查询词典 synthesis method

The computational complexity has been reduced about 5 times over against the original one. Moreover, the interpolation and quantization processing of CW is more reasonable; 2. A secondary power normalization algorithm is proposed in this dissertation. This normalization algorithm ensures that the energy sum of SEW and REW is 1. So, the energy ratio of SEW and REW can be achieved only by using SEW energy. This ratio is applied in REW quantization and CW composition; 3. For more efficient quantization for Slowly Evolving Waveform magnitude, Rapidly Evolving Waveform magnitude and power parameters, firstly, by applying the Equivalent Rectangular Bandwidth theory, classifiable multi-codebooks method, analysis-by-synthesis approach and so on, a predictive AbS multi-codebooks SEW magnitude quantization scheme is proposed. In the scheme, pitch information is exploited to determine which codebook is searched; secondly, for REW magnitude quantization, this dissertation proposed a DCT-matrix multi-codebooks quantization scheme. The classification in muti-codebooks is based on pitch and quantized SEW power. The multi-codebooks structure may offer more the information in quantization and solve the problem of the bit requirement limits in quantization by consuming some extra storage space; Furthermore, for the switch quantization of CW gain, a new classified parameter is proposed.

本文的主要贡献体现为如下几方面：一、为了减少WI模型的计算复杂度，提出了基于快速傅立叶变换、三次B样条插值和周期延拓技术的特征波形(Characteristic Waveform，CW)表示和对齐的快速算法，与原方法相比，计算量下降到原方法的1/5，同时也使得CW在插值和量化时更合理；二、为了严格保证SEW与REW的能量和为1，提出了一种特征波形的二次功率归一化算法，仅需要SEW能量就可以算出二者的能量比，并可应用到后续的REW的分类量化和CW合成中；三、为了对慢渐变波形(Slowly Evolving Waveform，SEW)幅度、快渐变波形(Rapidly Evolving Waveform，REW)幅度和特征波形功率进行有效量化，本文首先采用临界频带理论、分析合成技术、感觉加权技术以及预测式矢量量化技术，提出了一种基于基音周期分类的SEW分析合成预测式多码书量化方法；其次，本文根据基音和量化后SEW的功率信息对REW幅度进行分类，提出了一种基于离散余弦变换的REW矩阵多码书量化方法。

Synthesis of Antidote of N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane BI Hong-mei, ZHANG Jin-yan, LIANG Ying, SHEN Yong (College of Arts and Sciences Heilongjiang August First Reclamation University, Daqing 163319, Heilongjiang, China) Abstract: N-Dichloroacetyl-2-methyl-1-oxa-4-aza-spiro-4.4-nonane was synthesized by one pot method with isopropanolamine, cyclopentanone and dichloroacetyl chloride. The optimum reaction conditions obtained are as follows:the proportion in moles of the above materials is 1∶1∶1.2, reaction solvent is toluene, reaction temperature is -15 to -10 ℃,reaction time is 3 h, under the optimum condition, the yield of the compound is 50.0%.

除草剂解毒剂N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷的合成毕洪梅，张金艳，梁英，沈勇(黑龙江八一农垦大学文理学院，黑龙江大庆 163319)摘要：以33%的氢氧化钠水溶液为缚酸剂，异丙醇胺、环戊酮和二氯乙酰氯为原料，采用&一锅法&合成了N-二氯乙酰基-2-甲基-1-氧杂-4-氮杂-螺[4.4]壬烷，采用正交实验法得到最佳反应条件：反应原料摩尔比为1∶1∶1.2，苯作溶剂，反应的温度为-15 ℃~-10 ℃，搅拌时间为3 h，产率达到50.0%。

In the third part of this paper, a facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

对肼基苯磺酸是由对氨基苯磺酸经亚硝酸钠重氮化得到的重氮盐用亚硫酸氢钠还原、水解、硫酸酸化制得，本文经多次实验确定了反应原料、用量及反应条件，得到的产品纯度好，产率高。

A facile method is presented for synthesis of malonaldehyde dianil from propargyl alcohol by oxidizing using chromium trioxide and addition reaction with aniline.

以丙炔醇为原料，经三氧化铬氧化生成丙炔醛后，直接与苯胺反应简便地合成了β-苯胺基丙烯醛缩苯胺。

The method simplifies the synthesis process of 4, 4'-dihydroxy enterolactone, widens the pharmaceutical applications of arctiin, and provides a new healthcare food for preventing and treating climacteric syndrome, osteoporosis, hyperlipemia, breast cancer and endometritis.

本发明简化了化学合成4，4′-二羟基肠内酯的步骤，同时也为扩大牛蒡苷的药用范围，提高它的药用价值提供了新途径；也为预防和治疗更年期综合征、骨质疏松、血脂升高，乳腺癌、子宫内膜炎等提供了一种新的保健产品。

On the other hand, a method for the synthesis of-vinyl chalcogenides by the coupling of vinyl bromides with thiols or diphenyl diselenide using copper salts as catalysts in ionic liquids based on amino acids also has been described. The ionic liquids play multiple roles in the reaction: they act as solvent, base, and excellent promoter for the copper-catalyzed coupling reactions.

在新型的氨基酸负离子的离子液体中，开发了一个亚铜盐催化的Z-型溴代烯烃与硫族元素的交叉偶联反应，为立体选择性的制备Z-型烯基硫醚或烯基硒醚类化合物提供了一个新的方法；在此反应体系中，离子液体不仅起到了反应溶剂的作用，而且还起到了金属催化剂的配体和中和反应副产物的碱的作用。

The first part of this dissertation described a new effective method for asymmetric synthesis of,α,α-disubstituted amino acids from the asymmetric Strecker reaction products of aldehydes.

在本论文的第一部分，我们开发了一条以醛为原料，以不对称Strecker反应和不对称烷基化为关键步骤的合成α，α双取代氨基酸的有效方法，并对其立体选择性结果进行了机理探讨。

Synthesis of dodecyl polyglucoside by means of exchange method was studied.

摘 要：采用交换法合成十二烷基葡萄糖苷，考察了催化剂、醇糖比、反应时间、反应温度及脱醇工艺等对反应结果的影响。

According to the characteristics of the electrocatalysis synthesis process, and based on the causes of ionic membrane pollution, a kind of effective cleaning method in-situ of polluted membrane was presented.

根据电催化合成过程特点，从离子膜被污染的原因分析入手，提出了有效的污染膜原位清洗法。

Aim at twelve-bar kinematic chain with single joints,it combines topological graphs analysis with structure principle of mechanisms and method of innovative synthesis of epicyclic gear trains.

在将单铰运动链用于周转轮系创新综合方法的过程中，针对十二杆单铰运动链，将拓扑图分析和周转轮系创新综合的结构学原理及方法结合，得到了由十二杆单铰运动链生成的新型周转轮系的结构原型。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。