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While the molar ratio of WD-20 and tetraethyl orthosilicate was 0.2, the sol-fraction of the prepared nanocomposites was 6%,glass transition temperature was above 250 ℃ and the transmittance was more than 80% at the wavelength between 450 nm and 800 nm and the size of dispersed SiO2 phase was less than 100 nm.

当WD-20与四乙基原硅酸盐之比为0.2时,所制备的纳米复合材料的溶胶分数为6%、玻璃化转变温度为250 ℃以上、可见光透过率在80%以上、SiO2分散相尺寸小于100 nm。

Palmitic acid-silicon dioxide nano-composite phase change material was prepared by sol-gel process from tetraethyi orthosilicate and palmitic acid.

采用溶胶—凝胶法,以正硅酸乙酯和棕榈酸为主原料,制备了一种有机—无机纳米复合相变材料。

Nanu-SiO2 was syrtthesized though hydrolyzation-condensation of n- tetraethyl orthosilicate in organic solvent using sol-gel method.

西北工业大学理学院,西安710072摘要:采用溶胶一凝胶法,利用正硅酸乙酯在有机溶剂中的水解-缩合制备纳米SiO2。

Porous carbons were prepared with tetraethyl orthosilicate as the silica template and solube starch and β-cyclodextrin as carbon precursor by sol-gel method.

以正硅酸乙酯为模板硅源,β-环状糊精和可溶性淀粉分别为碳前驱体,运用溶胶-凝胶法制备了多孔炭材料。

The sol-gel solution was prepared by mixing ethyl orthosilicate, absolute alcohol and 0.1molL^(-1) HCl in a definite proportion, and adding an appropriate amount of silicotungstic acid as active material, strring for 30min and then standing for 24h at room temperature.

溶胶-凝胶溶液系将正硅酸乙酯、无水乙醇及0.1molL^(-1)盐酸按一定比例混合后加适量的硅钨酸作为活性物质,搅拌30min混匀后在室温放置24h配成。

Monolayer high anti-reflective coatings are coated by sol-gel method with tetraethyl orthosilicate and silicon oil(MW≈500) as precursor and ammonia as catalyst.

以正硅酸乙酯和硅油为前驱体,在碱性催化体系中制备出有机硅改性二氧化硅溶胶,采用提拉法获得了具备疏水性能的二氧化硅减反膜。

Hydroxyethyl cellulose and tetraethyl orthosilicate are chosen as the stuffs for the reaction, and HEC/SiO2 organic/inorganic hybrid are prepared by Sol-Gel process.

以羟乙基纤维素、正硅酸乙酯为原料,采用溶胶-凝胶技术合成了HEC/SiO2有机-无机杂化材料。

Samples prepared by sol-gel method have the largest OSC and suitable specific surface area.

采用溶胶—凝胶法制备的储氧材料老化前有较大的储氧量和合适的比表面。

Crystalline and amorphous nano-Al_2O_3 powder were synthesized by room-temperature hydrolysis method and direct oxidic method respectively, and nano-SnO_2 powder was produced by sol-gel technology. Their microstructure features and growth behavior of crystal grain were studied in detail, and corresponding model and theory were put forward to explain them.

采用室温水解法和直接氧化法分别获得了晶态和非晶态纳米Al_2O_3粉,采用溶胶-凝胶法制备了纳米SnO_2微粉,研究了它们的微结构特征与晶粒生长行为,并提出了相应的模型与理论去解释。

Nanocrystalline Pb(Zr0.52Ti0.48)O3 was prepared from lead acetate, zirconium oxynitrate and tetrabutyltitanate by a sol-gel method.

以醋酸铅,硝酸氧锆,钛酸四丁酯为原料用溶胶-凝胶法制备了纳米Pb(Zr0.52Ti0.48)O3。

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