查询词典 silica gel

The main object of this research is to investigate synthesis of Cu23Cl Cu and CuO nanoparticles through electrospinning and heat-treated method The research is mainly focused on preparative parameter and the change of heat-treated temperature to form the nanoparticles inlaid in silicon fibers the shape and color change are dicussed First of all to prepare the Polyvinyl butyral and silica dioxide complex nanofiber by electrospinning and then to investigate different heat-treated temperature and reactive time to being an influence on the products The results detected by SEM XRD TEM EDS FTIR combined sol-gel process and electrospinning can prepare Polyvinyl butyral and silica complex nanofiber The experimental result is found when heat-treated temperature is 100~4750C it can produce Cu23Cl nanoparticles; Above 4750C~ 4900C it can produce Cu nanoparticles; Above 450~7000C it can produce CuO nanoparticles And the viscosity is lain between 20~40cp and the sol-gel process time is 3hr it can produce the thinner fibers The average diameter of the fibers are 107 88±21 01nm;Due to the nanoparticles inlaid in the silica fibers the thinner fibers can be inlaid the smaller nanoparticles so this is the result that the experiment is expected To calcine the complex fibers is to produce surface silica fibers contain Cu23Cl Cu and CuO nanoparticles due to surface plasma resonance it make the color of the fibers become yellowish green from light white green turn into the red nuclear finally As the experimental result to utilize sol-gel process combine electrospinning can produce porous silica fibers contain Cu23Cl Cu and CuO nanoparticles

本研究旨在探讨「利用放电纺丝和热处理法来合成Cu23Cl、Cu和CuO奈米粒」之研究，实验著重在制备参数与热处理温度变化对所形成的奈米粒镶嵌在二氧化矽纤维中的形态与颜色变化探讨。首先，利用放电纺丝法制备出聚乙烯醇缩丁醛及二氧化矽之奈米纤维，比较不同的热处理温度与反应时间的改变对产物生成产生影响，进而研究不同热处理温度和时间对生成奈米粒的影响。产物经由SEM、XRD、TEM、EDS和FTIR等仪器分析结果显示，结合溶胶-凝胶法(sol-gel process)和放电纺丝法可产生聚乙烯醇缩丁醛及二氧化矽复合奈米纤维。实验结果发现，若热处理温度在100~4750C下可得到Cu23Cl奈米粒，475~4900C 可得Cu奈米粒，450~7000C以上可得 CuO奈米粒。而黏度介於20~40cp间和溶胶-凝胶时间为3hr时，可产生直径比较细的纤维，纤维直径为107 88±21 01nm；且由於奈米金属颗粒镶嵌在二氧化矽纤维中，直径比较细的纤维，可以得到比较小的奈米金属颗粒，这与实验预期相符。而锻烧此复合物产生多孔的二氧化矽纤维并包含Cu23Cl、Cu和CuO奈米微粒时，由於表面电浆子共震关系，而使纤维颜色由淡白黄绿色变成黄绿色，再变红褐色。由实验结果得知，利用溶胶-凝胶法(sol-gel process)结合放电纺丝法和不同热处理温度，可产生Cu23Cl、Cu和CuO奈米粒镶嵌在二氧化矽纤维。

In order to install the electrothermic Board, silica gel used for blocking the release version of silica gel used for blocking the General selection of grass-roots level to 1-3 mm in thickness of the aluminum plate. Silica gel layer from the aluminum plate between the bond strength directly linked to silica gel used for blocking the version of the service life, if the silican layer from the aluminum plate between the bond strength is not high enough, the high temperature and high pressure easy to crack.

当然，在本质操纵洋上述几个参数的设定不是白云苍狗的，而给根据本质处事洋的需给举行拔取和设定，如铜、锌版不同，平均的烫印压辛、较矮的烫印温量和较缓的烫印速率会爆发更抱负的烫印成果，因为平均的烫印压辛使电化铝的黏结性更好，较矮的烫印温量使电化铝的光华量更矮，而较缓的烫印速率是为了适答较矮的烫印温量。

According to different technological requirements of battery component, B series automatic laminating machines can set different technological parameters, boast reasonable and compact structural design, as well as the design of stable continuous feeding and discharge mechanism; PLC automatic control, high-definition touch screen display, humanistic intelligence control system; urgent, emergent and accurate alarm system is able to deal with unexpected states of the equipment, to ensure that the equipment is safe and reliable and the components are not damaged; oil heating style and thickened hot plate make the temperature more equal and even; unique tightening structure of silica gel plate further smoothes the tightening of silica gel plate, prevents the frilling of silica gel plate, and makes the replacement of silica gel plate quicker and more convenient.

B系列全自动层压机可根据电池组件不同的工艺要求，设置不同的工艺参数，合理紧凑的结构设计，稳定的连续式出入料机构设计；PLC自动控制，高清晰触摸屏显示器，拥有人性化智能控制系统，设置紧急、应急及准确的报警系统以应对设备突发情况，保证设备安全可靠，使组件不受损伤；采用油加热方式，加厚热板，温度更均匀；独特的硅胶板张紧机构设计，使硅胶板的张紧更平整，杜绝硅胶板的起褶现象，硅胶板更换更方便快捷。

Our country produces late , among them silica gel product starting A, orbed B type silica gel Yu 1973 Enterprise develops out and industrialization produces some annual Shanghai chemical industry, have filled in the blank space packing in the homeland with silica gel.

