查询词典 sol-fa

The effects of thepreparation conditions on the structures and performances of the sol samples were studied,followed by investigating the formation mechanism of the anatase TiO_2 particles. Thecharacterization of the as-obtained sol-gel samples shows that the TiO_2 and P-doped TiO_2sols have anatase crystal structures, and the latter has higher crystallizability than theformer.

通过对TiO_2溶胶进行微观结构表征，发现：TiO_2溶胶和掺磷TiO_2溶胶均呈锐钛矿晶型，颗粒呈梭形，分散性较好，后者的结晶度更高；两者在可见光区均有较大的光吸收，最大吸收波长为550nm，磷的加入使得TiO_2的禁带宽度变大。

The composite film appeared semitransparent and brown to yellow from optical microscopy. Results show that shorter time sol-heating results in thiner film with less surface roughness, less conglutination to base, and easily to disconnect, while longer time sol-heating results in thicker film with better conglutination to base and worse roughness. RDX distributes in the film everywhere on the whole but discretely on the scale of 2.4 μm according to EDS results. XRD curve of RDX/RF film shows the superposition of RF non-crystal bread curve and RDX crystals diffraction curve. RDX diffraction peaks are broadened and its crystal size is calculated to be lower to 43 nm.

实验所得薄膜半透明，呈棕红色至黄色；实验表明，溶胶恒温加热时间较短时，所得薄膜的单层厚度较小，较平整，但附着力小，干燥后易脱落；恒温加热时间较长时，所得薄膜的单层厚度较大，不易脱落，但表面平整性较差；能谱测试表明，薄膜中的RDX整体上分布较为均匀，但在测试点位间距为2.4μm的微观尺度上呈离散状分布；XRD测试表明，RDX/RF复合物薄膜表现为RF的非晶态馒头峰与RDX衍射峰的叠加，RDX衍射峰明显宽化，其晶粒度可低至43 nm。

The rheological characteristics of sol solution have been studied. It turns out that the relation of viscosity with temperature can be expressed by the relation μ=μ〓exp , and that the solution's rheological characteristics during the sol—gel transiton are as follows: at first the dilatant fluid changes to Newton fluid, then to pseudoplastic, and finally to gel.

本文对溶胶溶液流变特性进行了研究，结果表明：温度对粘度的影响可用Arrhenius方程来表示；随放置时间的增加，溶液由膨胀型流体向牛顿型流体转变，再向假塑性流体转变，最后成为凝胶。

This paper studied the plasma transport in SOL (Scrape-Off Layer) and divertor region of the HL-2X, using'two-point'mode, computed the plasma's temperature, density and impurity radiation power lose in SOL are computed and analyzed.

为了避免破坏器壁和杂质污染芯部等离子体，有效地排出D-T反应的废料，根据现有的HL-2A的不足之处，本论文研究了HL-2A的改进装置HL-2X边界删削层和偏滤器等离子体的输运。

Contents: Geocentric System of Nature; Sacred Numbers, 7 and 12; Twelve Thousand year Cycle; Ancient Triad; God Sol; Ancient Cosmogony; Fall and Redemption of Man; Incarnations of God Sol; Fable of the Twelve Labors; Solar Worship; Zodiacal Symbols of Solar Worship; Signs of the Cross; Future Rewards and Punishments; Ancient Christianity; The Prophecies; Roman or Modern Christianity; Freemasonry and Druidism; The Sabbath; Pious Frauds, Personifications of the Divisions of Time.

内容：地心体系的性质；神圣的号码，第7和第12名；12000年为周期；古代黑社会；上帝溶胶；古老的宇宙观；秋季和赎回男子；化身上帝溶胶；寓言中的十二个劳动力；太阳崇拜；黄象征太阳的崇拜；迹象交叉；未来奖惩；古代基督教；预言；罗马或现代基督教；济和浪漫；安息日；虔诚诈骗，化身的表决时间。

Combining ion exchange process and silicon hydrolyze process Silicon dioxide mother nuclide with a specific particle size was prepared from sodium silicate through the dropwise technique , then the large particle size , high concentration and stable silica sol was prepared . The stability of silica sol also can be improved by enwrap .

