查询词典 sulfur chloride

Chloride by the acid and inorganic acid chloride, such as phosphorus trichloride, phosphorus pentachloride, thionyl acyl chloride (SOCl2) the role of the system was.

酰氯可由羧酸与无机酸的酰氯，如三氯化磷，五氯化磷，亚硫酰氯（SOCl2）作用制得。

Take the sodium silicate,the ferric chloride and the aluminum chloride prepared the high stability as the raw material research to polysilicate aluminum ferrite chloride.

以水玻璃，氯化铁和氯化铝为原料研究制备了高稳定性聚硅酸氯化铁铝。

As a key step of the synthesis, the Friedel-crafts acylation was researched. And the optimal operation variables were determined through orthogonal experiment: when 0.lmol acetanilide, 0.26mol aluminum chloride, 0.12mol propionyl chloride and 200ml carbon disulfide are introduced, and the reaction time is 5 hour, the yield can be up to 57.3%. The solid super acid catalyst was preliminary studied. Four solid super acid catalysts were prepared to take the place of aluminum chloride, and it was indicated that AlCl3 acidic resin can better catalyze the Friedel-Crafts reaction of acetanilide.

对合成路线中的Friedel-Crafts酰基化反应进行了研究，运用正交实验设计确定了最佳工艺条件：当乙酰苯胺用量为0.1mol时，AlCl_3用量为0.26mol、丙酰氯用量为0.12mol、溶剂用量为200ml、反应时间为5h，产率可达到57.3％；对于固体超强酸催化剂进行了初步研究，合成了四种催化剂，其中负载AlCl_3强酸性树脂对于乙酰苯胺的Friedel-Crafts酰基化具有一定的催化活性。

Our company specializes in operating plating materials: sulfamic acid nickel, nickel sulphate, nickel chloride, nickel carbonate, etc.; environmentally friendly sewage treatment materials: polyacrylamide, polypropylene acid sodium, ferrous sulfate, etc.; washing cleaning materials: OP - 10, TX-10, NP-9, K-12, JFC, sodium carboxymethyl cellulose, etc.; cosmetic raw materials: Triclosan, Resorcinol, stearic acid and so on, basic chemical raw materials: Industrial salt, soda ash industrial ammonium chloride, ammonium chloride agriculture, Sodium Sulfate, Sodium Molybdate, Ammonium Molybdate, as well as chemical products such as UV-absorbers.

本公司专业经营电镀原料：氨基磺酸镍，硫酸镍，氯化镍，碳酸镍等；环保污水处理原料：聚丙烯酰胺，聚丙烯酰钠，硫酸亚铁等；洗涤清洗原料：OP-10，TX-10，NP-9，K-12，JFC，羧甲基纤维素钠等；化妆品原料：三氯生，间苯二酚，硬脂酸等，基础化工原料：工业盐，纯碱，工业氯化铵，农业氯化铵，元明粉，钼酸钠，钼酸铵等以及紫外线吸收剂等化工产品。

The hydrophobic monomers such as glycidyl octyl dimethylammonium chloride, glycidyl dodecyl dimethylammonium chloride, glycidyl tetradecyl dimethylammonium chloride was applied to the hydrophobic modification of two kinds of sodium cellulose sulfate in isopropyl alcohol under 65℃.The success of synthesis of a kind of novel amphoteric surfactant by FT-IR and NMR. 3. By the measuring surface tension of all kinds of amphoteric polymeric surfactants based on cellulose, the critic micelle concentration was obtained such as 0.4wt%、0.3wt%、0.25wt% and corresponding surface tension was about 30mN/m

通过动态接触角测量仪确定了各种纤维素表面活性剂的表面张力和临界胶束浓度，结果表明该类表面活性剂可与小分子表面活性剂的降低表面张力的能力相媲美，最低可达28.41 mN/m，随着疏水基中碳链的增长，降低表面张力的能力下降，而临界胶束浓度从0.4wt%相应降低0.25wt%；应用环境扫描电镜确定其不同浓度胶束形态，结果表明在较低浓度下形成棒状单分子胶束，随着浓度的升高，单分子胶束逐渐聚集成树枝状胶束，进一步提高浓度，则聚集成网状结构；此外，采用了高级流变仪对其溶液的流变性质进行了研究，结果表明其溶液属于剪切变稀流体，是高分子溶液特有的性质。

