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The kinetics of discomposing reaction of LiNiO〓 is also studied. LiNiO〓 is modified by adding small quantity of additives. The performance of derivatives of LiNiO〓, in which Ni was partially substituted with Co, Mn and Ti is also studied.

利用加入少量添加剂的办法对LiNiO〓进行了改性，本论文还研究了用Co、Mn、Ti部分替代Ni制备的LiNiO〓系列派生物的结构、性能和充放电反应机理。

Chapter 1: The reactions of methylenecyclopropanes with phenylsulfenyl chloride or phenylselenyl chloride give cyclobutene derivatives along with ring-opened products in good total yields at 0 °C in various solvents. The reactions of methylenecyclopropanes with diphenyl diselenide give the di-phenylselenyl substituted ring-opening products which can be transformed to 2,5-dihydrofuran derivatives under the oxidation with hydrogen peroxide at room temperature.

在第一章中，我们发现亚甲基环丙烷类化合物在0℃时即可很快与苯硫氯或苯硒氯发生反应生成取代环丁烯类化合物和正常的开环产物；而与二苯基二硒的反应则需加热到150℃以上才能进行反应，生成的二苯硒基开环产物在双氧水氧化下可以转化为取代二氢呋喃类化合物。

The effect of alfalfa hay meal partially substituted for complete diets on performance and economic profit in feeding Duroc swine was investigated in order to study a proper feeding amount of alfalfa hay meal for pure breed Duroc swine.

为探讨紫花苜蓿草粉在纯种杜洛克猪中的适宜添加量，考察了苜蓿草粉替代部分杜洛克猪全价日粮对其生长性能及经济效益的影响。

This protocol could also be used for the selective reduction of the endocyclic double bond of the 3-electron withdrawing group substituted coumarins. This method is clean, mild, and efficient.2 ZrCl_4 / HEH was found to be a selective and efficient reagent combination for the direct reductive amination of electron rich aldehydes and ketones with weakly basic amines after scanning various catalysts such as InCl_3, BiCl_3, CF_3COOH and so on.

图一 1。我们用汉斯酯作为有机还原剂，乙醇为溶剂，实现了4-甲叉基噁嗯唑酮和吡唑酮环外双键的高选择性还原；此外，我们还将这一还原体系用于3-吸电子集团取代-3，4-二氢香豆素环内双键的选择性还原。

The main metabolites in each reactor were detected by UV/VIS, infrared and high performance liquid chromatography and mass spectrometry. Probably, the mother dye molecule facultatively hydrolyzed to produce 1-NH2-2-hydroxy anthraquinon, OH-substituted anthraquinon and 3,4-dihydroxy-benzonic acid.

对各反应器中主要的代谢产物分别进行紫外-可见、红外和高效液相色-质联谱仪检测分析后发现，母体染料经兼氧水解首先生成1-氨基-2-羟基蒽醌以及还原态的—OH基取代蒽醌隐色体，进一步水解生成3，4-二羟基苯甲酸。

In this dissertation, after combining the high stability of C9 diaryl substituted fluorene derivatives with the high carrier mobility and hole-injection ability of pyrene, a series of novel blue-light-emitting materials were designed and synthesized.

在本论文中，将9位双芳基芴结构的高稳定性能和稠环芳烃芘的高载流子迁移率、空穴注入能力结合起来，设计、合成了一系列新型蓝光材料，并研究了它们的光电性能。

Three new ferrocenylmethyl-substituted indenes and cyclopentadienes were synthesized by the addition of hydrogen anion and carbon anion to fulvene and benzo fulvene respectively, moreover, their structures were characterized by NMR and MS.

本文以二茂铁基富烯和二茂铁基苯并富烯为前体，通过负氢和负碳对双键的加成，合成了3个新型的二茂铁基甲基取代的茚及环戊二烯，并对其结构进行了核磁及质谱表征。

Five novel asymmetrical molecular tweezers based on diethoxycarbonyl-and diphenyl glycoluril with different substituted groups of aromatic ringsand 1,2 -dihydro-indazol-3-one moiety as sidewalls were designed and synthesized.

合成了五个含单个1，2-二氢-引唑-3-酮和不同取代的苯环(H，OMe，Me，Br)为墙面的基于二乙基酯基甘脲和二苯基甘脲的不对称分子钳。

Alkyl substituted imidazoles were synthesized by reaction of alkyl amines with glyoxal, formaldehyde and ammonia in methanol.

在对环境保护和资源的可持续利用倍受关注的今天，绿色化学是化学发展的必然趋势。

Since 2002, Institute of Coal Chemistry, Chinese Academy of Sciences has been developing a new technology to prepare high-purity glyoxylic acid by maleic anhydride ozonation, which has been completed, and now the research of the downstream products of glyoxylic acid including vanillin, heliotropin and the substituted mandelic acid is underway.

中科院山西煤化所从2002年开始进行研究，完成顺酐臭氧化法制备高纯乙醛酸新技术工艺的开发，现正进行乙醛酸下游产品香兰素、洋茉莉醛、取代扁桃酸的技术研究。

She gently rebuff ed him, but agreed that they could be friends

她婉言拒绝了，但同意作为朋友相处。

If in the penal farm, you were sure to be criticized.

要是在劳改农场，你等着挨绳子吧！