和"单质硅一步溶解法"相结合的方法，用离子交换法制备晶种，并采用滴加工艺制备一定粒径大小的二氧化硅作为母核，在催化剂和分散剂共同作用下水解单质硅的方法使二氧化硅母核颗粒进一步增长成大粒径的二氧化硅颗粒，并另外还采用水溶性高分子对纳米SiO_2粒子进行"原位表面包覆"提高其稳定性，制备了大粒径，高浓度，稳定的纳米硅溶胶。

The method comprises:(1) weighing lead acetate hexahydrate and thioacetamide, and preparing aqueous solutions respectively, so that the concentration ratio of Pd2+ to S is 1:(1-4);(2) adding acetic acid into thioacetamide solution to adjust the pH value to 2-4;(3) adding poly surfactant into lead acetate solution, ultrasonicating to mix uniformly and obtain a colorless and transparent sol;(4) mixing the sol and thioacetamide solution;(5) placing the mixed solution in a sealed container, irradiating by 2.5 MeV and 40 mA electron accelerator with irradiation dose of 25-40 Mrad;(6) washing the product, centrifuging for separation, and drying to obtain black PdS nanoparticles.

本发明方法的工艺过程如下：首先称取一定量的六水合醋酸铅和硫代乙酰胺，各自配制成水溶液，其浓度比为使其中的铅离子浓度与硫原子浓度的比例为1∶1～1∶4；在硫代乙酰胺溶液中加入适量醋酸调节其pH值至2～4；醋酸铅溶液中加入少量表面活性剂聚乙烯醇，然后超声振荡，混合均匀，制成无色透明溶胶；随后将溶胶与上述的硫代乙酰胺溶液混合；将该混合液置于密闭容器中，并将其放置于2.5MeV、40mA的电子加速器产生的电子束辐照下进行辐照处理，其辐照剂量为25～40Mrad；然后将反应生成物清洗，并用高速离心机离心分离，然后干燥，最终得到黑色纳米硫化铅颗粒。

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应，用茚〓和1，1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物，发现可控制反应条件，使1，1'-联茚与〓反应，并高产率地得到具有新颖结构的单加成物，用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征，测得它的两个〓杂化的桥头碳的化学位移为〓ppm，证明生成的衍生物为6∶6闭式环加成，〓NMR谱中共给出38个信号，表明〓联茚衍生物分子具有〓对称性；在波长532nm，脉冲宽度8ns的激光下，〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近，由于〓联茚单加成衍生物熱稳定性好，在四氢呋喃，丙酮等极性溶剂中溶解性好，能分别均匀地掺入溶胶-凝胶中，已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能；使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究，通过等温压缩曲线测试，证明浓度为〓〓时，〓联茚衍生物能够形成单层膜。

Based on the polymerizable and unpolymerizable structure directed agent through supramolecular self-assembly method, the above prepared surface modified SiO〓 sol or TiO〓 sol was interacted with monomer and cross liker by co-assembly, with the formation of layered organic/inorganic nanocomposite thin film that mimic nacre on glass substrate.

在动静摩擦系数测定仪上研究了它们的摩擦学性能。发现无论是未聚合薄膜还是聚合薄膜与钢球对磨时，与空白玻璃片相比都具有较低的摩擦系数，仅为O.1左右，而且两者摩擦系数相同。

This dissertation is relation to SrO(La2/3Sr1/3MnO3)n the manganese oxides with RP structure. We mostly studied the structure and electrical transport properties, The major studies are listed below: The classes of magnetoresistance were introduced, the electron and crystal structure and the mechanism of double exchange of manganite pervosike related to colossal magnetoresistance have been summarized. More attention had also been paid to the advance in the study of RP structure manganite and grain system. The principle and process of sol-gel method were introduced. With sol-gel method a series of different grain size La2/3Sr1/3MnO3 sample were prepared.

本文以Mn3+：Mn4+=2：1的Ruddlesden-Popper结构锰氧化物SrO(La2/3Sr1/3MnO3)n为研究对象，系统的研究了利用溶胶-凝胶法制备的n=∞的La2/3Sr1/3MnO3和n=2的La4/3Sr5/3Mn2O7两个系列样品的结构和电磁性质，主要内容包括以下几点：简单介绍了磁电阻效应的分类，概述了具有超大磁电阻效应的锰基钙钛矿氧化物的电子晶体结构和双交换等相关的物理机理，给出RP结构系列锰氧化物的晶体结构和电磁相图以及研究状况，分析了颗粒系统的研究进展。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。