查询词典 synthesis method

In this paper, the preparations, analytical methods, physical characteristics of ferrates and the application of ferrates in the fields of synthesis of organic compounds, treatment of waste water and the usage as cathode material in alkaline batteries are summarized. The electrochemical preparation of sodium ferrate is described and the relationships between the main parameters in the process are deeply investigated. One method of in-situ electrosynthesizing potassium ferrate of high purity with both high efficiency and low energy consumption is invented. The cyclic voltammogram and feature characterization of iron anode in alkaline solutions is studied. One preparation method of ex-situ electrosynthesizing tripotassium sodium ferrate of high purity is created.

本文概述了高铁化合物的制备方法、分析方法、物理化学性质及其在氧化合成有机物、水处理和用作碱性电池正极材料等领域的应用；深入系统地研究了高铁酸钠的电化学制备及其影响参数之间的关系；研发了一种高效率低能耗直接电合成高纯度高铁酸钾的工艺方法；探讨了铁电极在浓的苛性碱溶液中的循环伏安特征及其极化特征；研发了一种电化学制备高铁酸三钾钠的工艺方法并用多种现代分析测试技术对K_3Na(FeO_4，)_2进行了表征。

This article arbitrates the legal regime take the Sino-US negotiable securities dispute as the object of study, the union legal science and the finance study knowledge, synthesis utilization methods and so on comparison analytic method, historical analytic method and law explanation study, in arbitrates the system to our country negotiable securities dispute to carry on the thorough analysis in the foundation, absorbed the American negotiable securities dispute to arbitrate the system and the related suggestion, discussed the construction perfect negotiable securities dispute to arbitrate each main system which with emphasis the legal framework needed, and arbitrated the legal regime to our country present negotiable securities dispute to carry on the analysis, then put forward the improvement proposal.

本文以中美证券纠纷仲裁法律制度为研究对象，结合法学和金融学的知识，综合运用比较分析法、历史分析法和法解释学等方法，在对我国证券纠纷仲裁制度进行深入分析的基础上，吸收了美国证券纠纷仲裁制度和相关建议，重点探讨了构建完善的证券纠纷仲裁法律体系所需的各主要制度，并对我国目前的证券纠纷仲裁法律制度进行分析，进而提出改进的建议。

Finally through to the GMRY crisis management present situation analysis and the company interior crisis cause based on the strategic stratification plane and the operation stratification plane two stratification planes, launches the strategic stratification plane and the operation stratification plane research from the management study basic strategy management process frame and the balance idea branch customs station frame to the GMRY enterprise crisis cause, and the method which using the subjective tax power and the objective tax power, qualitative and the quota unifies determined the target the weight, unifies using the level analytic method and the fuzzy synthesis judgment law then constructs the GMRY crisis to forewarn the distinction model, and forewarns the analysis system through the enterprise crisis, surveys crisis condition which GMRY at present locates, And proposed the crisis forewarns the solution and the implementation enterprise crisis early warning system measure and the suggestion.

最后通过对GMRY公司危机管理现状的分析及公司内部危机诱因基于战略层面及运营层面的两个层面，从管理学基本的战略管理过程框架和平衡计分卡框架对GMRY公司企业危机诱因展开战略层面与运营层面的研究，并运用主观赋权和客观赋权、定性与定量相结合的方法确定出指标的权重，运用层次分析法及模糊综合评判法相结合进而构建出GMRY公司危机预警判别模型，并通过企业危机预警分析系统，测算出GMRY公司目前所处的危机状态，并提出危机预警解决方案和实施企业危机预警系统的措施和建议。

According to the Box-Benhnken design principle,the method of response surface method with 3 factors and 3 levels was used. The factors influencing the technological parameters were determined by means of regression analysis. Response surfaces were finally graphed with the yield as the response value. The synthesis conditions were optimized as follows:reaction reagent was NBS,stoichiometric proportion between NBS and anhydrovinblastine was 1.07; the dosage of TFA was 22 mL/L; reaction temperature was －68 ℃ and duration was 90 min.

在单因素实验基础上，根据Box-Benhnken实验设计原理，采用三因素三水平的响应面分析法，研究了各个因素及其交互作用后，得到了合成7′-Br-脱水长春碱的最佳工艺条件：以二氯甲烷为溶剂，采用NBS为溴代剂，其用量与底物的物质的量比为1.07∶1，TFA的加入量22 mL/L，在－68 ℃下反应90 min，终止反应后，得到卤代产物。

Two methods were used to prepare small functional peptides. One is synthesis with enzymatic method. Another is the method of hydrolyzing protein with enzyme.

对功能短肽的合成方法进行了探索，从合成与蛋白水解两种途径制备了功能短肽。

Study on the Synthesis of the Stage-2 FeCl_3- GIC Using the Mixing Method;2. In this article, ternary GIC FeCl3-ZnCl2- GIC is synthesized by molted salt method.

采用混合熔盐法，合成出不同阶结构的石墨层间化合物 FeCl3-ZnCl2-GIC，应用XRD、SEM、EDS对产物的晶体结构、表面形貌及元素组成进行表征，并测试其电导率。

And precipitation rate of vanadium was higher than 98.5%. Five vanadium catalysts were made withγ-Al_2O_3 and the mesoporous molecular sieve MCM-41 as carrier, and were made by dipping method, intermingle process and functionalizing method respectively. The characterization of their pore size, crystal structure, specific surface area and V_2O_5 load of catalysts were studied by XRD, the adsorption /desorption of N_2 technique, Raman spectroscopy and XRF. The activities of the catalysts estimated by the synthesis of DPC with DMC and phenol.

钒催化剂的制备与表征及活性评价：是分别以γ-Al_2O_3和介孔分子筛为载体，采用浸渍法，掺杂法及官能化法制备了5种钒催化剂；分别对其进行了XRD分析、N_2吸附-脱附分析、红外光谱分析和荧光分析，对其孔径、晶型结构、比表面积和V_2O_5负载量进行了表征；以碳酸二甲酯和苯酚的酯交换合成碳酸二苯酯的典型反应为依据，对钒催化剂进行了活性评价。

The method described here proved to be an effective, practical method for the synthesis of these three Saponins and other analogs.

这是一个有效、实用的合成这一类皂甙的通用方法。

It has been a long history in the synthesis of amorphous metal borides and phosphides materials by using the electroless deposition method. This method is efficient, low cost and convenient for the deposition of the amorphous as well as crystalline metal-metalloid materials.

用化学镀方法制备硼化物和磷化物的非晶态合金材料由来已久，是一种高效、低耗的简易制备方法。

Therefore the method of synthesis ethers is a potential method to pretectalcohols.

因此在本实验中，这种新的合成溴代醚的方法是一种潜在的醇保护的新方法。

Nowadays, most of research are to build a transmutative Petri Nets through adding controlling place sets, controlling arc sets and controlling policy to the basic Petri Nets, while the Controlled Petri Nets could be used to argue many controlling theory problems conveniently and to induce many logically and physically supervisory and solve the Event Feedback Controlling Problems and State Feedback Controlling Problem in DEDS supervisory theory.

目前大多数的研究表现为在变形后的受控Petri网基础上，利用各种方法求得各种逻辑型、结构型控制器，解决DEDS监控理论中的事件反馈控制问题与状态反馈控制问题。

On one hand, there are discussions with the works council and union about extension of short time working up to the end of September.

一方面，有讨论，工程理事会和联盟关于延长工作时间短至9月底。