查询词典 spectral analysis

Their structures were elucidated on the basis of chemical and spectral analysis. RESULTS: Twelve compounds were isolated from the 95% ethanol extract of the aerial parts of L.rotata. Their structures were identified as luteolin (1), luteolin 7-O-β-D-glucopyranoside (2), apigenin (3), apigenin 7-O-β-D-glucopyranoside (4), apigenin7-O-6-(E-p-coumaroyl-β-D-galactopyranoside (5), tricin (6), acacetin (7), genkwanin (8), lamiophlomiol A (9), lamiophlomiol B (10), shanzhiside methyl ester(11)and syringic acid (12), respectively.

结果：从独一味地上部分的乙醇提取物中分离得到了12个化合物，分别鉴定为木犀草素(1)、木犀草素7-O-β-D-吡喃葡萄糖苷(2)、芹菜素(3)、芹菜素7-O-β-D-吡喃葡萄糖苷(4)、芹菜素7-O-（6-反式－对－香豆酰基）－β-D-半乳糖苷(5)、小麦黄素(6)、刺槐素(7)、芜花素(8)、独一味素A(9)、独一味素B(10)、山桅苷甲酯(11)及丁香酸(12)。

Mechanism of the synthesization of aminobenzene sulfonate high performancing water-reducing was proved by virtue of mass experiment and infrared spectral analysis.

在合理酸碱催化作用下，形成初级生成物，然后和对氨基苯磺酸钠苯环的邻位缩合反应，同时氨基上只有一个氢和甲醛反应生成仲胺，最后形成高聚物。

On the basis of spectral analysis, these compounds were identified as Kaempferol , Kaempferol-3-O-β-D-glucopyranoside , Kaempferol-3-O-β-D-galactopyranoside, Quercetin , Quercetin-3-O-β-D-arabinopyranoside, Quercetin-3-O-β-D-galactopyranoside, gallic acid, methyl gallate-4-O-β-D- galactopyranoside, caffeicacid, methyl caffeate, 4-cafeoyl-(3"a, 4"a, 5"β)- trihydroxyquinic acid, 3"-cafeoyl-(3"a, 4"P, 5"P )-trihydroxyquinic acid methyl ester, 5"-cafeoyl-galactonic acid , pumiloside, loganic acid , 5R,6S,7E-megastima-3-on-7-en-9-ol 9-O-β-D-glucopyranoside. 2a, 3β-dihydroxy-oleanoic acid , 2a, 3β, 23-trihydroxy-oleanoic acid, 3a, 6a-dihydroxy-oleanoic acid, 3β-hydroxy-ursoic acid, 2a, 3a, 23-trihydroxy-ursoic acid , 2a, 3β, 23-trihydroxy-ursoic acid, 2β, 3β, 19a -trihydroxy-ursoic acid, 2a , 3β, 19a -trihydroxy-ursoic acid-28-O-β-D-glucopyranoside , 2a. 3a, 19a-trihydroxy-ursoic acid-28-O-β-D-glucopyranoside, 2a, 3a, 19a, 23-tetrahydroxy-ursoic acid, 1a, 3a, 19a, 23-tetrahydroxy-ursoic acid-28-O-β-D-glucopyranoside , 3a, 19a, 23-trihydroxy-ursoic acid.

