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P chlorophenoxyacetic sodium was synthesized by p chlorophenol with 2 chloroacetic acid in the 20% hydroxide sodium aqueous solution.

采用一步法由氯乙酸与对氯苯酚在氢氧化钠质量分数为 0 2的水溶液中的反应制得。

Four series of metal bile acid complexes were synthesized, including transition metal cholate and deoxycholate complexes, rare earth cholate and deoxycholate complexes.

合成了四个系列的金属胆汁酸配合物，包括过渡金属胆酸及脱氧胆酸配合物，稀土元素胆酸及脱氧胆酸配合物。

The synthesized peptide was purified by the chromatograph and identified by mass spectrograph.

用色谱仪和质谱仪对合成的多肽进行纯化、鉴定。

Influence of the concentration of Cr in the leachate and quantity of Pb(CH3COO)2 of Pb(NO3)2 on the reaction of synthesizing yellow chrome was also studied. Finally, according to the criterion and standard method in GB3184-82, some yellow chrome synthesized in the experiments was sampled and the concentration of PbCrO4 in these samples was determined. The following conclusion can be drawn from these experiments.

根据中华人民共和国国家标准GB3184-82中的规定铅铬黄颜料的技术质量指标和检测方法，测定了铬黄样品中铬酸铅含量的厂迄回【、矾士牢位论父泅仰yW盯皿'S川mS达标情况，结论如下：门）反应中重铬酸盐的浓度并不需要达到前人所提出的150～2509·L'的范围，在一定条件下低于此浓度时对铬黄生成反应并无不利影响。

In the first part, twelve peptides, including eight conservative amino acid residues in the amino acid sequence of hydrophilic S helix of AOX. were synthesized by solid-phase method. The polypeptide was coupled to a -chymotrypsinogen, and the antibodies were obtained through immunizing rabbit by injecting this complex.

第一部分，我们按照交替氧化酶(Alternative Oxidase，AOX)位于线粒体内膜外侧亲水区S螺旋的氨基酸序列，用固相法合成由12个氨基酸残基组成的多肽，将此多肽与α-牛胰凝乳蛋白酶原A相连，用作半抗原，免疫家兔制备人工合成12肽的抗体。

Six 3,6-dichloropyridazine-derivatized cinchona alkaloid catalysts were synthesized and applied in IFB reaction.

二氢奎宁二聚体2c最差(56%ee)，与环己二酮相比，环戊二酮作为反应原料时，产物的ee值降低。

A new chiral quaternary ammonium sails prepared from cinchonine was designed and synthesized.

本课题设计并合成了一种新的辛可宁型手性季铵盐。

A new chiral quaternary ammonium salt 1a was synthesized by the reaction of cinchonine and(2,4,6-)trimethyl benzyl chloride.Etherification between 1a and benzyl bromide,allyl chloride,or methyl give corresponding etherified quaternary ammonium salts 1b,1c,and 1d.

由辛可宁和2，4，6-三甲基苄氯，合成了一种新的手性季铵盐(1a)，并进一步用苄基溴、碘甲烷和烯丙基氯对分子中的羟基进行醚化，得到相转移催化剂1b、1c和1d。

It is demonstrated that the chiral quaternary ammonium salts catalysts exhibit promising catalytic properties for the substrate. Part III: The synthesis and the characterizing of the macroporous aminomethyl resin-supported cinchona alkaloid complexes and the study on its catalytic properties The part consists of two subsections. the macroporous aminomethyl resin -supported cinchona alkaloid complexes were synthesized by the stuff (cinchonine, quinine and macroporous aminomethyl resin). Their structures were characterized by means of elemental analysis, XPS, TG/DTA; the chiral polymer-supported complexes were first used as catalysts for the reduction of ketones. Their catalytic properties for the reduction processes were investigated. The comparison of the products e.e., the conversion of the substrate among different reduction processes was employed with determined by HPLC. The effects of the time, the temperature, the ratio of catalyst to substrate, reaction solvent as well as the recycle times were also discussed.

第三章聚-4-氨甲基苯乙烯负载金鸡纳碱金属络合物的合成与表征及其不对称催化性能研究本章分为两节，以辛可宁和奎宁及聚-4-氨甲基苯乙烯为原料，合成了4种聚-4-氨甲基苯乙烯负载金鸡纳碱络合物催化剂，并对它们的结构用元素分析、X-射线光电子能谱、TG/DTA等几种测试手段进行了表征；首次将所合成的手性高分子负载的金属络合物用于催化芳香酮不对称还原反应，详细研究了所得的手性高分子负载的金属络合物对不同底物的催化性能，用HPLC等分析手段定量检测了还原过程的底物转化率及其产物对映异构体选择性，并考察了反应时间、反应温度、催化剂和底物投料比、反应溶剂和循环次数对催化性能的影响。

Amino(9-deoxy)epicinchonine was synthesized from cinchonine through the Mitsunobu reaction and was treated with p-toluenesulfonyl chloride,4-chlorobenzene sulfonyl chloride respectively to give two new chiral sulfonamide s.

以辛可宁为原料，经Mitsunobu反应合成了9-氨基(9-脱氧)表辛可宁，然后分别与对甲苯磺酰氯、对氯苯磺酰氯反应，合成了两个新手性磺酰胺，其结构经红外光谱和核磁共振确证。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。