查询词典 sintering

The invention discloses a dielectric hole-microhole composite material and synthesizing method in the inorganic porous material, adsorbing material and catalytic material technical domain, which comprises the following steps: adopting zeolite molecular sieve as raw material; reacting with sodium bisilicate solution under 30-60 deg.c for 10-300 min; disintegrating particle part of zeolite molecular sieve into piece with microhole structure; adding cetyl trimethyl ammonium bromide as molder; adjusting pH value of mother liquid to 10-12; aging 1-8h; adding in the high-pressure autoclave to do water heat synthesizing reaction at 80-130 deg.c for 24-72h; separating solid; washing; drying; sintering under 500-600 deg.c for 5-10h; obtaining the Si-Al porous material with dielectric hole and microhole composite structure.

本发明属于无机多孔材料、吸附材料和催化材料技术领域，涉及具有介孔-微孔复合材料及其合成方法。其特征是以沸石分子筛为原料，用偏硅酸钠的水溶液在30～60℃反应10～300分钟，使沸石分子筛的颗粒部分解离形成具有微孔结构的碎片，加入模板剂十六烷基三甲基溴化铵，然后调节母液pH值为10～12，老化1～8小时，然后加入高压釜于80～130℃进行水热合成反应。反应24～72小时后，分离出固体，水洗、干燥，然后于500～600℃焙烧5～10小时，得到具有介孔和微孔复合结构的硅铝多孔材料。本发明的效果和益处是所发明的合成方法可用于合成多种沸石结构和介孔结构的复合材料，所合成的材料经过质子交换可以具有较强的酸性，在吸附和催化领域具有广泛应用前景。

The results of boron, borax and boronic iron concentrate as additives in the production of sintering pellets are compared and analyzed.

比较分析了硼、硼泥、含硼铁精矿作为添加剂在烧结球团生产中的应用，得出了含硼铁精矿作为烧结球团的含硼添加剂在经济上、工艺上都是可行的，且性能优于硼泥的结论。

To find and confirm the most effective preparing technology, the effect of sintering temperature and calefactive velocity upon mechanical properties and microstructures of the materials before and after infiltration were studied. In order to control the coefficient of thermal expansion and colors of the glass as well as the fluidity and infiltration property of the melted glass, we modified the formula of the glass.

在材料制备的同时，研究和比较了氧化铝升温速率及烧结温度对玻璃渗透前后材料的力学性能和微观结构的影响，以期寻求最佳的制备工艺；并改进渗透玻璃配方，以调控玻璃的热膨胀系数和颜色以及在高温下的流动性、浸润性。

The conventional method of preparing fine cemented carbide is to reduce and carburize fine W and WC powder at low temperature, then inhibitors,such as TaC, Cr3C2 and VC, are usually added into the powder to prevent the WC grains from coarsening during sintering.

制取这种微晶硬质合金通常的方法是，用还原和碳化方法，首先得到细W粉和WC粉，然后加入TaC、Cr3C2和VC等晶粒长大抑制剂，并且通常是将这些抑制剂加入到W粉或WC粉中，防止WC晶粒在烧结时长大变大变粗。

Through sintering at high temperature, better properties of the castable was obtained.

在不同高温烧成后，有机结合剂的浇注料性能得到提高。

The adding of ZrO_2 could suppress the appearance of the Celsian during the sintering process and then improve the insulation properties of the dielectric, result in stainless-steel satisfy the thick film circuit's needs.

加入ZrO_2能够有效抑制烧结过程中单斜相的析出，大大改善介质层的绝缘性能，使基板满足厚膜电路对绝缘性能的要求。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时，再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节；实验中选用CaCl2作为电解熔盐，并对其进行预处理(100℃，保温1小时； 300℃，保温2小时)；经热力学计算，还原钛氧化物的氧分压至少要低于5.11×10-7Pa，结合电解过程中所用熔盐CaCl2有极强的吸水性的特点，电解装置应有较高的密封性，自行设计了一套密封性可靠的电解装置，便于实验过程中熔盐预处理和氧分压的控制；通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时，电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃，实验结果表明电解时间与TiO2质量密切相关，质量越大需要电解的时间越长；通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤，可减少熔盐及其它杂质对电解产物检测结果的影响；最后，通过循环伏安法、计时电流法对电解机理的研究，确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

The coprecipitate precursor of La0.9Ba0.1Er0.85Mg0.18O3-α solid electrolyte material was prepared by microemulsion method and the dense ceramic sample was obtained by calcining and sintering the precursor.

采用微乳液法合成了La0.9Ba0.1Er0.85Mg0.15O3-α固体电解质材料的共沉淀前躯体，通过初烧和烧结制得致密的La0.9Ba0.1Er0.85Mg0.15O3-α陶瓷样品。

Based on the accidents in test and operation of line-frequency coreless induction furnace , the safety proceedings in furnace lining sintering, furnace drying and the melting operation and the emergency treatment methods of service interruption, leakage of steel and accident of cooling water have been pointed ou

针对无芯工频感应电炉试炉及运行过程中易发生的事故，提出了炉衬烧结和烘炉、熔炼操作过程中应注意的安全事项，以及停电、漏炉、冷却水事故的紧急处理方

This thesis has systematically studies the microstructure of the sinter bearing fluorine of different compositions and in different sintering condition.(1) The main units of the Low Fluorine Sinter are magnetite、hematite、 SFCA、larnite、glass and pore. The cuspidine doesn't form for the low content fluorine, and the fluorine is in glass; Sinter basicity dominates the forming of the larnite and SFCA, when basicity is between 1. 72 and 1. 96, there are more larnites in the binder phase, and when the basicity is biger than 1. 96, there are more SFCA in the binder phase; the hematite appears like magnetite and usually is around pore.

为此，本文对不同组成、不同烧结条件的烧结矿样品进行了系统的显微分析和研究，其主要内容包括：(1)构成低氟烧结矿的主要组元有磁铁矿、赤铁矿、铁酸钙、硅酸二钙、玻璃体和气孔，由于含氟量的降低，枪晶石等含氟矿物并未形成，氟分布在后期凝固的玻璃体中，其中硅酸二钙和铁酸钙受碱度影响较大，硅酸二钙在碱度为1.72～1.96范围内形成较多，铁酸钙在碱度大于1.96含量增多，赤铁矿呈磁铁矿假象，多分布在气孔周围，各组元的生成顺序为：磁铁矿—硅酸二钙—铁酸钙—玻璃体。

I didn't watch TV last night, because it .

昨晚我没有看电视，因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来，在北京的很多小区里，电梯液晶电视被撤了下来。