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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现;3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布;4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒;5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明:1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致;2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响;3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现; 3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布; 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒; 5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明: 1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致; 2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响; 3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

The authority would judge any single character (Han sentence is formed by joining of characters) or any single sentence's neutrality; if the authority had decided these words, or sentence were derogative or cynic towards the rulers, then persecution would begin.

管理局将法官任何单一字元或任何单句的中立性;如果当局已决定这些话,或判刑的贬损或愤世嫉俗对统治者,然后将开始迫害。

With regard to the fact that there is neither complete legal system nor independent substantive law or procedural one against juvenile criminality,it is necessary for judicial offices of different levels to perfect the judicial remedy,such as juvenile court system and suspending proceedings system.Other ways include:to change the state of single criminal,to break through the limits of single trial and to reassess the judge determination system and the juage's practice of abandoning designative jurisdiction,etc.

鉴于目前我国法律对未成年人犯罪问题尚未形成完整的法律体系,还没有独立的未成年人犯罪实体法和程序法,需要各级司法机关进一步探索完善未成年犯罪的司法救济体系,比如少年法庭体系,暂缓起诉制度,改变刑事单一化的现状,突破审判单一化的局限,重新确定法官评价体系及法官职能摈弃指定管辖的做法等。

In the second experiment, dichoptic display (15 ms for single eye, 30 ms for single eye, 30 ms for both eyes) was used to investigate the mechanisms of these brightness effects.

第2个实验,采用单眼和双眼分离两种观察方式,使得刺激呈现单眼呈现15ms,单眼呈现30ms,双眼呈现30ms3种情况,在刺激呈现结束后,要求被试报告闪光刺激明暗关系。

At least one single roller type multicolor single-side printing device or one perfecting machine device is installed in the machine frame and the power mechanism brings the roller and the ductor mechanism into operation by the drive mechanism.

滚筒式单筒多色印刷装置,含有滚筒,油墨辊机构,定位机架,在一个滚筒周边设置至少有两种不同颜色的油墨辊机构,在滚筒上或滚筒一端面上设有油墨分配机构,所述油墨辊机构彼此之间的传墨次序受油墨分配机构控制。

One was emphysematous model by single endotracheal instillation of porcine pancreatic elastase 800 EU /Kg,the other was normal control received single endotracheal instillation of equal volume 0.9% NaCl.

结果 :运动锻炼后NE和EE组心肌和腓肠肌肌纤维氧化性能明显改善,SDH活性升高(P 0 5 ),但膈肌肌纤维中SDH活性仅在EE组有提高(P 0 5 )。

This paper emphasized on the strength testing of paper-bag which was produced by Foshan Sanshui KelunPaper.Inc. The test was done according to the Chinese Standards(GB/T453—2002、 GB/T450—2002、GB9774—2002 etc.).It showed that , the average CD ensile strength of a single paper is 2.96KN/m, above the normal value of 2.0 KN/m; The average MD ensile strength of a single paper is 3.88 KN/m, above the normal value of 3.8 KN/m; The combined CD ensile strength is 7.88 KN/m, above the normal value of 6.0 KN/m; The combined MD ensile strength is 11.91 KN/m, above the normal value of 11.4 KN/m.

本文针对佛山三水科伦纸业公司生产的纸袋进行了强度方面的测试,根据国家标准(GB/T453—2002、GB/T450—2002、GB9774—2002等),借鉴厂内已有的检测方法,测出了该厂生产用纸单层的横向抗张强度的平均值为2.96 KN/m,高于行业经验值2.0 KN/m;纵向抗张强度平均值为3.88 KN/m,高于行业经验值3.8 KN/m;组合横向抗张强度为7.88 KN/m,高于行业经验值6.0 KN/m;组合纵向抗张强度为11.91 KN/m,高于行业经验值11.4 KN/m。

In this paper the mathematical models and methods for GPS single-point positioning are studied systematically on the theory.All kinds of error correction formulas are studied,such as ironsphere correction,troposphere correction,relativistic effect correction,earth rotation correction ,earth tides correction ,satellites antenna phase center offset correction. GPS single-point positioning programs is coded with pseudoranges and broadcast ephemerides,phases and broadcast ephemerides,and phases and precise ephemerides.And a great amount of computation has been done using the data collected .The results are computed with the 24 hour pseudoranges observation data before and after the canceling of the SA.

本文从理论上系统地研究了GPS单点定位的数学模型和方法,研究了各项误差改正公式,例如电离层改正、对流层改正、相对论周期部分改正、地球旋转改正、地球固体潮改正、卫星天线相位中心偏差改正;编写了伪距与广播星历、相位和广播星历及相位和精密星历的定位程序,并使用有关数据进行了大量的计算工作。

It can realize multiple analog single collection, multiple control single output .It can realize the communication between local equipment and epigynous machine by 485 bus.

它能实现多路模拟量输入,多路模拟量输出,PWM控制信号输出,通过485总线实现控制器与上位机的实时通信。

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推荐网络例句

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。