查询词典 synthesis method

This paper is studied on a new synthesis method of amino-modified organic silicone micro-emulsion of cationic style by one step with a silane-alkyl coupling,3-(2-aminoethyl)-aminopropyl methyl dimethoxy silane while opening-cyclo polymerization of the octa-methyl cyclo tetra siloxane,thus the optimal manufacturing conditions are determined by comparing test of their properties.

采用硅烷偶联剂氨乙基氨丙基甲基二甲氧基硅烷改性，八甲基环四硅氧烷开环聚合，探索一步合成阳离子型氨基改性有机硅微乳新方法，通过其性能测试得出其最佳工艺条件：反应温度：80℃，反应时间：3 h，十六烷基三甲基溴化铵用量：5%，脂肪醇聚氧乙烯醚用量：5%，预乳液滴加时间：2 h。

Using pure Ti and Ni powders, a promising artificial bone material, nearly equiatomic stoichiometry Ti-Ni shape memory alloys porosity was prepared by combustion synthesis method.

使用Ti、Ni纯元素粉末，用燃烧合成技术制取了近等原子比的多孔Ti-Ni形状记忆合金，一种理想的人造骨骼材料。

The compound 103-1 is investigated in synthesis method, structure analysis, herbicidal activity, crop safety and toxicological test.

第五章是对优选化合物进行系统研究，以明确优选化合物的实际应用前景。

The invention relates to a synthesis method of N-acetylaminoglucose, which comprises dissolving D-glucosamine hydrochlorate and alcohol at the mass ratio of 2-2.5:100, adjusting the pH value of the solution to 9-10, filtering, taking the filter liquor, mixing and adding acetic anhydride at the 50-60wt% amount of D-glucosamine hydrochlorate, mixing and reacting for 2h, using absolute ethyl alcohol to recrystallizing, filtering and recrystallizing via water, to obtain rod-shape food grade N-acetylaminoglucose.

本发明涉及一种N-乙酰氨基葡萄糖的合成方法。该方法的具体步骤为：将D-葡萄糖胺盐酸盐和乙醇按2～2.5∶100的质量比溶于水中，调节该溶液的pH值为9～10；过滤，取滤液，搅拌下加入乙酸酐，其加入量为原料D-葡萄糖胺盐酸盐量的50～60wt％；搅拌反应2小时后，用无水乙醇进行重结晶；过滤，晶体再用水重结晶，得棒状食品级N-乙酰氨基葡萄糖。

A new synthesis method of Taxane s was reported involving radicals generated from hypophosphorous acidn initiated by 2,2′-azobisisobutyronitrile.

由偶氮二异丁腈引发次磷酸产生次磷酸根自由基，以链式自由基反应机制脱除紫杉烷类化合物结构中的含氧基团，简单、高效地合成了紫杉烷。

A new synthesis method of Taxanes was reported involving radicals generated from hypophosphorous acid n initiated by 2,2′-azobisisobutyronitrile.

由偶氮二异丁腈引发次磷酸产生次磷酸根自由基，以链式自由基反应机制脱除紫杉烷类化合物结构中的含氧基团，简单、高效地合成了紫杉烷。

A new synthesis method of metal-free phthalocyanine using 1,3-diiminoiso- indoline as main material and trimethoxysilane as hydrogen donator was developed in this paper.

本文建立了以酞菁素为原料，喹啉为溶剂，三甲氧基硅烷为供氢剂，合成无金属酞菁的新方法。

In the paper, the multidentate carboxylic acid ligands were used to combine with Cd, resulting in the three dimensional MOCPs single crystals—C12H16CdN2O8, with a low temperature hydrothermal synthesis method. The sample was characterized with IR spectra to affirm the organic groups in the frameworks, single-crystal X-ray diffraction to determine the crystal structure and composition of the frameworks, N2 adsorption isotherms at low temperature to measure the specific surface area and pore size distribution, and with TGA/DGA analysis to scale the thermal stability. Furthermore, the dissolution property and the photocatalytic activity of MOCPs under the ultraviolet ray condition were explored.

本文用低温水热合成法，用多齿羧酸配体异烟酸和Cd配位合成出[Cd(C6H4O2N)2(H2O)4]∞三维晶体并进行了表征：采用红外光谱法确认骨架中的有机官能团；用单晶X射线衍射分析法测定MOCPs的晶体结构，并确定其骨架的组成；通过低温氮气吸附等温线测定了其比表面积和孔径分布；以热重分析和差热分析测定材料骨架的热稳定性；测定了晶体的溶解性能；最后以亚甲基蓝为目标降解物，对[Cd(C6H4O2N)2(H2O)4]∞的光催化活性及亚甲基蓝的氧化动力学进行了探索(来源：A2444BC论文网www.abclunwen.com)。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下：一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸；蒸馏NMP；干燥增溶剂；二、在氮气气氛下，Py与NMP混匀后加入密封的反应器中，再加入增溶剂，然后加入5-氨基-2-苯并唑，搅拌；三、在氮气气氛下，将步骤二的混合液搅拌并升温至50℃～150℃后加入脂肪族二酸，再加入TPP后缩聚；四、再倾入甲醇析出沉淀，过滤，清洗沉淀，再干燥；即得到含唑环半芳香聚酰胺。

During the process of imidacloprid preparation, using phosphorus pentachloride dehydration and greatly excess 2-nitroiminoimidazolidine, the yield may reach 90%, and the purity is over 95%, so this a fairly good synthesis method.

吡虫啉合成中用五氧化二磷脱水法和过量2-硝基亚氨基咪唑烷法收率接近90%，纯度达95%以上，是较佳的合成方法。

As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸，那乌黑、忧郁的眼睛，她便会相信，他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失