查询词典 silica gel

The immobilization of palladium on silica gel in Heck reaction has been developed.

本文报道了一种新型硅胶负载钯催化剂在Heck 反应中的应用。

Solani. The extract was further separated into two parts and one part separated by ethyl acetate while the other was separated by petroleum ether. Based on the inhibition experiment against R. solani, ethly acetate extract has a rather strong effect on R. solani with 89.70% inhibition rate and 15.52 mgmL^(-1) EC 50.The effect of petroleum ether extract on R. solani is relatively weak. The former was again divided into five parts in silica gel column, of which the second part significantly inhibits R. solani. During the periods of 24 and 48 hrs, the inhibition rate of the second part on R. solan is respectively 89.58% and 80.36%.

结果表明：鸭粪乙醇提取物对水稻纹枯病菌有抑制作用，24h内最高菌丝生长抑制率和EC50分别为88.64%、26.11mgmL^(-1)；鸭粪乙醇提取物经萃取分离得到石油醚和乙酸乙酯两种组分，其中石油醚组分抑菌效果较弱，乙酸乙酯组分抑菌能力较强，其对水稻纹枯病菌抑制率为89.70%，EC50为15.52mgmL^(-1)；对乙酸乙酯组分进行硅胶柱层析分离得到5种流份，其中第2流份有显著抑菌活性，在24h和48h内对水稻纹枯病菌的抑制率分别为89.58%和80.36%。

Methods Compounds were separated and purified by silica gel column chromatography and their structures were identified on the basis of spectral data and physico-chemical property.

方法采用硅胶柱层析进行分离纯化化合物，根据理化性质和现代波谱技术进行结构鉴定。

The sporophore of Cordyceps militaris and the cordycepin content of intermediate products were monitored in the whole course according to the relation between fixed and mobile phases of solvents in a combination system of binary and quaternary solvents, in which the applied methods were successively supercritical fluid extraction, alcohol sedimentation, low-pressure normal-phase silica-gel chromatography, reversed-phase high-performance liquid chromatography and fractional crystallization.

根据溶剂的固定相与流动相之间的相对关系，采用了二元和四元组合的溶剂系统，顺次采用超临界流体萃取法、醇沉法、低压正相硅胶色谱法、反相高效制备液相色谱法、分步结晶法和反相高效液相色谱法，子实体及其中间产物中的虫草素含量变化情况。

The solidified alcohol has been prepared by using sodium stearate and silica gel as solidified agent.

以硬脂酸钠和硅胶作为固化剂制备固体酒精，通过实验得出了最佳工艺条件。

Molecularly imprinted polymers of sulfamethazine(SM 2 ) were prepared with silica gel as a sacrificial material, methacrylic acid and 4 vinylpyridine(4 Vp) as functional monomers, glycol dimethacrylate as crosslinker. The polymer properties were investigated by static adsorption experiments. Scatchard analysis shows that the adsorption ability of MAA MIP is superior to that of 4 Vp MIP. The dissociation constant of MAA MIP is 9 59×10 -4 mol/L. The value of apparent binding a...

以磺胺二甲嘧啶为模板分子，分别用甲基丙烯酸和4乙烯基吡啶为功能单体，二甲基丙烯酸乙二醇酯为交联剂，采用牺牲硅胶法合成了磺胺分子印迹聚合物，通过静态吸附实验，系统研究了不同单体对聚合物识别性能的影响；Scatchard分析表明，以甲基丙烯酸为单体的聚合物具有较高的吸附能力，其离解常数Kd为959×10-4mol/L，最大表观结合位点数Qmax为3070μmol/g。

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下：首先，以磺胺异噁唑和磺胺二甲嘧啶为模板，分别以4-乙烯基吡啶，甲基丙烯酸，丙烯酰胺为功能单体，以二甲基丙烯酸乙二醇酯为交联剂，偶氮二异丁腈为引发剂，采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

To the question of partial environmental pollution, this subject adopts nanometer to assemble technology and method , compound with antibiotic function silver ion and carrier of zeolite with structure of narrow passage of size of nanometer, make it have antibiotic function , compound silver zeolite of ion implement artificial to activate with the particle hole 2 times distributing and transforming, make ammonia correctly, sulphurate the hydrogen, the formaldehyde waits for the peculiar smell gas to absorb the function fast, add and abolish such auxiliary raw materials as the glass dust , clay ,etc. afterwards, make one with the silica gel solution, is it form usable particle to cook powder body that finish.

针对局部环境污染的问题，本课题采用纳米组装技术和方法，将具有抗菌功能的银离子与具有纳米尺寸孔道结构的沸石载体复合，使其具有抗菌功能，然后将复合了银离子的沸石实施人工活化和二次颗粒孔分布改造，使对氨气，硫化氢，甲醛等异味气体具有快速吸附功能，最后再加入废玻璃粉、粘土等辅助原料，用硅胶溶液造粒，将做好的粉体烧结成便于使用的颗粒。

South of companies Linfei Chang calcium superphosphate workshop for the silica gel filtration, washing and pressing.

南化公司磷肥厂用于普钙车间硅胶的过滤、洗涤和压榨。

The electrochemical characteristics of toluidine blue immobilized within self-assembled silica gel were studied in detail.

实验中，详细探讨了甲苯胺蓝在凝胶组装修饰电极中的电化学行为。

Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车，和一双合并为一移交&整个lotta爱&。

This is Kate, and that's Erin.

这是凯特，那个是爱朗。