查询词典 synthesis method

Macroporous tributyl amine aminating strongly basic anion exchange resin-a phase transfer catalyst with high catalytic activity for nucleophilic substitution,which was screened out via combinatorial chemistry method –was used to catalyze the nucleophilic substitution reactions for synthesis of benzyl acetate,benzyl propionate,benzyl butyrate and benzyl valerate.

用组合化学方法筛选出的对无外加碱条件下的亲核取代催化活性最高的聚合物季铵盐–三丁胺胺化强碱性阴离子交换树脂为相转移催化剂，催化合成了乙酸苄酯、丙酸苄酯、丁酸苄酯、戊酸苄酯等羧酸苄酯。

DATA SYNTHESIS: Diabetes had been seriously threatening human health, and islet cell transplantation was a possible method that could cure the diabetes, however there was not enough islet resource so that people started to look for other vicariousness resource of islet cells.

资料综合：糖尿病是严重威胁人类健康的疾病之一，胰岛细胞移植是治愈糖尿病的可能方法，但由于胰岛细胞数量有限，不能满足临床需要，人们开始寻找胰岛细胞的可替代资源。

Using the method of record on spot, the thrust correlation data to the construction process are recorded, the analysis have indicated that the jacking force have complex influence factors, basically assumed the linearity with the pipe distance; The synthesis friction coefficient jumps to a peak value from zero at the beginning section, then gradually drops until stabilizes to a lower level and keep to the end.

分析表明顶力影响因素复杂，与顶距基本呈线性递增关系；综合摩擦系数从出洞时的剧增到一峰值，逐渐下降直至稳定到一较低的水平直至进洞结束；顶管施工对上层土体的扰动是明显的，须采取有效的措施进行监测和预防其破坏程度过大。

Imino-1, 3-thiazetidines is the basic structure of a kind ofbioactive herbicide and insecticide. Our method has advantage in synthesis highly substituted2-imino-1, 3-thiazetidines, therefore it has practical value to some extent. We also researched the reactions catalyze by active zinc dust.

提供了成四员噻吖丁啶杂环衍生物的方法。2-亚胺基-1，3-噻吖丁啶是一类具有生物活性的除草剂及杀虫剂的核心结构，我们的方法在合成多取代的2-亚胺基-1，3-噻吖丁啶方面有一定的优越性，从而具有一定的实用价值本文另一部分的工作是探讨锌粉催化的反应。

Cancers and hypertension and infection Another natural method of controlling proteinase activity is the synthesis of an inactive form of the enzyme, the zymogen.

自然界中另一个控制蛋白酶活性的方法是合成出酶的一种非活性形式，即酶原。

Objective To determine the contents of residual acetone in acetoacetic ester,the raw material for the synthesis of Edaravone, by gas chromatography.Methods Sample solution was injected on a GDX column (0.18 mm～0.25 mm) with nitrogen as the carrier gas.The residue was calculated by the external standard method.

摘要］ 目的：用气相色谱法测定依达拉奉合成起始原料乙酰乙酸乙酯中丙酮的残留量方法：采用固定相二乙烯苯乙基乙烯苯型高分子孔小球（直径为0.18 mm～0.25 mm），氮气为载气，用外标法测定乙酰乙酸乙酯中残留丙酮的含量。

Different aspects associating the DMAE-NHS-based CLIA were studied in this thesis,including synthesis of acridinium ester,chemiluminescent characteristics of DMAE-NHS,labelling antibody or streptavidin with DMAE-NHS,two-site sandwich chemiluminescent immunoassay for TSH,two-site sandwich chemiluminescent immunoassay involved biotin-streptavidin system for TSH,and competitive chemiluminescent immunoassay using biotin-streptavidin system for TLVThe desired acridinium ester,DMAE-NHS,was synthesized according to the reference method with some modifications.

目前国内尚未见有关DMAE·NHS的合成及其应用于CLIA的研究报导，本论文研究了吖啶酯DMAE·NHS的有机合成方法，DMAE·NHS的发光性能，DMAE·NHS及其与抗体偶联物的热稳定性，DMAE·NHS标记TSH单克隆抗体和链亲和素，TSH CLIA，TSH BAS-CLIA和TT_4 BAS-CLIA。

The invention relates to the synthesis of N-aryl group-3-(4-Beta-D-pyran allose glycoside phenyl)-5-formyl isoxazole-4-formamide and discloses a helicid derivative which can improve the functions of a central nervous system and the preparation method thereof; wherein, the compound has good sedative, hypnotic and anti-convulsant effects and is taken in the 2000 edition Chinese Pharmacopoeia with the drug name of helicid tablets.

N-芳基-3-(4-β-D-吡喃阿洛糖苷苯基)-5-甲酰基异唑-4-甲酰胺的合成，发明公开了具有改善中枢神经系统功能的豆腐果苷类衍生物，及其制备方法。该类化合物具有良好的镇静、安眠、抗惊厥作用。目前已以药品名&神衰果素片&被收入2000年版《中国药典》。

Peptide synthesis. PMAP-23 peptide was synthesized by the solid phase method using Fmoc(9-fluorenyl-methoxycarbonyl)-chemistry.Rink Amide 4-methyl benz hydrylamine resin (0.55mmol/g) was used as the support to obtain a C-terminal amidate peptide.

多肽合成。萨夫- 23肽合成固相法芴-化学 try.rink 酰胺4 -甲基奔驰hydrylamine树脂( 0.55mmol /克)，被用来作为支持以获得一个c端酰胺肽。

Glycogen synthesis of the cells was examined by the anthrone method.

将HepG2细胞置于10-7 mol/L 的胰岛素培养基中培养24 h，建立胰岛素抵抗细胞模型。

And Pharaoh spoke to Joseph, saying, Your father and your brothers have come to you.

47：5 法老对约瑟说，你父亲和你弟兄们到你这里来了。

Additionally, the approximate flattening of surface strip using lines linking midpoints on perpendicular lines between geodesic curves and the unconditional extreme value method are discussed.

提出了用测地线方程、曲面上两点间短程线来计算膜结构曲面测地线的方法，同时，采用测地线间垂线的中点连线和用无约束极值法进行空间条状曲面近似展开的分析。