从珙桐中分离鉴定得到了28种化合物，它们分别是：山奈酚，3-O-β-D-吡喃葡萄糖基-山奈酚甙，3-O-β-D-吡喃半乳糖基-山奈酚甙，槲皮素，3-O-β-D-吡喃阿拉伯糖基-槲皮素甙，3-O-β-D-吡喃半乳糖基-槲皮素甙，没食子酸，4-O-β-D-吡喃半乳糖基-没食子酸甲酯，咖啡酸，咖啡酸甲酯，4-咖啡酰基-(3&α，4&α，5&β)-三羟基鸡纳酸，4-咖啡酰基-(3&α，4&β，5&β)-三羟基鸡纳酸甲酯，5'-咖啡酰基-半乳糖酸，pumiloside，loganic acid，5R，6S，7E-megastima-3-on-7-en-9-ol9-O-β-D-glucopyranoside，2α，3β-二羟基齐墩果酸，2α，3β，23-三羟基齐墩果酸，3α，6α-二羟基齐墩果酸，3β-羟基熊果酸，2α，3α，23-三羟基熊果酸，2α，3β，23-三羟基熊果酸，2β，3β，19α-三羟基熊果酸，2β，3β，19α-三羟基熊果酸-28-O-β-D-吡喃葡萄糖甙，2α，3α，19α-三羟基熊果酸-28-O-β-D-吡喃葡萄糖基甙，2α，3α，19α，23-四羟基熊果酸，2α，3α，19α，23-四羟基熊果酸-28-O-β-D-吡喃葡萄糖基甙，3α，19α，23-三羟基熊果酸。

To study the bioactive components from water soluble extract of the Chinese eaglewood, various column chromatography of Chinese eaglewood led to the isolation of ten compounds. Their structures were elucidated as 2,3-bis(3-hydroxyphenyl)- propan-1-ol (1), [(2R,3R)-3-(4-amino-3,5-dimethoxyphenyl)oxiran-2-yl]methanol (2), 8-chloro-4'- methoxy-5,6,7,3'-tetrahydroxy-2-(2-phenethyl)-5,6,7,8-tetrahydrochromone (3), 4'-methoxy-5,6,7,3'-tetrahydroxy-2--5,6,7,8-tetrahydrochromone (4), the isomer of 4 (5), 4'-methoxy-5,6,7,8-tetrahydroxy-2-(3'-hydroxyphenethyl)-5,6,7,8- tetrahydrochromenone (6), 4'-methoxyisoagarotetrol (7), 6-hydroxy-2-(2-hydroxy-2- phenethyl)-chromone (8), 6-hydroxy-2-(2-phenethyl)-chromone (9), 6-hydroxy-2-(4'- hydroxy-2-phenethyl)-chromone (10), and Guaiacylacetone (11) by means of spectral analysis and comparison with references.

为了进一步发现沉香中具有生理活性的化学成分，本文对国产沉香的水溶性成分进行了研究，从中分离得到11个化合物，通过红外、紫外、质谱、核磁共振(1H-NMR， 13C-NMR， COSY， HSQC， HMBC， ROESY)波谱解析，分别鉴定为：2，3-二(3-羟基苯基)-丙-1-醇(1)，[(2R，3R)-3-(4-氨基-3，5-二甲氧苯基)-2-氧化烯基]甲醇(2)，8-氯-4'-甲氧基-5，6，7，3'-四羟基-2-(2-苯乙基)-5，6，7，8-四氢色原酮(3)，4'-甲氧基-5，6，7，3'-四羟基-2-(2-苯乙基)-5，6，7，8-四氢色原酮(4)，化合物3的差向异构体(5)，4'-甲氧基-5，6，7，8-四羟基-2-(3'-羟基-2-苯乙基)-5，6，7，8-四氢色原酮(6)，4'-甲氧基异沉香四醇(7)，6-羟基-2-(2-羟基-2-苯乙基)色原酮(8)，6-羟基-2-(2-苯乙基)色原酮(9)，6-羟基-2-(4'-羟基-2-苯乙基)色原酮(10)和Guaiacylacetone (11)。

Their structures were identified by physicochemical constant and spectral analysis (IR, UV, EI-MS, 1H-NMR, 13C-NMR, and HMBC). Results The compounds were identified from their ethanol extracts as: 6, 8-dihydroxy-2-[2-(3'-methoxy-4'-hydroxyl phenylethyl)] chromone and 6-methoxy-2-[2-(3'-methoxy-4'-hydroxyl phenylethyl)] chromone.

