查询词典 spectroscopic

The oxidation kinetics of depleted uranium was studied in pure oxygen pressure of 5 kPa at below 100°C by using spectroscopic ellipsometry. The relationship of the thickness of uranium oxide with time is measured. The results indicate that below 100°C in the initial period, the relationship between oxidation layer thickness and time is parabolic. The oxidation mechanism of depleted uranium is discussed and the active energy of depleted uranium at given experimental conditions is 87.165kJ/mol from calculation.

采用椭偏技术研究了45~95℃和5kPa纯氧气氛中金属铀的氧化，通过不同温度下金属铀表面氧化层厚度随时间的变化规律，得到贫铀在初始氧化阶段的表面氧化层厚度与时间的关系均呈现抛物线规律；绘制出了在不同温度下金属铀表面的氧化动力学曲线，由此得到在低于100℃，5kPa的纯氧气氛下贫铀表面形成氧化物的反应活化能为87.165kJ/mol。

This paper studies spectroscopic analysis of alloy visible spectrum.

对合金材料可见光谱看谱分析技术进行了研究，讨论了分析用谱线的选取方法，摄制并标定了相应的彩色图谱。

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物，利用理化性质和波谱技术(UV、IR、EI／MS、ESI／MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构，分别为9种蒽醌类化合物：大黄酚，大黄素甲醚，大黄素，芦荟大黄素，大黄酸，番泻苷A或B，ω-羟基大黄素(ω-hydroxylemodin)，大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside)，芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside)；3种菲醌类化合物：丹参酮ⅡA(tanshinoneⅡA)，隐丹参酮，丹参酮Ⅰ(tanshinone Ⅰ)；1种异黄酮：7，3'-二羟基-5'-甲氧基异黄酮（7，3'-dihydroxy-5' methoxyisofla-vone）以及原儿茶醛，原儿茶酸，黄芪甲苷(astragaloside Ⅳ)，苦杏仁苷，2，3，5，4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷（2，3，5，4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside），Z—儿茶素，桂皮酸。

Chapter four deals with the synthesis , spectroscopic and structural study of two novel chiral annuloid compounds derived from 1,2-diaminocyclohexane via silicon and phosphor.

第四章讨论了两个硅、膦环合环己二胺手性配体化合物的合成及其光谱特性与结构特征。

MethodsThe methanol extracts of the pericarp of Arnebia euchroma oil extract were separated with various chromatography technologies to produce some pure compounds and their structures were elucidated by spectroscopic and chromatographic methods.

方法利用色谱法对中药紫草油膏中的化学成分进行分离；利用核磁共振、质谱波谱方法对分离得到的单体化合物进行结构鉴定。

MethodsThe methanol extracts of the pericarp of Arnebia euchroma oil extract were separated with various chromatography technologies to produce some pure compounds and their structures were elucidated by spectroscopic and chromatographic methods.

方法利用色谱法对中药紫草油膏中的化学成分进行分离；利用核磁共振、谱波谱方法对分离得到的单体化合物进行结构鉴定。

The spectroscopic and electrochemical studies suggest the energy structure of this class complex can be easily controlled by modification. With the introduction of electron-donating arylamino groups, the obtained complexes show intense and continuous absorption bands in the region of 250-550nm with strong metal-to-ligand charge transfer dπ(Pt →π* transitions (ε~ 2×104 dm3 · mol-1 · cm-1). Complexes involving the construction of D-π-A type systems also display continuous absorption bands in the region of 400-750nm, rising from the overlapping effect of MLCT and LL'CT bands.

其中，芳胺及其二聚体类修饰基团的引入，使其配合物MLCT吸收谱带的摩尔吸光系数增加，并在250～550nm范围内形成了强的连续吸收；具有D-π-A结构的配合物，由于MLCT吸收谱带和LL'CT吸收谱带的协同效应，导致在400～750nm范围内形成连续吸收；得到了从绿光到深红光的磷光发射系列配合物，并采用真空蒸镀的方法获到了外量子效率分别为5.7%和5.0%的橙光和橙红光多层电致发光器件。

A near infrared diffuse reflectance spectroscopic method to determine the content, moisture and pH of benzylpenicillin sodium for injection was presented.

建立近红外漫反射光谱法测定注射用青霉素钠含量、水分和 p H等品质参数的方法。

The preliminary study suggests that nanoparticles from human samples share spectroscopic characteristics with calcified bacteria that exist in freshwater lakes.

前期研究表明来自于人体样本中的毫微粒与存在于淡水湖中的钙化细菌光学特征相似。

The allelochemicals of the fungus were isolated by chromatographic methods and identified by spectroscopic methods in this paper.

本论文主要对日本曲霉的化感物质进行进一步的分离鉴定，并研究各化感物质的化感作用活性。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了