查询词典 synthesis

The preparation method comprises monomer synthesis and polymer synthesis. The polymer synthesis is that cyclopentadienyl sodium monomer is added into metallic cobalt complex-triphenyl phosphorus cobalt chloride under strict oxygen-free and water-free conditions, and then double inner alkyne or outer alkyne conjugate monomer is added in, and after reaction, the precipitation, filtering, abstersion and vacuum-drying are carried out, the large molecules polymer containing cyclopentadienyl cobaltocenium organometallic cobalt is obtained.

制备方法，包括单体合成和聚合物的合成，聚合物的合成是在严格无氧无水条件下，在金属钴配合物三-三苯基磷氯化钴，加入环戊二烯钠单体，随后加入双内炔或双外炔共轭单体，反应后沉淀，过滤，洗涤，真空干燥，得到含环戊二烯茂钴有机金属钴的大分子聚合物。

In this paper, through a series of experiments, two series of quaternary-ammounium Gemini surfactants were synthesized, namely the pair alkylene double quaternary ammonium salt surfactant m-s-m·2Br and the pair the alkylene double quaternary ammonium salt surfactant -s-·2Br. We has carried on the attribute with the infrared spectrum to its structure, and to affected the factor which the synthesis pair the alkylene double quaternary ammonium salt surfactant responded to carry on the discussion. We has discovered the synthesis pair the ethylene double quaternary ammonium salt surfactant m-2-m·2Br optimum condition: The bromo alkane and a tetramethyl ethylene diamine mole of ratio is 3.0: 1.0, makes the solvent by the ethyl alcohol, 80℃ under responds for 48 hours in the backflow temperature; Synthesis pair alkylene double quaternary ammonium salt surfactant 12-S-12 ·2Br optimum condition: 12 tertiary amine and 1, 3- propylene dibromide (1, 4- two bromines butane) a mole of ratio is 2.2: 1.0, makes the solvent by the ethyl alcohol, responds for 48 hours in the constant temperature 80 ℃ under backflow.

本文通过一系列的实验，合成了两个系列的Gemini型表面活性剂，即双烷撑双季铵盐表面活性剂m-s-m·2Br和双烷撑双季铵盐表面活性剂-s-·2Br，用红外光谱对其结构进行了表征，并且对影响合成双烷撑双季铵盐表面活性剂反应的因素进行了讨论，找出了合成双乙撑双季铵盐表面活性剂m-2-m·2Br的最佳条件：溴代烷与四甲基乙二胺的摩尔比为3.0：1.0，以乙醇作溶剂，在回流温度80℃下反应48小时；合成双烷撑双季铵盐表面活性剂12-s-12·2Br的最佳条件：十二叔胺与1，3-二溴丙烷(1，4-二溴丁烷)摩尔比为2.2：1.0，以乙醇作溶剂，在恒温80℃下回流反应48小时。

On the basis of the introduction and analysis of the history, current situation and development of explosive synthesis of superhard materials, the mechanism and technology of diamond and dense boron nitride synthesis by shock compression and some explosive mechanics problem in explosive synthesis have been studied systematically in this research.

本文在对超硬材料爆炸合成研究的历史、现状及发展趋势进行评介、总结与分析的基础上，以金刚石、高密相氮化硼为研究对象，对爆炸合成理论与技术，以及爆炸合成中所涉及的一些爆炸力学理论问题进行了较为系统的研究。其主要研究成果如下

In my works , synthesis of the Jesus and the machine emphasize on the relationship of Mind body and religion ; synthesis of infant and machine means training mind will bring new birth and hope; the last synthesis through human figure and animal machine express that the mind want to shake off the yoke of the body that take along with the brutalism.

其中，耶稣与机器的结合着眼于这种身心状态与宗教的关系，而婴儿与机器的结合强调内心修炼将会带来人的新生和希望，野兽机器与人的结合则把灵魂隐喻为欲挣脱身体枷锁的人，而野兽机器则代表我们的身体和身体本身携带的兽性。

The study on soluble protein after eclosion when cantharidin synthesis is active in Mylabris calida Palla would help to clarify the synthesis mechanism of cantharidin and involved enzymes of the synthesis.

研究斑蝥素大量合成期的芫菁体内可溶性蛋白，有助于阐明斑蝥素合成相关酶蛋白的种类和合成机理。

Its commercial technologic processes and products,such as Acetic Acid Production by Carbonylation of Methanol,Formyl Morpholine,Steam Reforming Catalyst,Low Pressure Methanol Synthesis,Dimethyl Formamide Production by Dehydrogenation of Methanol,Dimethyl Ether Synthesis by Methanol Dehydration,Hydrogen Production by Methanol Cracking,Methanol Synthesis Catalyst,PSA Gas Separation Devices, and etc.,have been applied in more than 800 plants over fields including chemical industry,petrochemical,food, metallurgy,machinery,military industry.Many technological products were exported to American,European,Asian countries as well as Hong Kong,Macao and Taiwan.Remarkable economic and social benefits are achieved.