At last,a convergent and general protocol to marine natural product,as demonstrated by the enantioselective total synthesis of malyngamides O,P,Q,R, 5"-epi-Q and 5"-epi-R bearing terminal vinylic chloride structure,was developed in detail.E,(7S)-7-methoxytetradec-4-enoic acid was prepared using the above described Johnson-Clainsen rearrangement,the terminal vinyl chloride was constructed using Wittig reaction as key step,the pyrrolidone derivative was constructed using L-serine as natural chiral pool.Starting from the synthesis of malyngamides O and P to explore the general route,an aldol reaction of methyl acetate with the vinyl chloride part in the presence of LDA gave the skeleton of amine portion,followed by amidation with the fatty acid finished the synthesis of malyngamide P.

先以malyngamides O和P为试点探索通用合成路线，将乙酸甲酯和烯氯部分在LDA存在下进行aldol反应得到氨部分的骨架，再将手性不饱和脂肪酸和氨部分进行酰胺化反应完成了malyngamide P的合成，将P在碱性条件下进行烯醇甲基化反应完成了malyngamide O的全合成。

The paper reviews the experimental results of chloride permeability of reinforced concrete cover based on ASTM C1202,and states that the resistance of ordinary marine concrete against chloride penetration is poor and the performance of concrete against chloride penetration can be remarkably improved by admixing with silica fume .

描述了按A STM C 1202方法试验研究保护层混凝土的氯离子渗透性能，指出以往普通港工混凝土的抗氯离子渗透性能较低，而掺入硅灰能显著提高混凝土的抗氯离子渗透性能。

The HPLC method has been used to investigate the stability of etimicin in 0.9% sodium chloride, 5% glucose, 10% glucose, compound sodium chloride, glucose sodium chloride and so on. In the experiment, the ODS-C18 column (4.6mm×250mm), mobile phase: methanol/water/acetic acid=80/16/4 (containing heptane sulfonic sodium 0.02mol/L), UV detection with wavelength of 330nm were employed. After integrating each of the menstruums with etimicin, the content and pH value were measured after 1h, 2h, 4h, 6h and 8h at a temperature of 17, 25 and 35℃, respectively.

实验采用HPLC法，以C18柱为色谱柱，CH3OH：H2O：HAc=80：16：4（含0.02mol/L庚烷磺酸钠）为流动相，检测波长330nm；对依替米星在生理盐水，5%葡萄糖，10%葡萄糖，复方氯化钠，葡萄糖氯化钠等溶媒中进行了稳定性研究，在室温(17℃)，25℃，35℃情况下，将依替米星与不同的溶媒配伍后，在1h，2h，4h，6h，8h分别测定它们的含量及pH值。

Part I, the Friedel-Crafts acylation on DAA and methyl dehydroabietic acid was carried out with acetyl chloride, benzoyl chloride or phthalic anhydride as acylating regents, anh- ydrous aluminum chloride as catalyst and with different solvents to compare with, we have got t- hree new compounds.

第一部分，分别以脱氢松香酸和脱氢松香酸甲酯为底物，乙酰氯、苯甲酰氯、邻苯二甲酸酐为酰化试剂，无水三氯化铝作催化剂，采用不同的溶剂及反应条件进行傅克酰基化反应，得到3个新化合物。

Ba0.7Sr0.3TiO3 powders are successfully prepared by the hydrothermal process where barium chloride, strontium chloride and titanium chloride are used as raw materials at 240℃ for 10 hours.

利用水热法研究了BST前驱物的初始配比、矿化剂NaOH过量浓度、水热时间和温度等条件对合成Ba0.7Sr0.3TiO3粉体的影响。

He paid $5,000 for this cupcake.

他我这个纸杯蛋糕花了5000美元。

I mean, if you want to, that is

我的意思是，如果你们想吃的话。