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SO〓〓/M〓O〓 solid superacid was applied to the photocatalytic oxidation of organic pollutants for the first time. Porous SO〓〓/TiO〓 solid superacid catalysts with high specific surface area were prepared by sol-gel method. The photocatalytic degradation of bromomethane was used as model reaction. The influence of impregnation with H〓SO〓 solution on the structure of catalysts and their photocatalytic performance was systematically studied by using X-ray diffraction, X-ray photoelectron spectroscopy, N〓 sorption analysis applying BET method, UV-Vis diffuse reflectance spectroscopy, FTIR spectroscopy, O〓-TPD and photocatalytic activity measurement. The acidity of TiO〓-based catalysts was investigated by Hammett indicator method, NH〓-TPD and IR spectra of pyridine adsorbtion. The mechanism of superacidifing effects on photocatalytic performances such as the photocatalytic degradation rate of bromomethane, apparent kinetic constant and apparent quantum efficiency was discussed.The results indicated that SO〓〓 is combined with metal ions of TiO〓 in a chelating bidentate mode.

本文首次将SO〓〓/MxOy型固体超强酸催化剂用于光催化氧化有机污染物研究,采用溶胶-凝胶法制备了具有多孔性和大比表面结构的二氧化钛基固体超强酸光催化剂SO〓〓/TiO〓,以光催化降解溴代甲烷为模型反应,系统地研究了H〓SO〓浸渍处理对催化剂表面酸性及其气相光催化性能的影响,结合XRD、BET、XPS、FTIR、Hammett指示剂法、吡啶吸附红外光谱、NH〓-TPD、O〓-TPD、紫外可见漫反射光谱等多种表征手段,深入地讨论了超强酸化对TiO〓的改性机理,阐明了引起SO〓〓/TiO〓超强酸催化剂光催化降解溴代甲烷的转化率、表观反应速率常数和表观量子效率变化的本质原因。

AIM To investigate the hypoglycemic effect of buccally delivered insulin solution in normal rats.

目的 研究胰岛素溶液(insulinsolution ,INS SOL)经正常大鼠口腔给药后的降血糖作用。

This thesis adopts the method of Sol-Gel to develop ZnO and ZnMgO alloying film and introduces the influence of technology parameters such as calefactive velocity, film thickness, anneal temperature on the performances of the film such as crystalline quality and photoluminescence in a detailed way.

本论文采用溶胶一凝胶工艺制备ZnO及ZnMgO合金薄膜,详细研究了升温速率、薄膜厚度、退火温度等工艺参数对薄膜的结晶质量和发光性能的影响。

Amorphous SiO_2,anatase TiO_2 and cassiterite SnO_2 hollow sphere s were successfully prepared using colloidal carbon spheres as template in conjunciton with the sol-gel method.

介观尺度的氧化物空心球材料在许多领域都有着潜在的应用价值[1],因此近年来受到人们的广泛关注。

Nano-sized hydrous ceric oxide with an average diameter size of 70 nm and specific surface area 212 m g were prepared using sol-precipitation method in conjunction with ultrasonic dispersion.

采用溶胶沉淀结合超声分散处理的方法,制备平均粒径为70nm,比表面积为212平方公尺g^(-1)的纳米级水合氧化铈吸附剂。

Nanocrystalline CeO 2 were prepared by sol gel method using cerous nitrate and citric acid. The powders were analyzed by XRD. It was showed that the synthesized CeO 2 was cubic in structure and CeO 2 particles were basically spherical in shape.

摘 要:以硝酸铈和柠檬酸为原料,采用溶胶凝胶法制备了纳米CeO2 对反应温度、金属离子与配体的摩尔比、凝胶烘干温度、焙烧温度等制备条件对产物的影响进行了研究。

Using cetyl trimethyl ammoniunm bromide as templating agent, the mesoporous TiO_2 with special performance was synthesized by a tartaric acid sol-gel method. The UV irradiation was used in this process.

以十六烷基三甲基溴化胺为模板剂,采用溶胶-凝胶法,在溶胶-凝胶制备过程中引入紫外光照辐射,制备出具有一定特殊性能的中孔TiO2材料。

Sol line asymmetry is an important characteristics in spectral observations of chromospheric flare, since it reflects directly the dynamic process of solar flare.

Hα谱线轮廓的不对称性是色球耀斑光谱观测中的重要特征,也是耀斑动力学过程的重要观测事实之一。

After colling in air atmosphere, the nano-sized sample was obtained The nano-sized TiO2-coated Er3+:YAlO3 upconversion luminescence agent was prepared through the sol-gel precess.

在空气中后,科林,纳米大小的样品,获得在纳米二氧化钛涂层掺Er3 +:YAlO3上转换发光剂是通过溶胶凝胶进动准备。

The process of converting to a sol; bringing to a colloidal solution.

转化为溶胶的过程;产生胶质溶液的过程。

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I didn't watch TV last night, because it .

昨晚我没有看电视,因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来,在北京的很多小区里,电梯液晶电视被撤了下来。

I'm running my simile to an extreme.

我比喻得过头了。