查询词典 sol-faing

Result: The nm-HAP-sol present the dispersed and uniformity needle. A431cells inhibition ratio was maximizing at the 5 day in the 400mg/L nm-HAP-sol group, the 200mg/L nm-HAP-sol group and the 100mg/L nm-HAP-sol group, inhibition ratio of the 400mg/L nm-HAP-sol group, the positive control group and the 50mg/L nm-HAP-sol group was respectively (77.89±6.29)%,(77.46±8.26)% and (1.23±0.15)%. It was detected that the number of A431 cells were persistently increasing in the 50mg/L nm-HAP-sol groups while decreasing in the 400mg/L nm-HAP-sol group, the positive control group and abidingly increasing for 4 and 3 days then decreasing in the 100mg/L and 200mg/L nm-HAP-sol group by inverted microscope.

结果：超声乳化法配制的HAP纳米溶胶呈均匀分散的针状；400mg/L、200mg/L和100mg/L溶胶组对A431细胞抑制率在第5天达到各组最大值，此时400mg/L溶胶组与阳性对照组的抑制率分别为（77.89±6.29）%和（77.46±8.26）%， 50mg/L溶胶组抑制率为（1.23±0.15）%；倒置显微镜下见50mg/L溶胶组细胞数目持续增加，聚集成簇，细胞呈现多角形或梭形，胞浆透亮，而100mg/L 和200mg/L溶胶组的细胞数目分别增加至第4天和第3天开始下降，400mg/L溶胶组和阳性对照组细胞数目持续减少，细胞体积缩小，漂浮细胞增多。

It was shown that the photocatalytic activity of TiO_2 catalysts that were prepared by sol-hydrothermal method was better than that prepared by sol-gel method from the comparison investigations of sol-hydrothermal and sol-gel methods, which result in the better dispersiveness of the former.

通过对溶胶-水热法和溶胶-凝胶法的比较研究，发现溶胶-水热法的制备样品的活性要高于溶胶-凝胶法，分析认为主要与前者的分散性较好有关。

In comparison with the conventional method of coating on the tool surface, carbide powders were coated with boehmite sol when dispersed in the mixture of boehmite sol and ethanol. The coated powders were then dried, separated, and hot-pressed. The sol preparation techniques were optimized in experiments and the property of the sol was studied at the same time.

本文从提高硬质合金刀具的耐磨性、探索新型刀具涂层方法入手，突破了在刀具表面进行涂层的传统方法，提出了用溶胶－凝胶法在硬质合金碳化物粉末表面涂覆一薄层氧化铝陶瓷制成复合粉末，然后热压制备刀具材料的新方法，开发成功一类新型的陶瓷涂层硬质合金复合刀具材料。

The polarization curves show that the corrosion current density of sol sealed film is about 2 orders of magnitude lower than that of the film sealed by sodium bichromate, the reason is that sol particles can not only seal pores of anodized film, but also form sol-gel coating on anodized film.

极化曲线显示溶胶封闭膜的腐蚀电流密度比重铬酸盐封闭膜的降低2个数量级，其原因是溶胶不仅封闭了氧化膜的孔隙，而且在氧化膜的表面形成溶胶凝胶涂层。

This invention discloses a new technology for preparing rear earth ionic doped fiber prefabricated rods with DC-RTA technology in a sol-gel method including preparing sol containing necessary doped ions, coating said sol uniformly on the inner wall of the quartz glass tube and burning it under high temperature to coagulate and vitrify them to a doped layer and repeating the above process to form a fiber prefabricated rod by oxygen and hydrogen flame after the doped layer reaches to a designed thickness and the fiber prefabricated rod can be made to various rare earth ionic doped fibers by an ordinary drawbench technology.

