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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area;2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support;3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier;4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling;5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene PolymerizationIn this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that:1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS;2.co-mlling time had no obvious effect on the texture of support after 12 hours;3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.
XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现;3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布;4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒;5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明:1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致;2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响;3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。
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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.
XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现; 3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布; 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒; 5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明: 1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致; 2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响; 3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。
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The research shows that the development of eco-environment and socio-economy belongs to environment lag-type of coordinated s development kind. From 2001 to 2004, the coordinated development value descended year by year. The sustainable development level shows degressive trend.
分析结果表明:成都市生态环境与社会经济之间属于协调发展类环境滞后型,且2001~2004年协调发展值逐年下降,可持续发展情况呈下降趋势。
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During an attack of parenchymal involvement, a typical magnetic resonance imaging examination shows a BS lesion extending to diencephalic structures, or to basal ganglia region[11], and cerebrospinal fluid examination usually shows pleocytosis and mild protein elevation.
当中枢神经系统实质受累时,于发作期行MRI典型的表现为从脑干延伸至间脑结构甚至基底节区的病灶;行脑脊液检查常可见细胞数增多、蛋白含量轻度升高
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In general, the chrome-included solution with the rain shows alkalescent, so it shows significant practical value to electrolyze and reduct Cr6+ in alkalescent media directly to dispose the extraction of chromium residues to disposal the chromium waste pollutant.
一般情况下,雨水淋淅出的含铬液体呈弱碱性,因此,直接在弱碱性介质中采用电解还原Cr~(6+)来处理铬渣浸出液,以治理铬渣污染具有实际意义。
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In the cuttage of rose ,five stromata were adopted in order to study their influence on the growth of the branches. The result of the experiment shows that vermiculite can ensure the highest survival rate. In the experiment, epicormic branches are treated with IBA at different concentration. The result shows that 200mg/L IBA can also promote the epicormic branch to root. The rooting rate is 91.0%. Temperature plays an important role in rose cuttage.
研究了5种不同基质对多头玫瑰插穗扦插繁殖的影响,结果表明:不同基质扦插成活率不同,以蛭石最好;在试验中,用吲哚丁酸IBA不同浓度溶液处理扦穗,结果表明: 200mg/L吲哚丁酸IBA对多头玫瑰扦插生根有很大的促进作用,生根率为91%;温度对多头玫瑰的扦插也有很大的影响。
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There are experimental results as follows:(1) Eriophorum comosum Nees shows strong cold resistance in plasmalemma permeability research. The lethal temperature of Eriophorum comosum Nees is the lowest LT_(50 in comparison with another two plants and is lower than -11.5℃ in August 2005 and December 2005; Soluble protein content of each plant is rising before or after cold hardiness. By SDS-PAGE, Protein band is analysed. Band quantity of Eriophorum comosum Nees is the most and its band color is darkest.(2) Soluble sugar content of three plants after cold hardiness are higher than before cold hardiness, moreover soluble sugar content after cold hardiness shows a decline and there is a narrow range in Eriophorum comosum Nees; Free Proline accumulation is changed by cold stress, and cold resistance is relative to free Proline accumulation; chlorophyll content of both three plants, including chlorophyll a, chlorophyll b and chlorophyll a/b, show a decline tendency along with the descent of temperature. Cynodon dactylon is highly sensitive to cold stress.(3) The soil POD and urease activities' absolute value of Erioophorum comosum Nees and Pogonatherum panideumHack were more than that of Cynodon dactylon before or after low temperature stress, especially POD activities.
实验结果表明:(1)在膜透性的研究中,丛毛羊胡子草抗寒性最强,采用电导率法测得半致死温度LT_(50最低,丛毛羊胡子草抗寒锻炼前后半致死温度LT_(50均小于-11.5℃;在可溶性蛋白含量研究中,抗寒锻炼前后三种植物的可溶性蛋白含量均增加,同时采用SDS-PAGE法,通过对蛋白条带分析,以丛毛羊胡子草条带数最多且着色深;(2)在可溶性糖的研究中,三种植物经抗寒锻炼后叶片可溶性糖含量都比抗寒锻炼前高,且经过抗寒锻炼后三种植物可溶性糖均呈下降趋势,丛毛羊胡子草可溶性糖含量下降较小;从游离脯氨酸含量可知,低温的胁迫影响了植物叶片游离脯氨酸的含量变化,植物的抗寒性与游离脯氨酸有关;低温胁迫下三种植物叶绿素含量随着温度的下降,叶绿素含量、叶绿素a、叶绿素b和叶绿素a/b均呈下降趋势,狗牙根对低温胁迫最为敏感;(3)低温锻炼前后,丛毛羊胡子草和金发草的土壤过氧化物酶与脲酶活性的绝对值均大于狗牙根的,特别是过氧化物酶,说明丛毛羊胡子草和金发草的酶活性大于狗牙根的。
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Four types of reservoirs in the member have been classified according to the standard, combined with the explorational practice. The result shows that the reservoirs in the member are poor in both porosity and permeability. Their pore-throat distribution shows three...