甲醇羰基化合成醋酸，甲酰吗啉，转化催化剂，低压合成甲醇，甲醇脱氢制二甲基甲酰胺，甲醇脱水制二甲醚，甲醇裂解制氢，合成甲醇催化剂，变压吸附制氢等成套工业装置和产品应用于全国800多家化工，石化，食品，冶金，机械，军工等企业，并出口美国，欧州，亚州等国及港，澳，台地区。

It was known that pyridine and Triton-x100 had a bad effect on the cell growth and lycopene production were studied. The results indicated that pyridine and triton-x100 inhibited cell growth and lycopene synthesis;β-ionone increased cell growth and lycopene synthesis when the concentration was 0.05 ml/L, but when the concentration became higher, there would be a decrease on the lycopene output; span-20 increased cell growth and lycopene synthesis effectively when the concentration reached 2.0ml/L, and the lycopene yield became 2.4×10~(-2) mg/L which was 3-fold than control.

研究了培养基中加入不同浓度的小分子效应物吡啶、Triton-x100、Span-20、β-紫罗酮、异烟肼对番茄红素产量的提高作用，结果显示培养基中加入很低浓度的吡啶(0.1ml／L)就会对菌体产生很强的毒害作用；triton-x100对类胡萝卜素的合成也有很强的抑制作用，试验的浓度为0.2ml／L到5ml／L，结果发现它对菌体的生长和番茄红素的合成都有抑制作用；β-紫罗酮在浓度为0.05ml／L时有很小的促进作用，而浓度升高就有了比较强的抑制效果；span-20在液体培养基中的加量为2.0ml／L时，对番茄红素的合成有很强的促进效果，产量达到了2.4×10~(-2)mg／L，比原始菌株产量提高了2倍，而浓度进一步增大就产生了很强的抑制效果。

Based on broad information collection, author compared and studied on the old synthesis process, and proposed the better process that started from benzyl chloride, then according to the sequence of " synthesis of benzylamine, synthesis of N-benzyl-N--acetamine, synthesis of 2-chloro-5-methylpridine ,2-chloro-5-trichloromethylpyridine,2-chloro-5-trifluropyridine " five steps to get the final product, CTFP.

本文在查阅大量文献资料和对2-氯-5-三氟甲基吡啶合成路线进行分析比较的基础上，提出了较佳合成路线，即以氯化苄为原料，合成的反应步骤为&苄胺&合成、&N-苄基-N--乙酰胺&合成、&2-氯-5-甲基吡啶&合成、&2-氯-5-三氯甲基吡啶&合成、&2-氯-5-三氟甲基吡啶&合成五步。

Production technology of synthesis of allantoin are reviewed, including glyoxal oxidation, electrochemical synthesis, calcium glyoxylate synthesis, dichloroacetic acid synthesis, ace-tochloral method, and oxidative decarboxylation.

评述了乙二醛氧化法、化学法、醛酸钙法、素三氯乙醛合成法、酸二氯乙酸法和尿酸氧化脱羧法等合成尿囊素的各种工艺。

Based on these, an improving μ-synthesis is presented, with which the high-purity distillation is designed well. 2. The robust performance problem of MIMO plant is explained with the plant direction angle, which shows that the robust performance varies with different input uncertainties and the μ-synthesis should be applied correctly according to the uncertainty structure. 3. Condition number and bandwidth are the important items for robust performance design in MIMO system. The H〓 two-block problems can not deal with the robust performance design of MIMO system because of the condition number cancellation. A general μ-synthesis procedure for MIMO system with uncertainties is presented. 4. For the SISO system, the object function in robust performance is amplified by at most 〓 than that of H〓 two-block problems in value: So the robust performance of SISO system can be done with the H〓 two-block problems to avoid the complicated μ-synthesis procedure. 5. All the conclusions and methods presented in this paper are demonstrated by some typical design examples.

从而形成一种改进的μ综合方去，并对精馏塔病态对象进行了鲁棒性能设计，得到令人满意的结果；（2）利用对象的方向角解释了MIMO对象鲁棒性能设计出现问题的原因，并提出不同输入摄动形式下系统的鲁棒性能问题也并不相同，因此利用μ综合处理鲁棒性能设计时，应根据不同的摄动情况采用不同的结构进行设计：（3）条件数问题和带宽问题是MIMO系统鲁棒性能设计的两个主要问题，指出由于条件数对消的存在使得一般H〓两块问题无法处理MIMO系统的鲁棒性能设计，而μ综合方法则是处理MIMO系统鲁棒性能设计的有效方法，并给出了其处理MIMO系统鲁棒性能设计的一般性方法；（4）提出对于SISO系统H〓两块问题（S/T问题、S/KS问题）的设计指标函数与鲁棒性能设计的μ指标函数在数值上最大差〓倍，因此对于一般SISO系统的鲁棒性能设计可以简单地用一般的H〓的两块问题处理，而避免μ综合设计的复杂过程；（5）本文中提出的结论和算法都利用H〓/μ发展中的典型例子：Doyle-Stein问题，Safonov的战斗机模型，精馏塔对象等进行了设计验证。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失