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In order to research the relations of carbon sources to structure of PHAs, six kinds of PHAs sample were synthesized by activated sludge with six different carbon sources respectively in the aerobic-anaerobic-anoxic process. Their structures were determined by 〓HNMR、〓CNMR and GC-MS. When the carbon source was acetate, the unit composition of PHAs was 93. 91mol％ 3-hydroxybutanoic acid and 6. 09mol％ 3-hydroxypentanoic acid ; When the carbon source was propionate, the unit composition of PHAs was 28. 66mol％ HB, 63. 13mol％HV, 2. 55mol％ 2-methy-3-hydroxy-butanoic acid (2MHB) and 5. 66mol％ 2-methyl-3-hydroxypentanoic acid (2MHV); When the carbon source was 80％ butyrate and 20％ 1, 4-butanediol, the unit composition of PHAs was 65. 03mol％ HB, 28. 06mol％HV, 1. 91mol％2MHB, 2. 69mol％ 2MHV, 0.73mol％ 4-hydroxy butanoic acid (4HB), 0.78mol％ 4-methyl-3-hydroxy-pentanoic acid (4MHV), 0.80mol％ 3-hydroxyhexanoic acid ; When the carbon source was 20％ butyrate and 80％ 1, 4-butanediol, the unit composition of PHAs was 61. 39mol％ HB, 23. 01mol％HV, 4. 58mol％2MHB, 5. 97mol％ 2MHV, 0.91mol％ 4HB, 2. 37mol％ 4MHV, 1. 77mol％ HHx; When the carbon source was 60％ pentanoate and 40％glucose, the unit composition of PHAs was 41. 24mol％ HB, 58. 76mol％HV; When the carbon source was 60％ benzoate and 40％ glucose, the unit composition of PHAs was 65. 48mol％ HB and 34. 52mol％ HV.

为了研究不同碳源与产物PHAs结构的关系，采用好氧-厌氧-缺氧模式利用6种不同碳源培养活性污泥得到6种不同的PHAs样品，通过〓HNMR、〓CNMR和GC-MS谱图确定了这6种PHAs的单体成分和比例：以乙酸钠培养活性污泥得到的PHAs的单体组成是93.91mol％3-羟基丁酸和6.09mol％3-羟基戊酸；以丙酸钠培养活性污泥得到的PHAs的单体组成除28.66mol％HB、63.13mol％HV外，另外还有2.55mol％3-羟基2-甲基丁酸（2MHB）和5.66mol％3-羟基2-甲基戊酸（2MHV）；以80％丁酸钠和20％1，4-丁二醇混合溶液培养活性污泥得到的PHAs含有七种单体组成：65.03mol％HB，28.06mol％HV，1.91mol％2MHB，2.69mol％2MHV，0.73mol％4-HB（4-羟基丁酸），0.78mol％4MHV（3-羟基-4-甲基戊酸），0.80％HHx（3-羟基己酸）；以20％丁酸钠和80％1，4-丁二醇培养活性污泥所得到的PHAs含有与3#样品相同的七种单体，只是比例不同，分别是61.39mol％，23.01mol％，4.58mol％，5.97mol％，0.91mol％，2.37mol％，1.77mol％；以60％戊酸钠和40％葡萄糖培养活性污泥所得到的PHAs由HB和HV组成，比例是41.24 mol％∶58.76 mol％；以60％苯甲酸钠和40％葡萄糖培养活性污泥所得到的PHAs也由HB和HV组成，比例是65.48 mol％∶34.52 mol％。

Using butyraldehyde and 1,2-propanediol as raw materials, H3PW6Mo6O 40 /TiO2 as catalyst, butyraldehyde 1,2-propanediol acetal is synthesized.

以二氧化钛负载磷钨钼杂多酸为催化剂，通过丁醛和1，2-丙二醇反应合成了丁醛1，2-丙二醇缩醛。

CdS nanoarods have been synthesized by using Cetyltrimethyl Ammonium Bromide as the soft template under γ-irradiation through the reaction of cadmium sulphide (CdSO4·8/3H2O) and thiacetamide in acidic condition for pH value of 3. The physical and chemical properties and the structure of CdS nanorods were characterized by XRD, UV-Vis, SAED, TEM and PL.

在pH=3的酸性条件下，以硫酸镉和硫代乙酰胺为反应前驱体，采用十六烷基三甲基溴化铵自组装形成的管状胶束为模板，通过γ射线辐照法成功合成了CdS纳米棒，并通过XRD、UV-Vis、SAED、TEM和PL等技术对反应中间产物及最终产物进行了表征。

Dimethyl N-cyanodithioiminocarbonate was facilely synthesized from calcium cyanamide, sodium carbonate and carbon disulfide, using dimethyl sulfate as a methylating agent in aqueous phase with an overall yield of 72% and purity of 99%.

用氰氨化钙、碳酸钙和二硫化碳等为原料，硫酸二甲酯为甲基化试剂，采用水相合成工艺制得荒酸二甲酯，总收率72%，纯度99%。

By means of hydrothermal method, high quality calcium stearate were cleanly synthesized by the reaction of calcium hydroxide with stearic acid in water.

以硬脂酸和氢氧化钙为原料，采用水热法合成出了色泽好的高质量硬脂酸钙。

CaTiO3 powder was synthesized by solid-state reaction of calcium nitrate with TiO2 formed by hydrolysis of tetrabutyl titanate.

以钛酸四丁酯的水解产物TiO2和硝酸钙为原料，固态反应合成CaTiO3。

The calcium propionate was synthesized with calcium oxide as raw material in this paper.

以氧化钙为钙源制取丙酸钙，对传统反应工艺进行了改进。

Three different calcium oxide catalysts were synthesized from different precursors and characterized by X-ray diffraction, scanning electron microscopy, and temperature-programmed desorption.

用不同的前驱物合成了三种CaO催化剂，并以X射线衍射、扫描电子显微镜、程序升温脱附等方法加以表征。

However, it is very toxic. Nocantharidin, a derivative of cantharidin first synthesized in China, is a new anti-tumor drug with strong anti-tumor activities and increases the number of while blood cells.

去甲基斑蝥素(noncantharidion， NCTD)为斑蝥素的衍生物，是我国首先合成的具有较强抗肿瘤活性和独特升高白细胞作用的新型抗肿瘤药物。

According to results of cantharidin structure-activity relationships, a series of cantharidin derivatives for the first time were designed, synthesized and characterized by IR, NMR and elemental analysis.

用IR、〓H NMR初步证实了斑蝥素衍生物和DCC生成稳定中间体是使含有芳香羧酸的斑蝥素衍生物与氨基葡萄糖及其衍生物不能进行反应的主要因素。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。