查询词典 sulfur chloride

Highly ordered mesoporous Zr-Ce-SBA-15 silica with hexagonal-platelet morphology was synthesized through a hydrothermal route by using pluronic P123 as a template, tetraethyl orthosilicate as a silica source, zirconyl chloride and cerous nitrate as a precursor. The main strategy of this method was to utilize the acidity self-generated from the hydrolysis of inorganic salts in the aqueous solutions, where no addition of mineral acids was necessary.

以P123为模板剂，正硅酸乙酯为硅源，氯化氧锆和硝酸亚铈为无机前驱盐，在不外加无机酸的条件下，利用无机前驱盐自身水解产生的弱酸性环境，通过水热合成路线一步合成了具有大的径轴比、短孔道、六方板状形貌的Zr-Ce-SBA-15介孔材料。

Determination of Phosphate, Chloride and Sulfate in Heteropoly Acid by Zwitterion Eluent

杂多酸是一种理想的催化剂载体［1，2］。

The results were as follows:(1) The method that HA was treated by ethanol of 2.5x volume for 20 hours turned out to be the most economic and efficient.(2) Zymolysis combined with deproteinization by chloroform was better than deproteinization by chloroform for several times in yield and purity of HA.(3) HA with purity of 71.1 60/o was obtained by the fermentation with cetylpyridinium chloride.

本文对发酵液中HA的分离提取方法进行对比研究，结果表明采用2.5倍体积的乙醇对HA沉淀，作用时间20小时最为经济合理；采用酶解结合氯仿除蛋白较之氯仿除蛋白，HA的产量和纯度均有所提高；经氯代十六烷基吡啶分级分离后，可得纯度为71.16％的HA产品。

METHODS The rats were abdominally injected with sodium chloride solution of gadoloside 15 mg·kg -1 ·d -1 for 30 days.

分别给各组大鼠按 15mg·kg- 1 ·d- 1 ip红景天苷氯化钠溶液。饲养 30d后，断头处死。

The optimum reaction conditions were as follows: rosin 5 g, m: in: m 1:2:2, palladium chloride 0.090 %, n: n1:10, hydrogen pressure 5 MPa, reaction temperature 160℃ reaction time 3 h, mass fraction of abietic acid could be under 1%, mass fraction of dehydroabietic acid was 5.6%, which conforms to the national standards. The regeneration of catalyst was investigated. After cycling five times, the product of hydrogenated rosin still conforms to the national standards without any treatment of catalyst.

在松香5g、m：m：m1：2：2、氯化钯0.090%、n：nl：10、氢气压力5MPa，反应温度160℃，反应时间3h的较佳工艺条件下，产物氢化松香中极酸的质量分数小于1%，去氢枞酸的质量分数5.6%，符合GB/T 14020-2006国家标准；并对催化剂的重复使用性能进行了考察，催化剂相不经过处理直接重复使用5次后，产品氢化松香仍然符合国家标准中关于枞酸和去氢枞酸的指标要求。

Benzaldehyde 1, 2-propylene acetalization was carried out with benzaldehyde and 1, 2-propylene alcohol in the presence of polyaniline doped with ferric chloride.

在以苯甲醛和1，2-丙二醇为原料合成苯甲醛1，2-丙二醇缩醛的反应中，探讨了PAn-FeCl3催化剂对缩醛反应的催化活性。

Benzaldehyde 1,2-propylene acetalization was synthesized from benzaldehyde and 1,2-propylene alcohol in the presence of polyaniline doped with copper chloride.

缩醛是一类重要化合物，具有原料来源丰富、生产工艺简单、化学性质稳定等优点，近20年来作为新型香料在日用香精和食品香精中均有广泛应用[1-2]。

A series of p-toluene sulfonylamido acetacylhydrazone derivatives were synthesized from p-toluenesulfonyl chloride which reacted with glycine to get the intermediate p-toluene sulfonylamido glycine, then through the esterification, hydrazinolysis to afford another intermediate p-toluene sulfonylamido acethydrazide, which condensed with different aldehydes to obtain the target compounds that were characterized by IR, 1H NMR, 13C NMR spectra and elemental analysis.

魏太保 ；冷艳丽；王永成；张建辉；张有明*摘要：以对甲苯磺酰氯为原料，通过与氨基乙酸反应得到中间体对甲苯磺酰氨基乙酸，再经酯化、肼解得到对甲苯磺酰氨基乙酰肼，然后与相应的醛缩合得一系列对甲苯磺酰胺基乙酰腙类化合物。其结构经元素分析， IR， 1H NMR和13C NMR确证。

After the diazotization ,2-aminophenol-4-(2-'carboxy)sulfanil phenylamine was coupled with acetoacetanilide,2-naphthol,1-phenyl-3-methyl-5-pyrazolone,1-naphthol-4-sulfonic acid,separately to get the different diazotized compounds,then complexed with potassium chromium sulfate or cobaltous chloride to obtain the yellow,orange,red,purple,blue and other colour dyestuffs.

2-氨基苯酚-4-(2'-羧基)磺酰苯胺重氮化，分别与乙酰乙酰苯胺、2—萘酚、1-苯基-3-甲基-5-吡唑啉酮、尼文酸、1-乙酰氨基-7-萘酚等偶合，得到不同的偶氮化合物，然后分别与硫酸铬或氯化钴进行络合反应，得到黄、橙、红、紫、蓝多种颜色染料，并进行了毛织品的染色实验。

The result indicated that manganese chloride,acetylacetone,sodium hydroxide,were grinded for 15 mins at room temperature with the molar ratio of 1∶4∶1.8,the yield of manganese ac...

结果表明：氯化锰、乙酰丙酮、固体NaOH按1∶4∶1.8的摩尔比，在室温下研磨15 min所得产率最高，产率为68%，比传统液相法的产率(25%)高出43%。

This was not understood at the time, and therefore went unaddressed, until ascension became so distorted that we chose to stop ascending and wait for a time when all records would be revealed.

这在当时没有被了解，因此进行着无改编，直到提升变得如此扭曲，我们选择去停止提升并等待所有记录能被揭示的那一天。

The attack＇s nuisance value is increased because mobile phone networks also send notifications of new voicemail by sms,so an attacked phone may stop advising of new voice messages too,it warned.

它警告：这种攻击的危害增长是因为移动电话网络也会通过短信发送新语音邮件的通知。所以受到攻击的手机可也以停止新的语音信息的提示。