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Nanoparticle ammonium zinc phosphate with dodecahedron morphology was synthesized via the solid-state reaction at room temperature.

采用室温固相反应制备纳米十二面体磷酸锌铵,用微热量法研究该反应的标准摩尔反应焓和纳米磷酸锌铵的标准摩尔生成焓,用4种热分析法研究纳米磷酸锌铵的分解动力学。

Peripheral plasma membrane proteins extracted from the spermatozoa from caput,corpus and cauda epididymis as well as vas deferens were probed with four lectins—Arachis hypogaea agglutinin、Canavalia ensiformis agglutinin、Dolichos biflorus agglutinin、Triticum vulgaris agglutinin.The results indicated that the 104 and 95kD AHA binding glycoproteins,and the 117、114、104、87、76、70kD ConA binding glycoproteins were synthesized and modified in the testis;the 120 and 65kD ConA binding glycoproteins,and the 54kD DBA binding glycoprotein were modified or lost during epididymal maturation;the 109kD ConA binding glycoprotein,the 74、70、45kD DBA binding glycoproteins,and the 57kD TVA binding glycoprotein were modified during epididymal maturation.

结果表明:与花生凝集素结合的104kD和95kD糖蛋白,与伴刀豆凝集素结合的117、114、104、87、76、70kD糖蛋白在睾丸中已完成了蛋白合成及修饰过程;与伴刀豆凝集素结合的120kD和65kD糖蛋白,与双花扁豆凝集素结合的54kD糖蛋白在精子附睾成熟过程中被修饰成其它种类的蛋白或被丢失;与伴刀豆凝集素结合的109kD糖蛋白,与双花扁豆凝集素结合的74、70、45kD糖蛋白,以及与麦胚凝集素结合的57kD糖蛋白是在附睾中完成其修饰过程的。

Furthermore, the important fragment which is composed of pentenyl cinnamic acid and D-Tyrosine, and the ester which is composed of L-N-methylated phenyl amino acid and diketopiprazine was synthesized with considerable yield The conjugation of the new DOPA analogue into the peptide in the total synthesis of Pepticinnamin E was investigatited

另外,本文作者还进一步合成了高收率的戊烯基肉桂酸衍生物与D-酪氨酸的缩合片段及L-N-甲基苯丙氨酸与哌嗪二酮的酯两个重要的结构组成部分;对新多巴衍生物片段嵌入肽链中的工作亦进行了有益的尝试。

In this Thesis,Ⅱ-Ⅵ semiconductor nanoclusters and doped nanoclusters were synthesized and their special photoluminescence properties were investigated in details.

本文在对半导体纳米晶的物理性质进行较为全面了解的基础上通过掺杂稀土离子来提高纳米颗粒的发光效率,为纳米晶材料的实用化提供实验依据。

The synthesized Mg2Al layered double hydroxide and its calcined product were characterized.

对合成的Mg2Al型层状双金属氢氧化物及其煅烧产物进行了表征。

By means of polymerase chain reactionand DNA recombinant techniques,the gene encoding mature ouse IL-4 was obtained from plasmid pCD-mIL4 and was inserted into expressionvector pBV220,which contains _RP_L double promoters,synthesized SD sequence and temperaturesensitive CIts857 gene,thus an expression lone eferred as pBV-mIL4 was constructed.

该质粒含有 P_RP_L 串联启动子,合成 SD 序列和温度敏感的CIts857基因,并且去除了完整小鼠 IL—4 cDNA 中3′侧翼非编码区,以原核系统高频使用的强终止密码子TAA 代替了原小鼠 IL-4基因的终止密码子 TAG,经 SDS-PAGE 及凝胶密度扫描分析,表达的重组小鼠 IL-4分子量约为14.2KDa,占总菌体蛋白量的25~30%。

In addition, a series of double stranded polymers by using furan-containing oligoaryls as linkers was synthesized.

另一方面,我们将连接降冰片烯骨架的基团,以一系列不同共轭长度的苯环呋喃交错寡聚物取代。

The former is to prepare polymolybdates coordinated' directly by organic ligands using Na2MoO4 and MoO3 precursors; The latter plays emphasis on exploiting a simple and effective routine to synthesize Keggin polytungstates in which the transition metal or Si acts as the heteratom by reaction precursor Na2WO4.We have synthesized a 4,4'-bipyridine bridging dumbbell-like polymolybdates a metatungs...

前者主要是制备有机配体键合的多金属钼酸盐;后者重点是探索出一个简易、有效的合成过渡金属或主族元素硅作杂原子的Keggin多金属钨酸盐的方法,然后通过变换过渡金属或有机配体的种类探讨对产物结构的影响,再对所得化合物的结构和组成通过物理测试手段进行表征,同时研究其在光、电、磁等方面的性质。

Mesoporous zincum sulfide is synthesized by room-temperature method and hydrothermal technique, employing the surfactant cetyltrimethyl ammonium bromide, duodecimal alkyl sulfonic natrium and lauryl amine as templates. All kinds of technic parameters' influence to the synthesis has been systematically discussed, and the extracting of templates have been investigated.

本论文以十六烷基三甲基溴化铵、十二烷基磺酸钠及十二胺为模板,采用水热法和室温法合成了介孔硫化锌,系统探讨了各种工艺参数对合成材料结构特征的影响。

The four components of uPA system could be synthesized and secreted by all the four cell lines, existed in duplet or triplet form (uPA/PAI-1,uPA/PAI-2,uPA/uPAR,uPA/PAI-1/uPAR and uPA/PAI-2/uPAR). The expression of uPA system were not in concomitance with the malignance of the cell lines.Subject headings urokinase; carcinoma, non-small-cell lung; cells,cultured

此4株细胞中均能合成与分泌uPA系统的4种主要成分,各因子以二联及三联复合物(uPA/PAI-1、uPA/PAI-2、uPA/uPAR、uPA/PAI-1/uPAR、uPA/PAI-2/uPAR)的形式存在;uPA系统的表达与这4种细胞的恶性程度并不一致。

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Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

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