结果 从沉香乙醇提取物中分得2个色酮类成分，分别鉴定为6，8-二羟基－2-［2-（3'-甲氧基－4'-羟基苯乙基）］色原酮{6，8-dihydroxy-2-[2-(3'-methoxy-4'-hydroxyl phenylethyl)]chromone，Ⅰ}和6-甲氧基－2-［2-（3'-甲氧基－4'-羟基苯乙基）］色原酮{6-methoxy-2-[2-(3'-methoxy-4'-hydroxyl phenylethyl)]-chromone，Ⅱ}。

The results showed that seedlings were abundant in both areas, but survival rates were low. The survival rate curve of the population fell between DeeveyⅠand DeeveyⅡ types. The trends of the disappearance rate and mortality rate curve are consistent. The spectral analysis indicated that there was a periodic regularity in the process of natural regeneration of cercidiphyllum japonicum.

结果表明：两个地区连香树种群幼苗个体比例都比较大，但死亡率很高；存活曲线介于DeeveyⅠ型和DeeveyⅡ型之间；消失率和死亡率曲线变化趋势一致；种群动态过程存在周期性，种群数量动态不仅受基波的影响，而且还显示出了小周期的波动。

The ethanol extract was dissolved with HCl, the acidic extract was basified to pH9-10 with NH_3-water and extracted with CHCl_3 to give total alkaloids. five alkaloids were isolated with column chromatography and preparative thin-layer chromatography, and three of them were identified as dehydrocorydaline、 corynoline and dihydrosanguinarine on the basis of spectral analysis MS,~1H-NMR,~(13C-NMR and physicochemical properties. All of them were found for the first time from this plant.

为研究灰绿黄堇的化学成分，本文将灰绿黄堇乙醇提取物采取酸提取、碱游离后萃取的方法得到总生物碱，然后利用柱色谱、制备薄层色谱等方法分离、纯化了灰绿黄堇中5种生物碱，并利用IR、MS、~1H-NMR、~(13)C-NMR等方法鉴定了其中的3种，分别为去氢紫堇碱、紫堇灵、二氢血根碱，均为首次在此植物中发现。

Methods Immunize hens with hepatitis B vaccine and collect the eggs. Extract egg yolk and dialyze to prepare EY-TF, then study its physical and chemical properties by spectral analysis, HPLC and Lowry method et al. according to the requirements in Chinese Pharmacopoeia.

方法用乙肝疫苗免疫母鸡，收集鸡蛋，取卵黄进行透析，制备EY-TF，参照药典要求，采用光谱法、高效液相色谱法、Lowry法等检测其理化性质。

Furthermore, seven compounds were isolated from CSPD and their chemical structures were authenticated by spectral analysis as tetrandrine, fangchinoline, tetrandrine-2′- N-β-oxide, tetrandrine-2′- N-α-oxide, dicentrine, dicentrinone, and adenine, respectively.

从粉防己专属性对照物质中分得粉防己碱、防己诺林碱、tetrandrine-2′- N-β-oxide，tetrandrine-2′- N-α-oxide，荷包牡丹碱、荷包牡丹酮和腺嘌呤等7个成分，经波谱分析鉴定了结构。

In this paper, we analyzed the larch extract tannin, aminom ethylation of larch extract tannin, quaternization of cationic larch extract tannin and amphoteric larch extract tannin (sulfonation of the larch extract tannin quaternary ammonium) by infrared spectral analysis, confirmed the quarternization and sulfonate groups, and measured its water treatment properties such as flocculation, scale inhibition, results showed that quaternization of larch extract tannin and amphoteric larch extract tannin have better water treatment ability, can realize the multifunction.

本论文采用红外光谱法对落叶松单宁、胺甲基化落叶松单宁、阳离子落叶松单宁季胺盐、两性落叶松单宁进行了化学结构分析，并对其水处理剂性能如絮凝、阻垢进行了检测。实验结果表明：落叶松单宁季胺盐和两性落叶松单宁均具有较佳的水处理能力，是性能良好的一剂多效工业水处理剂。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。