本发明属于光纤制造和光纤激光技术领域，具体公开了一种利用溶胶凝胶方法中的DC-RTA技术制备稀土离子掺杂光纤预制棒的新工艺。该工艺步骤包括预先配制好含有所需掺杂离子的溶胶，将该溶胶均匀涂覆在石英玻璃管的内壁后高温灼烧，使之凝结并玻璃化为一层掺杂层。反复上述涂覆灼烧过程，在掺杂层达到设计厚度后由氢氧焰高温收棒形成光纤预制棒。该方法所得到的光纤预制棒可以通过普通拉丝工艺拉制成各类稀土离子掺杂光纤。

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

In the aspects of research method, we took the method of preparing sol at first and then impregnating the wood to obtain ceramic-wood composite; this method made the wood use efficiently and increased the wood's weight gain percent. The ceramic-wood composite with performances of well decay resistance, dimensional stability, effloresce resistance and high strength was obtained by importing the cymene to the net of gel as the result of co-hydroxylation between MTES and TEOS. Making use of XPS ,we found that the apex of Si2p、O1s、C1s had evident chemical shift , which validated the existence of Si-O-C bonding.Key Words: Sol-gel, Ceramic-wood composite, Modified sol, Ecomaterials

在工艺方法上，采用先制备溶胶，然后浸注木材的工艺方法具有原料利用率高、提高增重率的优点；采用甲基三乙氧基硅烷和正硅酸乙酯共水解的方法，将甲基引入陶瓷化复合木材的凝胶内部，所制备的材料具有尺寸稳定性好、具有耐风化和耐腐朽性，强度高的特点；首次利用X射线光电子能谱，发现了Si2p、O1s和C1s谱峰发生了明显的化学位移，证实了Si－O－C键合作用的存在。

The A13 sol and Al(0H)3—Zr4 sol is prepared by peptization method with A1(NO3)3 , ZrOCl2 and NH3H2O as starting materials, using A1(NO3)3 solution and Zr4 sol as peptizing agents, and the preparation process, preparation conditions and colloid structure are analyzed.

本文以Al(NO_3)_3，ZrOCl_2和氨水为原料，分别以Al(NO_3)_3溶液和Zr_4溶胶作为胶溶剂，通过胶溶法制备Al_3溶胶和Al_3—Zr_4溶胶，并对两种溶胶的制备过程，制备条件和胶团结构进行了分析。

Aluminum Ispropoxide was hydrolyzed to prepare Al〓O〓 sol. The hydrolyzed 〓CHOH affected the sol peptization. The colloidal particle was the smallest when the peptization time was 12 hours.γ-Al〓O〓 membrane without cracks, thickness about 2μm, was prepared from 1M sol with a suitable amount of PVA solution. The mean pore size of the membrane was about 3nm. And, the H〓/N〓 separation factor was 3. 53, exhibiting good separation performance.

异丙醇铝为前驱体，水解制备Al〓O〓溶胶，水解产生的异丙醇影响溶胶的胶溶效果，并且胶溶12小时得到的胶粒最小。1M溶胶加PVA制备厚度2μm左右，无开裂γ-Al〓O〓膜，经600℃煅烧，平均孔径为3nm，H〓/N〓分离系数可达到3.53，表现了很好的分离性能。

The preparation method of the photocatalysis functional ceramics was as follows: firstly, to prepare the titanic acid sol and the titanic acid sol mixing iron ion; then, to load the soil in the stoneware tube and the honeycomb ceramics by the sol-gel technology; finally, to roast the product by the program heating.

先制备钛酸溶胶和掺入Fe3+的钛酸溶胶；用溶胶-凝胶法分别将它们负载于炻器管和矩形蜂窝陶体上；再用程序升温法煅烧，得到纳米TiO2光催化功能陶瓷。

The circulation, consumption and reproduction of the trilogy have not only testified to its historical significance and literariness, but also invested it with new meanings.

该三部曲的流通、消费与再生产不仅验证了其历史意义及文学性，而切还赋予它以新的意义。

If he thought that he could buy me off, he would be wrong.

如果他认为他可以收买我，那他就大错特错了。