研究结呆表明,塔中地区志留系下砂岩段储层表现为低孔低渗的储集特征,孔喉类型为单峰中孔、单峰细孔和单峰微孔型,以Ⅱ、Ⅲ类储层为主,Ⅱ类储层主要分布在下砂岩段下部,在塔中20至塔中30并区较发育,是塔中志留系勘探的有利区带。
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Notably, compounds 12–14 can be described as a 3D open–framework with nano–channels, compound 15 can be described as a 3D open–framework with double helical channels, while compound 16 can be described as a 3D heterochiral coordination polymer with double helical channels, which can be obtained by spontaneous resolution from the racemic phosphonic acid.X–ray powder diffraction analysis shows that compound 16 is a pure phase. Surface photovoltage spectroscopy of compound 16 indicates that it possesses positive SPV response in the range of 300–600 nm and shows p–type semiconductor characteristic.
值得注意的是,化合物12-14为具有一维纳米孔道结构的三维开放骨架结构,化合物15是具有双螺旋孔道的三维开放骨架结构,而化合物16是外消旋的有机膦酸配体通过自发拆分而形成的具有双螺旋孔道的多手性三维开放骨架结构。X-射线粉末衍射分析表明化合物16为纯相;化合物16的表面光电压光谱分析中,在300-600nm范围内有3个正的光(来源:ABC论文12网www.abclunwen.com)伏响应带,表明它具有p型半导体的特征;化合物16的诱导表面光电压谱进一步确定它的p型半导体的特征;磁性研究表明,化合物16中两Mn原子之间存在弱的反铁磁相互作用。
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The result makes clear, 2 class give urban sewage plant on the molecular quantity interval that organic owner should center the dissolvability in water water in kDa, and the content of organic matter compares hydrophoby the element of content big; of organic matter measures hydrophily interval distributings different organic thing shows water to accept filter film flux and hold back rate having distinct effect, the organic matter under molecular quantity 2kDa causes accept filter film to appear water flux attenuation bigger, organic matter is held back rate is minor, the organic matter that amounts to 57.2%; element to measure 10 ~ 100kDa causes accept filter film to appear water flux attenuation gentlier, organic matter is held back rate is older however highest the organic matter that amounts to 73.8%; to kiss scanty sex to differ shows water to accept filter film flux and hold back rate having distinct effect, classics is right of velar surface obstruction determine, confirm cause film to appear water flux and the main material that hold back rate change to be hydrophoby material, and the change that hydrophily material causes is minor.
结果表明,城市污水厂二级出水水中的溶解性有机物主要集中在kDa的分子量区间上,且疏水性有机物的含量比亲水性有机物的含量大;分子量区间分布不同的有机物对纳滤膜透水通量和截留率有着不同的影响,分子量2kDa以下的有机物引起纳滤膜透水通量衰减较大,有机物截留率较小,达57.2%;分子量10~100kDa的有机物引起纳滤膜透水通量衰减较平缓,有机物截留率却较大最高达73.8%;亲疏性不同的有机物对纳滤膜透水通量和截留率有着不同的影响,经对膜表面阻力的测定,证实引起膜透水通量和截留率变化的主要物质为疏水性物质,而亲水性物质引起的变化较小。
- 相关中文对照歌词
- Shows
- Love These Goon Shows!
- One Man Shows
- When Anger Shows
- Water Shows The Hidden Heart
- Get Busy Living Or Get Busy Dying (Do Your Part To Save The Scene And Stop Going To Shows)
- Talk Shows On Mute
- That Shows You What I Know
- Game Shows Touch Our Lives
- Moons And Horror Shows
- 推荐网络例句
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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.
随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。
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But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.
不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。
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Closes the eye, the deep breathing, all no longer are the dreams as if......
关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。