查询词典 sodamide

A certain reference value was indicated in this experiment for industry synthesis of cedrol methyl ether by sodamide method.

本实验对甲基柏木醚氨基钠法工业化生产具有一定的参考价值。

In this paper, the cedrol methyl ether was synthesized by sodamide method.

本文采用氨基钠法合成甲基柏木醚。

Two steps were included in this reaction, first, sodium alkoxide was synthesized by th reaction between sodamide and cedrol, then cedrol methyl ether was synthesized by methylation reaction between sodium alkoxide and dimethyl sulfate.

反应分两步，首先氨基钠与柏木脑反应生成醇钠，然后醇钠与硫酸二甲酯进行甲基化反应生成甲基柏木醚。

Based on groups of single factor experiments, the yield could reached to 88.8% with the conditions: sodamide: cedrol :dimethyl sulfate = 1.6:1:0.9, refluxed 2h in first step reaction, and reacted at room temperature 1h after instillation of dimethyl sulfate, followed refluxed 1h in the second steps.

通过多组单因素实验发现氨基钠：柏木脑：硫酸二甲酯的摩尔比为1.6：1：0.9，第一步反应条件控制在回流2h，第二步反应先室温（25℃）滴加硫酸二甲酯后反应1h，再回流反应1h，得率可达88.8%。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。