我国生产硅胶产品起步较晚，其中A，B型球状硅胶于1973年上海某化工企业研制出并工业化生产，填补了国内包装用硅胶的空白。

The effect of the amount of silica powder and sulfuric acid employed as well as polyacrylamide added on the properties of the gel electrolyte was studied and the mechanism of the peptization of silica powder to form thixotropic silica gel electrolyte was discussed.

研究了SiO2粉末和H2SO4用量及聚丙烯酰胺添加量对凝胶电解液性能的影响，并分析讨论了SiO2粉末胶溶形成触变性硅凝胶电解液的机理和特点。

The purification-pretreatment technique of 8 kinds of solid phase extracting column stuffing (silica gel, acid silica gel, Florisil, siliceous magnesium sorbent, Al2O3, celite 545, acid celite, Al2O3+silica gel) for the prepared polluted soil containing 13 kinds of organochlorine pesticides (α-HCH,β-HCH,γ-HCH,δ-HCH, o,p'-DDT, o,p'-DDE, p,p'-DDT, p,p'-DDD, p,p'-DDE, a-endosulfan, dieldrin, endrin, hexachlorobenzene) was screened prior.

用製备的8种固相萃取柱填料（硅胶，酸化硅胶，氟罗里硅土，硅镁型载体，Al2O3，硅藻土载体545，酸性硅藻土，Al2O3+硅胶）对含有13种有机氯农药的污染土壤的纯化预处理技术进行了优化筛选。

One route was that the amino-groups on the silica gel were transformed to tertiary amines by Eschweiler-clarke reaction that amine-groups react with formaldehyde and methanoic acid to prepare tertiary amines; the silica gel intermediates with tertiary amine groups reacted with chorohydrocarbons to prepare insoluble silica gel quaternary ammonium salt bactericides. Another route was that the amino-groups on the silica gel reacted with excessive chlorohexadecane; the preparing intermediates were quaternized with iodomethane to obtain insoluble silica gel quaternary ammonium salt bactericides.

一条路线是根据埃施韦勒-克拉克(Eschweiler-clarke)胺甲基化反应，进行胺基叔胺化反应，制成带有叔胺官能团的硅胶中间体，此中间体上的叔胺与卤代烷反应生成杀菌活性官能团季铵盐，制成硅胶类水不溶性季铵盐杀菌剂；另一条路线是带有胺反应活性中心的硅胶与过量正氯代十六烷反应，得到的中间体再用碘甲烷季铵化，得到最终产品——水不溶性季铵盐杀菌剂。

Three part of research works had been carried out in the dissertation. The first part: a kind of multidentate amine modified silica gel was synthesized through the following steps:(1) introduce the amino groups onto the surface of silica-gel by the treatment of surface silanol groups withγ-aminopropyl trimethoxy silane;(2) michael addition of excess trihydroxymethyl propyl triacrylate to amino groups on the silica gel surface;(3) amidation of the unreacted double bonds of TMPTA on the surface of TMPTA modified silica gel with diethylenetriamine;(4) the multidentate amine modified silica gel was finally obtained by the reaction of amino groups on the surface of DETA modified silica gel with double bond of butyl acrylate.

本论文进行了三部分研究工作，第一部分：通过多步反应对硅胶进行改性合成了一种多齿胺改性硅胶配体，合成过程如下：1通过γ-氨丙基三甲氧基硅烷与硅胶表面的硅羟基反应，使硅胶表面带有氨基；2利用硅胶表面氨基与过量的三羟甲基丙烷三丙烯酸酯发生Michael加成反应；3利用二乙烯三胺与TMPTA改性硅胶表面未反应的双键发生反应使硅胶表面氨基化；4最后用丙烯酸正丁酯与DETA改性硅胶表面氨基充分反应成功合多齿胺改性硅胶配体。

By contrasted with silica gel, the corn hull desiccants by hydrolyzation method and heat treatment method have advantages as stabilization on moisture adsorption, less water of reversible adsorption and high moisture adsorption ratio in high humidity. These desiccants have disadvantages as lower moisture ratio than silica gel in low humidity and slower moisture adsorption speed than silica gel. The corn hull desiccant by derivation method has advantages as high moisture adsorption ratio, high moisture adsorption speed, stabilization on moisture adsorption and hardly any water of reversible adsorption.

通过与变色硅胶干燥剂的对比，通过水解法和热处理法得到的玉米渣皮干燥剂的优点是吸水稳定，可逆吸附水少，在高湿度下吸水率高，不足是在较低的湿度下，吸水率比变色硅胶干燥剂略低，吸水速度比硅胶慢；通过衍生方法得到的玉米渣皮干燥剂的优点是吸水率高，吸水速度快，吸湿稳定持久，几乎不含可逆吸附水，不足是再生后产品容易结块。

Amino functional silica gel was synthesized by reacting silane coupling agent with silica gel. Then dendrimer-like polyamidoamine on the silica gel surface was prepared using Micheal addition of the amino and methyl acrylate, and ester-exchange of ethylene diamine and the ester group.

用硅烷偶联剂对硅胶表面进行氨基功能化，利用氨基与丙烯酸甲酯发生的Michael加成反应和乙二胺与酯进行的交换反应在硅胶表面合成了聚酰胺－胺树状大分子。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。