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Benzoylated phenyl a - and B - 2 - thio - D - fructofuranosides were synthesized and coupled with protected sucrose acceptor to synthesize a - D - fructofuranoside - linkage stereospecifically by employing NIS/AgOTf as catalysts.

在果糖的合成研究中，合成了四苯甲酰基苯基果糖硫苷，并首次将其用作糖苷化反应的给体，在NIS/AgOTf的促进之下，与乙酰化保护的蔗糖受体反应，从而以高产率立体专一地合成了α构型的呋喃果糖苷。

Here we synthesize mesoporous titanosilicate MTS-9 and ferrisilicate MFS-9 by using zeolite TS-1 and FeS-1 seed solution as inorganic precursor respectively and triblock copolymer surfactant as template.

我们分别使用TS-1和FeS-1导向剂为无机原料，以三嵌段共聚化合物表面活性剂为模板，合成了钛硅介孔分子筛MTS-9和铁硅介孔分子筛MFS-9。

Here we synthesize mesoporous aluminosilicate MAS-7 and MAS-9 and titanosilicate MTS-9 by using Beta, ZSM-5 and TS-1zeolite seed solution as inorganic precursor respectively and triblock copolymer surfactant as template.

我们分别使用Beta ，ZSM-5和TS-1导向剂为无机原料，以三嵌段共聚化合物表面活性剂为模板，合成了硅铝介孔分子筛MAS-7和MAS-9，钛硅介孔分子筛MTS-9。

Therefore, the goal ofour work is to synthesize new microporous titanosilicates. A new titanosilicate with a high Si/Al molar ratio (named JLU-3, JilinUniversity No.3), has been synthesized hydrothermally by using Triethylamine astemplate in the SiO2-NaOH-TiO2 system.

鉴于含钛硅微孔材料多具有优良的氧化催化性能，其合成和性能研究一直为国际上的热点，我们把新型钛硅微孔材料开发作为研究方向。

The first step was to synthesize imidazoline. The mole ratio of oleic acid and diethylene triamine was 1:1.2, the xylene was 30%. Temperature was controlled in about 160 ℃ on this stage, timing for acylation reaction was about 1.5 hours.

第一步咪唑啉的合成：油酸和二乙烯三胺摩尔比为1：1.2，以二甲苯为携水剂，反应温度控制在160℃酰化反应1.5小时，然后升温至220℃环化反应，反应时间6.5小时。

A study was conducted to synthesize oligoester alcohol s from poly production wastes via transesterification with diethylene glycol and tribasic alcohol.

将涤纶废产物用二甘醇和三元醇经酯基转移合成齐聚酯多元醇，并用其制备聚氨酯硬质泡沫塑料。

While at Phase IV, with specific growth rate increasing, the carbon flux of PP decreased gradually, and the carbon flux of Tricarboxylic Acid Cycle, which providing enough precursors and energy to synthesize human-like collagen, decreased slightly with specific productivity of human-like collagen increasing.

在第Ⅲ阶段，随着比生长速率的增大，进入磷酸戊糖途径的碳流量先增大后减小，当比生长速率为0.15h~(-1)时达最大值，其次是0.20h~(-1)的，以合成足够的前体和NADPH满足细胞生长所需；在诱导后，随着比生长速率的增大，进入磷酸戊糖途径的碳流量逐渐减小，而进入三羧酸循环的碳流量随着类人胶原蛋白比产率的增大而稍有减小，以提供足够的前体和能量合成目标蛋白。

Methods Tetra-calcium phosphate was prepared by high heating, than imitated the internal situation of humanbody, for hydrolization and solidation,to synthesize the hydroxy-calcium phosphate,as artificial bone in sement-type ,then im-planteted them into the large segmental defect of radius of New Silan rabbits model. The implanted materials were taken out at 4th, 8th, 12th, and 16th weeks after implantation. The histological sections, with HE and Masson's trichromic staining made, to evaluate the effectiveness of repair of bony defect.

方法高温法制备出磷酸四钙，然后在模拟体内环境下将其与无水磷酸氢钙发生水化固化反应，合成水泥型羟基磷灰石人工骨，将自制的CPC人工骨植入新西兰兔桡骨大段骨缺损模型中，术后4、8、12、16周取材，采用HE染色和Masson三色染色分析评价骨缺损修复效果。

Methods Triethyl phosphite and ethyl chloroacetate were used as starting materials to synthesize pregabalin by Arbuzov reaction, Wittig-Horner reaction, Michael addition, reduction and resolution.

以亚磷酸三乙酯和氯乙酸乙酯为起始原料，经Arbuzov反应、Wittig-Horner反应、Michael加成、还原、拆分5步反应得到普瑞巴林。

We adopt a similar discotic liquid crystalline synthesis way to synthesize target molecules 7, 11, 15, 19, 21 in this article. The target molecules have a central triphenylene core and different side chains including triphenylamine derivatives and carbazole molecules. We observe these molecules optical and electrochemical properties and the effect of hole-transport layers in organic light emitting diode.

本篇论文的研究主旨是采用类似盘状液晶的合成方式，以三伸苯作为分子的核心，藉由改变不同的三苯胺及咔唑醚基侧链来合成目标化合物7、11、15、19、21，并观察分子的光学性质变化，电化学行为，以及作为电洞传输材料在有机电激发光元件上的效果。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。