查询词典 sample method

No entire nitrendipine crystals were observed visually in SEM photos. The results of X-ray diffraction and differential scanning calorimetry analysis indicated that the crystalline form of nitrendipine was highly dispersed in microspheres, so as amorphous state. The drug release rate of microspheres could be controlled with adjusting the ratio of solid dispersion carriers and retarding agents formulated. The agitation speed and temperature of the preparation process have distinct effect on micromeritic properties of microspheres. The release profiles of the microspheres were mainly affected by the stirring rate of paddle, the concentration of SDS and pH of dissolution medium. Cooling speed and time, however, have no evident influence on the drug release rate of the microspheres. The dissolution data showed that the mechanism of drug release from microsphers was mainly diffusion-controlled. The incorporation efficiencies of 3 batches sample were exceed 96. 8％, which implied that the current method was suitable for design sustained-release dosage form for poorly water-soluble drug.

在扫描电子显微镜下观察，在微球内外未发现尼群地平的完整结晶，X-射线粉末衍射和差示扫描量热试验结果也显示，尼群地平已经被高度分散在微球中；微球的释药速度可通过调整处方中固体分散体载体和阻滞剂的比例控制；制备温度和搅拌速度对微球的质量影响较大；溶出仪的搅拌速度，释放介质的浓度和pH对微球的释放有较大的影响；制备过程中的冷却速度和冷却时间对微球的释放行为影响不很明显；方程拟合的结果表明缓释微球的释药行为符合扩散机制；测定三批微球样品的包封率均在96.8％以上，表明该法适合于制备难溶性药物的缓释微球。

The SVM method is based on the theory of structural risk minoration. It can map the sample space to a higher feature space by selecting an optimal Kernel function, and get a linear regression in this higher feature space.

中文摘要：支持向量机方法是基于结构风险最小化原理提出的，通过采用合适的核函数将样本空间映射到一个高维特征空间，再在高维特征空间进行线性回归。

A method for the determination of mixedness degree of red mud and limestone by spectrophotometry with 1,10-phenanthroline was developed. The mixture of red mud and limestone was dissolved by hydrochloric acid, and iron content in the sample solution was determined by spectrophotometry with 1,10-phenanthroline.

用盐酸提取赤泥和石灰石的混合料后，通过邻二氮菲分光光度法测定提取液中铁含量，进而求得混合料中氧化铁的质量分数，以此来衡量混匀度。

A method for the determination of phenol and catechol in tobacco leaf by high performance liquid chromatography with methanol and 0.05 mol/L of monopotassium phosphate as mobile phase at a flow rate of 0.5 mL/min was described. Phenol and catechol were extracted from tobacco sample by distillation and solid phase extraction with Sep Park C 18 cartridge.

引 言挥发酚是烟草中一类重要的成分，它在烟草燃烧时直接进入烟气，大多有不好的气味，而且很难被掩盖；特别是苯酚和儿茶酚对呼吸系统有腐蚀作用和助癌作用，近年来逐渐引起了烟草化学工作者的注意〔1〕。

In the paper, the multidentate carboxylic acid ligands were used to combine with Cd, resulting in the three dimensional MOCPs single crystals—C12H16CdN2O8, with a low temperature hydrothermal synthesis method. The sample was characterized with IR spectra to affirm the organic groups in the frameworks, single-crystal X-ray diffraction to determine the crystal structure and composition of the frameworks, N2 adsorption isotherms at low temperature to measure the specific surface area and pore size distribution, and with TGA/DGA analysis to scale the thermal stability. Furthermore, the dissolution property and the photocatalytic activity of MOCPs under the ultraviolet ray condition were explored.

本文用低温水热合成法，用多齿羧酸配体异烟酸和Cd配位合成出[Cd(C6H4O2N)2(H2O)4]∞三维晶体并进行了表征：采用红外光谱法确认骨架中的有机官能团；用单晶X射线衍射分析法测定MOCPs的晶体结构，并确定其骨架的组成；通过低温氮气吸附等温线测定了其比表面积和孔径分布；以热重分析和差热分析测定材料骨架的热稳定性；测定了晶体的溶解性能；最后以亚甲基蓝为目标降解物，对[Cd(C6H4O2N)2(H2O)4]∞的光催化活性及亚甲基蓝的氧化动力学进行了探索(来源：A2444BC论文网www.abclunwen.com)。

Moreover, we examine how the agency cost between managers and liquid shareholders is affected by nonliquid shares and stateowned shares, which we believed to exist only in Chinese Market. Through the same method of event study, we find a symmetric effect regardless of the proportion of nonliquid shares, and this shows that the proportion of nonliquid shares is not a factor of conflicts between managers and liquid shareholders. As for the sub-sample with stateowned shares, there is a larger positive price impact for firms with high proportion of stateowned shares, which tells us that the stateowned shares do raise the problem of "absence of the owner", and it is a part of agency cost in China.

我们进一步检验了国内特殊存在的非流通股以及国有股对于管理层与流通股东之间代理成本的影响，通过同样的事件研究方法对上述样本进行市场宣告反应检验，结果发现非流通股比例不同的公司其市场反应并无显著差异，说明非流通股的存在对管理层与流通股东之间的代理问题没有影响；而国有股比例不同的公司其市场宣告反应存在显著差异，这说明国有股产生的&所有者缺位&问题成为国内代理成本的一部分，并确实影响了现金股利的发放。

In this paper we present a shear force nonoptical detection method for tip-sample distance control, which is realized by using a piezoelectric bimorph cantilever.

我们采用双压电陶瓷片发展了一种切变力非光学检测探针-样品间距控制方法。

Random sampling is simply a method of selecting item s for inclusion in a sample; it can be used in conjunction with either stati stical or nonstatistical sampling.

随机采样仅仅是选取样本项目的一种方法，它既可以用于统计抽样，也可以用于非统计抽样。

The oxidable potential difference of DA and AA was about 184 mV at Poly-Evans Blue modified electrode. So it is used to simultaneously determine the DA and AA without any interference. The interference of other components could be efficiently eliminated at the modified electrode, and this method can be used for determination of DA and AA in real sample with satisfactory results.

当DA与AA共存时，由该修饰电极检测的二者氧化峰电位差达184mV，故可同时测定DA和AA，并有效消除其它组分对DA测定的干扰，已用于实际样品中DA和AA含量的测定，结果令人满意。

Slaking pretreatment: distilled water and potassium persulphate solution are added and placed into a slaking hole of a COD slaking instrument, and simultaneously blank solution is taken and processed together with a sample to be detected with the same method; C.

消解预处理：加入蒸馏水和过硫酸钾溶液，置于COD消解仪的消解孔中；同时另取空白溶液，与待测样品同时以同样方法处理；C。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。