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The powder baked at 680C is perfect in properties, and zinc oxide will decompose when the reduction temperature exceeds 700 C,Results of XRD, SEM and TEM for the targets indicate that secondary phase ZnAl2O4 exists in the targets synthesized with reduced or unreduced compound powders, but not in the target synthesized with nanometer powders.

各靶材样品的XRD、SEM和TEM分析结果表明：以还原和未还原ZAO粉为原料的靶材组织中出现了第二相组织：ZnAl_2O_4，而以纳米ZnO、Al_2O_3粉为原料的靶材组织中未见第二相。

Mesoporous zincum sulfide is synthesized by gentle wet chemosynthesis method, with DDA as templates and Zinc acetate and TAA as precursors. The effect to the synthesis of the ratio of reactive components, the volume of pH, reactive time and reactive temperature has been dicussed systematically, and structures of the as-synthesized samples have been characterized by X-ray diffraction, N2 adsorption-desorption, scanning electron microscopy, Fourier transform-infrared spectra, UV-vis diffuse reflectance spectroscopy, transmission electron microscopy.

以十二胺为模板，醋酸锌及硫代乙酰胺为前驱体，温和湿化学法合成了硫化锌无序介孔结构，系统研究了反应物配比、pH值、反应温度、反应时间对材料合成的影响，运用X射线衍射、N2吸附-脱附、扫描电镜、红外光谱、紫外-可见吸收光谱、透射电镜等分析手段对介孔材料的结构进行了详细的表征。

Then GaN nanostructured thin films comprised of regular hexagonal crystal grains have been successfully synthesized by ammoniating Ga2O3 films at the temperature of 850℃ for 15 rain in a quartz tube. X -ray diffraction reveals that the synthesized GaN is of a hexagonal wurtzite structure with lattice constants a =0.318 nm and c =0.518 nm.

然后将硅基Ga2O3置于管武石英炉中，在850℃的氨化温度下氨化15min后，成功制备出GaN薄膜，该薄膜由正六边形的晶粒组成。X射线衍射表明GaN具有六方纤锌矿结构，晶格常数为a=0.318nm和c=0.518nm.X射线光电子能谱的测试确定了样品中Ga-N键的形成，并且Ga和N的化学计量比为1：1。

In this article, the properties of the synthesized fibers including the rmicrocosmic appearance, the thermodynamic stability and so on were investigated and tested, and their swelling capabilities were also studied. The results show that the decompounded temperature of the synthesized fiber is increased by about 100K and the cross-linked fibers have good swelling capability in solvents and non-solvents.

本文还对合成后纤维的微观形貌、热稳定性等性质进行了考察与测试，对其溶胀性能进行了初步研究，结果表明合成后纤维发生热分解的温度要比原纤维高100K左右，在良性和非良性溶剂中都有很好的溶胀性能。

The most important, PsaA/B apoproteins can be synthesized obviously in the dark, which is different with the early report [1] that PsaA/B apoproteins can't be synthesized in the etiolated plants such as pea, barley. This different may come from that the volume and size of the chloroplast is not markedly reduced in dark-grown Y-1 cells and many enzymes involved in photosynthesis are localized on the chloroplast envelope.

同时发现，叶绿体基因编码的PSI核心多肽PsaA/B能够在暗条件下合成，而资料报道[1]高等植物如豌豆、大麦的黄化体中不能合成PsaA/B蛋白，这可能是由于在脱绿的Y-1细胞中叶绿体的量并没有发生明显的减少，且仍具有相对完整的大小和形状，而在叶绿体的被膜上具有许多参与光合作用的酶系统。

The results show that nano-crystalline NiAl intermetallic compound can be synthesized by MA taking elemental powders of NixAl100-x(x＝25,30,40,50) as green reactants. Supersaturating solid solution NiAl intermetallic compound can be synthesized by MA using nonstoichiometric Ni-Al powders, and the synthesis mechanism is combustion reaction which includes forced solid solution based on atomic diffusion.

研究表明：NixAl100-x四种成分的元素粉末通过机械合金化方法均制备出纳米晶NiAl金属间化合物粉末；非化学计量配比成分的Ni-Al粉末通过机械合金化合成NiAl过饱和固溶合金，其机械合金化合成机理为含有以原子扩散为基础的强制固溶的燃烧合成反应。

Chapter V: A 1-D Zn coordinatin polymers is synthesized by the reaction of sodium azide, nicotinic acid and zinc chloride. A 3-D Ag supramolecular complex is synthesized by the reaction of sodium azide, 2-methylimidazole and silver chloride.

第五章：采用叠氮为基本构建单元，和烟酸共同桥联金属Zn得到一种一维链状配位聚合物；和2－甲基咪唑反应，得到一种银的三维超分子配合物。

As for PAn-based composites, the influences of the kinds of oxidant, the amount of hydrochloric acid and barbon black on conductivity were investigated, Li/PAn button-type secondary batteries were assembled with PAn-based composites which were synthesized by chemical oxidative polymerization and used as cathode, the influences of the kinds of oxidant, synthesized technics, conducting carbon black added mode and PAn/metal oxide composites used as cathode on the properties of these batteries were studied.

对于聚苯胺基复合材料体系，研究了氧化剂种类、盐酸用量、炭黑用量对复合材料电导率的影响；以化学法制备的聚苯胺基复合材料作正极组装了Li/PAn二次扣式电池，探讨了氧化剂种类、聚合工艺、导电剂的加入方式以及PAn与金属氧化物复合后作电池正极的性能。

Synthesis and structural characterization of novel cycioplatinated complexes with 2-aryl imidazolines 2-arylimidazoline ligands 2a-2d were synthesized from benzoyl chloride or p-methoxybenzoyl chloride with aminoethanol or valinol and 2e was synthesized from 2-phenylimidazoline.

新型2-芳基咪唑啉环铂化合物的合成与结构表征以苯甲酰氯或4-甲氧基苯甲酰氯和氨基醇(2-氨基乙醇或外消旋的缬氨基醇)为原料，合成了四种2-芳基咪唑啉配体2a-2d，以2-苯基咪唑啉为原料合成了配体2e，其中2d为新化合物。

Mmunoglobulin is composed of two heavy chains and two light chains. Normal Ig is synthesized and assembled in B cells according to special ratio. Generally speaking, light chain is synthesized a bit faster than heavy chain which results in the existence of some free light chains in serum. Normally, the number of sFLC was kept in a suitable scope.

g由两条重链和两条轻链组成，正常人Ig在B淋巴细胞中按照一定比例合成，并进行装配，一般情况下轻链的合成速度略快于重链，因此血中会出现一定比例的游离轻链(free light chain，FLC)，正常人血清游离轻链(serum free light chain，sFLC)维持在一定范围。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失