晶体。

After sodium bisulfite reacted with methanal at 60-65℃ for 0.5h, aniline was dripped into the system to synthesize phenylaminomethyl-sodium sulfonate subsequently, the diazol solution of p-nitroaniline was dripped into phenylaminomethyl-sodium sulfonate synthesized to form 4'-nitro-4-aminoazobenzene. The compound was then added into diazol solution of p-chloroaniline to obtain the object product, which was identified by IR spectrum and element analysis.

在60~65℃温度下，亚硫酸氢钠与甲醛反应半小时之后滴入苯胺生成苯胺基甲基磺酸钠，另将硝基苯胺重氮化得到重氮盐溶液滴入苯胺基甲基磺酸钠中得到4'-硝基-4-氮基偶氮苯，然后将其滴入氯苯胺重氮化后的重氮盐溶液中，得经红外光谱检验和元素分析证实的目标产物。

Tris-1,3,5-triazine and 2,4,6-Tris-1,3,5-triazine were synthesized from 2,4,6-trichlloro-1,3,5-triazine, the water solution of methylamine and dimethylamine.The products were characteried by FT-IR and DSC.

以三聚氯氰、甲胺和二甲胺水溶液为原料，合成了2，4，6-三甲胺基-1，3，5-均三嗪和2，4，6-三二甲胺基-1，3，5-均三嗪HMM），并用FT-IR和DSC对其进行了表征。

In this thesis, 1, 5-diaryl-3-pyrazilidinones, 1, 5-diaryl-3-hydroxypyrazoles and 3-(2, 3, 4, 6-tetraacetyl-β-D-glucopyranos-1-yl)-1, 5-diaryl-1H-pyrazoles are designed and synthesized.1, 5-diaryl-3-pyrzolidinones were obtained by condensation of 3-arylpropenates and phenylhydrazine or fluorophenylhydrazine under the catalysis of sodium methylate and the yields were about 55-80%.

在本文中，设计合成了1，5-二芳基-3-吡唑烷酮化合物、1，5-二芳基-3-吡唑烷酮化合物和3-(2，3，4，6-四乙酰基-β-D-吡喃葡萄糖-1-基)-1，5-二芳基吡唑化合物。以3-芳基-2-丙烯酸酯为原料，与芳基肼在醇钠的催化作用下，反应可以生成1，5-二芳基-3-吡唑烷酮，产率在55%以上。

The steps were as follows: trimethyl borate-10 was synthesized from boron-10 trifluoride-ether complex and sodium methylate,which was hydrolyzed to synthetize boric-10 acid .

为了开发经济高效的硼-10酸生产路线，文中对于以工业生产得到的三氟化硼-10-乙醚络合物为原料生产硼-10酸的工艺进行了初步研究。

The steps were as follows: trimethyl borate-10 was synthesized from boron-10 trifluoride-ether complex and sodium methylate,which was hydrolyzed to synthetize boric-10 acid.

首先采用三氟化硼-10-乙醚络合物与甲醇钠反应生成硼-10酸三甲酯，之后水解合成硼-10酸。

Methods The microstructure and components of the synthesized coatings were studied by means of X-ray diffraction and electron probe microanalysis.

利用X射线衍射仪和电子探针分析仪对涂层进行相分析、组织观察和成分分析。

Mesoporous molecular sieves, named SAN-01, were hydrothermally synthesized with microcline, a natural ore, as starting material, and the seeds of 13X zeolite as pore-wall＇s crystal source.

以微斜长石制备的硅铝酸盐前驱物为主要原料，以13X沸石晶核剂为孔壁结构导向剂，水热合成了含有13X沸石基本结构单元的硅铝酸盐介孔分子筛SAN-01。

Aluminosilicate mesoporous molecular sieves are synthesized with natural ore and microcline as main raw materials,and the precursors of 13X zeolite as crystal source,by integrating the synthetic procedures of mesoporous MCM-41 and microporous 13X zeolite.

以天然矿物微斜长石为主要原料，13X沸石前驱体为晶核剂，结合介孔分子筛MCM-41与13X沸石合成工艺，合成了孔壁中含有13X沸石基本结构单元的铝硅酸盐介孔分子筛。

Aluminosilicate mesoporous sieve s with 13X zeolite units in the pore wall were synthesized with a natural ore,microcline,as the main raw material,and the precursors of 13X zeolite as the crystal source,by integrating the procedures for MCM-41 and 13X zeolite synthesis.

以天然矿物微斜长石为主要原料，以13X沸石前驱体为晶核剂，结合介孔分子筛 MCM-41与13X沸石合成工艺，合成了孔壁中含有13X沸石基本结构单元的铝硅酸盐介孔分子筛。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失